Rectification-molecular sieve membrane coupling process and device for ternary water-containing eutectic system separation
A coupling device and molecular sieve technology are applied in the field of ternary system rectification-membrane separation coupling technology devices, which can solve the problems of azeotropic system separation, limited practical application system, low processing capacity of membrane separation process, etc. The effect of low capacity, reduced process energy consumption, and reduced reflux ratio
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[0034] The technical problem to be solved by the present invention is to provide a ternary system rectification-molecular sieve membrane coupling device and its operation method, so that the device can be widely applied to the separation of ternary azeotropic systems, not only solving the problem of traditional rectification process The difficult problem of azeotropic system separation, and the problem that the low processing capacity of the membrane separation process leads to the limitation of the practical application system.
[0035] The structure of the rectifying column of the coupling technique provided by the invention is as figure 2 with image 3 As shown, in the figure, the rectification tower is made of multi-stage trays, wherein at least one stage tray 1 is provided with a molecular sieve membrane module 2 inside, and the molecular sieve membrane module 2 used here is filled with a molecular sieve membrane, and the molecular sieve The membrane can be NaA, ZSM-5, ...
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