Vaginal effervescent tablets for treating woman's inflammation and their preparation
A technology for gynecological inflammation and effervescent tablets, which is applied in the field of Chinese patent medicine for treating gynecological inflammatory diseases and its preparation, which can solve the problems of high cost, inconvenient transportation and storage, and inability to extract it, so as to increase the utilization rate and improve the efficacy of the medicine , the effect of reducing production costs
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Embodiment 1
[0040] Example 1 Preparation of Medicinal Powder for the Treatment of Gynecological Inflammation
[0041] Raw material formula: rhubarb 248g, comfrey 100g, catechu 10g, borneol 7g.
[0042] Preparation method: (1) take rhubarb and comfrey, extract 3 times with 88% ethanol, each time for 2 hours, filter, and use the dregs for later use, add β-cyclodextrin 60g, PVPk30 60g and poloxamer 10g to the filtrate, Mix well, recover ethanol under reduced pressure, and obtain concentrated solution of alcohol extraction; take medicinal residues and add water to decoct twice, 1.5 hours each time, filter, and centrifuge the filtrate at high speed, concentrate the centrifugate to a relative density of 1.23 (60°C), and extract with alcohol The concentrates are combined, spray-dried and pulverized to obtain rhubarb and comfrey extract powder;
[0043] (2) Take borneol, 56g of β-cyclodextrin, and refer to the method [Song Hongtao, et al. Journal of Shenyang Pharmaceutical University. pink;
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Embodiment 2
[0046] Example 2 Preparation of Medicinal Powder for Treatment of Gynecological Inflammation
[0047] Raw material formula: rhubarb 210g, comfrey 120g, catechu 12g, borneol 8g.
[0048] Preparation method: (1) get rhubarb, be crushed into coarse powder, sterilized, and ultrafinely pulverized into ultrafine powder with particle diameter≤10um to obtain rhubarb ultrafine powder;
[0049] (2) Get comfrey, extract 2 times with 95% ethanol, each time for 2.5 hours, filter, the dregs are for subsequent use, add PVPk30 70g, hydroxypropyl methylcellulose (HPMC-E5) 30g, soybean lecithin 8g to the filtrate , fully stirred evenly, recovered ethanol under reduced pressure, and concentrated to obtain a concentrated solution for alcohol extraction; take the dregs and add water to decoct twice, each time for 1 hour, filter, and the filtrate was centrifuged at a high speed, the centrifugate was concentrated to a relative density of 1.38, and extracted with alcohol The concentrates were combin...
Embodiment 3
[0052] Example 3 Preparation of Medicinal Powder for Treatment of Gynecological Inflammation
[0053] Raw material formula: rhubarb 218g, comfrey 110g, catechu 13g, borneol 6g.
[0054] Preparation method: (1) get rhubarb, be crushed into coarse powder, sterilized, and ultrafinely pulverized into ultrafine powder with particle diameter≤10um to obtain rhubarb ultrafine powder;
[0055] (2) Take comfrey, extract 3 times with petroleum ether, each time for 1.5 hours, filter, and use the dregs for later use, combine the filtrates, recover petroleum ether under reduced pressure, add 80g of PEG6000, 30g of hydroxypropyl-β-cyclodextrin to the residue , lecithin 5g, ethanol 550ml, after heating and refluxing for 40min, ethanol is recovered under reduced pressure, freeze-dried, and crushed at low temperature to obtain fine powder of solubilized matter of comfrey fat-soluble extract: take the dregs and add water to decoct twice, each time for 1.5 hours , filtered, the filtrate was cent...
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