Process for synthesizing anode material of lithium ion cell
A technology for lithium ion batteries and cathode materials, which is applied in the field of synthesizing cathode materials for lithium ion batteries, can solve problems such as environmental pollution, waste of water resources, pollute the environment, etc., and achieve the effects of reducing costs and saving water sources.
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Embodiment 1
[0014] Example 1: At room temperature, a certain amount of cobalt nitrate and lithium hydroxide are dissolved in water respectively to form a solution with a concentration of 3mol / L, and the two solutions are uniformly mixed and reacted until the two solutions react completely and no longer continue to generate Until the cobalt hydroxide precipitates; the mixture of the cobalt hydroxide precipitate and lithium nitrate aqueous solution formed by the reaction is filtered to form a filter cake, and the filter cake is dried to measure the amount of Li therein. Mix the dried lithium-containing filter cake with a certain amount of lithium carbonate, and the amount of lithium carbonate added is carried out according to the atomic ratio of cobalt and lithium at a ratio of 1:1 (the lithium atoms also include the lithium atoms adsorbed on the filter cake. ), and then fired at a constant temperature of 900°C for 1.5h to synthesize lithium cobaltate.
[0015] The molecular formula of lith...
Embodiment 2
[0016] Embodiment 2: at 50 ℃, at first a certain amount of cobalt nitrate, the mixture of manganese nitrate and nickel nitrate (wherein cobalt ion, manganese ion, nickel ion ratio are 1: 1: 1) and lithium hydroxide are dissolved in water respectively ( The solution concentration is 3mol / L), the lithium hydroxide solution and the mixture solution are uniformly mixed and reacted until the complete reaction of the two solutions does not continue to generate hydroxide (cobalt hydroxide, manganese hydroxide, nickel hydroxide) precipitation; The mixture of hydroxide precipitate and lithium nitrate aqueous solution was filtered to form a filter cake, the filter cake was dried, and the Li content therein was measured. Mix the dried lithium-containing filter cake with a certain amount of lithium carbonate in a ratio of 1:1.02 of cobalt+manganese+nickel atoms:lithium atoms (the lithium atoms also include the lithium atoms adsorbed on the filter cake) ), and then fired at a constant temp...
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