One-pot preparation method and application of composite photocatalyst cds/zif-8
A ZIF-8, composite light technology, applied in organic compound/hydride/coordination complex catalysts, chemical instruments and methods, physical/chemical process catalysts, etc., can solve the problem of unsuitable industrial production applications, complex preparation steps, etc. problem, to achieve the effect of high-efficiency photo-splitting water hydrogen production performance, simple process, and few method steps
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Embodiment 1
[0043] In this example, a one-pot method is used to prepare the composite photocatalyst CdS / ZIF-8, and the steps are:
[0044] (1) Add 1mmol Zn(NO 3 ) 2 ·6H 2 O and 9mmol Cd(NO 3 ) 2 4H 2O was added into 100mL of methanol together, stirred until clear and transparent, and solution A was obtained.
[0045] (2) 18mmol C 4 h 6 N 2 (2-Methylimidazole) was added into 100 mL of methanol, stirred until clear and transparent, and solution B was obtained.
[0046] (3) After mixing solutions A and B, let them stand for aging for 11 hours, and then add 27 mmol CH to the mixed solution 4 N 2 S (ammonium thiocyanate), stirred for 3h, and centrifuged to obtain a yellow reaction product.
[0047] (4) After the reaction, the reaction product was alternately washed three times with distilled water and ethanol, and dried at 50°C to obtain the supported composite photocatalyst CdS / ZIF-8.
[0048] During the one-pot preparation of CdS / ZIF-8, adding Zn ions, Cd ions and excess 2-methyl...
Embodiment 2
[0050] This embodiment is on the basis of embodiment 1, the "18mmol C in step (2) 4 h 6 N 2 (2-Methylimidazole)" was changed to "27mmol C 4 h 6 N 2 (2-Methylimidazole)".
Embodiment 3
[0052] This embodiment is on the basis of embodiment 1, the "27mmol CH in step (3) 4 N 2 S (ammonium thiocyanate)" to "36mmol CH 4 N 2 S (ammonium thiocyanate)".
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