Preparing method for phenol series substances
A series and material technology, applied in the field of preparation of phenolic series substances, can solve the problems of difficult to obtain valuable utilization of lignin, conversion rate, catalytic technology, and economical efficiency, etc., to reduce investment The cost effect of recycling and recycling
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Embodiment 1
[0026] Nitrogen: sulfur: oxygen: a mixture of hydrogen elements, the weight mixing ratio = 0.6: 2.1: 1.8: 0.35, then add activated carbon accounting for 60% of the weight of the mixture, and stir at 110 ° C for 3 to 4 hours to make a catalyst ,spare. After the pulping waste liquor from the chemical treatment process is separated from the pulp fibers, a lignin-containing waste liquor with a concentration of 10% is obtained. The waste liquid is concentrated and spray-dried to prepare crude lignin dry powder with a water content of less than 15% and an inorganic matter content of less than 4%.
Embodiment 2
[0028] In addition to the mixture of nitrogen: sulfur: oxygen: hydrogen elements, its weight mixing ratio=0.5:2.0:1.7:0.3, then add activated carbon accounting for 50% of the mixture by weight, and stir at 100 ° C for 4 hours, other processes With embodiment 1.
Embodiment 3
[0030] In addition to the mixture of nitrogen: sulfur: oxygen: hydrogen elements, the weight mixing ratio=0.7: 2.3: 1.9: 0.4, then add activated carbon accounting for 70% of the weight of the mixture, and stir at 120 ° C for 3 hours; Except that the waste liquid is dried by air flow, other processes are the same as in Example 1.
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