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Method for preparing compound HSS-8 from traditional Chinese medicinal material physochlaina macrophylla

A technology for compounds and Chinese medicinal materials, applied in the field of preparing compound HSS-8, to achieve the effect of broadening the preparation route

Pending Publication Date: 2020-09-29
HENAN UNIV OF CHINESE MEDICINE
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  • Abstract
  • Description
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Problems solved by technology

[0005] At present, there is no report about the compound HSS-8 contained in Huashan ginseng or other plants of the genus Physiophthora where Huashan ginseng belongs

Method used

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  • Method for preparing compound HSS-8 from traditional Chinese medicinal material physochlaina macrophylla
  • Method for preparing compound HSS-8 from traditional Chinese medicinal material physochlaina macrophylla
  • Method for preparing compound HSS-8 from traditional Chinese medicinal material physochlaina macrophylla

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Embodiment Construction

[0024] The following describes the substantive content of the present invention in detail in conjunction with the drawings and embodiments, but does not limit the protection scope of the present invention.

[0025] The method for preparing compound HSS-8 from Huashan ginseng comprises the following steps:

[0026] Step S1, pulverize 2 kg of Chinese medicinal material Panax ginseng, soak and extract with 95% ethanol (5 L × 3 times), combine the extracts, and concentrate under pressure to obtain 473 g of crude extract;

[0027] Step S2, suspending the crude extract obtained in step S1 with 2L of water, extracting with n-butanol (2L × 3 times), collecting the n-butanol extract, and concentrating to obtain the n-butanol extract extract;

[0028] Step S3, take step S2 gained n-butanol extract extract (65g) and use normal phase silica gel column chromatography to use dichloromethane:methanol=20:1 (4 column volumes), 10:1 (4 column volumes) ) elution, and according to TLC analysis, ...

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Abstract

The invention discloses a method for preparing a compound HSS-8 from a traditional Chinese medicinal material physochlainae macrophylla. The invention discloses a method for preparing a compound HSS-8by taking physochlaina macrophylla as a raw material for the first time. In the prior art, the compound HSS-8 contained in the physochlaina macrophylla is not reported, and the compound HSS-8 contained in other plants in the physochlaina where the physochlaina macrophylla is located is not reported. The method broadens the preparation way of the compound HSS-8, and compared with the prior art, the method has outstanding substantive features and remarkable progress.

Description

technical field [0001] The invention belongs to the field of natural medicine chemistry and relates to a method for separating and preparing known compounds, in particular to a method for preparing compound HSS-8 from Chinese medicinal material Huashan ginseng. Background technique [0002] Huashan ginseng is the dry root and rhizome of Physochlaina infundibularis Kuang, a plant of the genus Physochlaina in the Solanaceae family. It was first seen in "Supplements to Compendium of Materia Medica" written by Zhao Xuemin in the Qing Dynasty. Ginseng, drunken grass, etc., perennial herbs, are special medicinal plants in my country. They are mainly distributed in the central to eastern Qinling Mountains of Shaanxi, western and southern Henan, and southern Shanxi. They have been listed as national second-class protected plants. Its roots are used as medicine, hot in nature, sweet, slightly bitter, and astringent. Functions and indications Cure cold phlegm cough, heart palpitations...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07C235/34C07C231/24
CPCC07C235/34C07C231/24
Inventor 王潘李军张丽萍赵璇娄勇许瑞珠高改谢治深张振强徐江雁
Owner HENAN UNIV OF CHINESE MEDICINE
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