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Systems and methods for producing high-purity fine powders

Active Publication Date: 2021-10-14
GM GLOBAL TECH OPERATIONS LLC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patent describes a method for making high-purity fine powders without using expensive or inefficient processes. The method can use low-cost raw materials, such as recycled alloys or low-grade materials, to produce the fine powders. The method can also produce powders with a desired size and a narrow distribution, as well as cleaner and smoother surfaces compared to other methods.

Problems solved by technology

However, production of such high-purity fine powders generally requires complex, energy-intensive processes.
Such processes are overly burdensome, particularly when nanosized particles are not desired.

Method used

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  • Systems and methods for producing high-purity fine powders
  • Systems and methods for producing high-purity fine powders
  • Systems and methods for producing high-purity fine powders

Examples

Experimental program
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Effect test

example 2

[0066]A hypereutectic melt is formed including aluminum in an amount of 77.0 atomic percent on a basis of all atoms in the hypereutectic melt, silicon in an amount of 22.0 atomic percent on a basis of all atoms in the hypereutectic melt, and copper in an amount of 1.0 atomic percent on a basis of all atoms in the hypereutectic melt. The hypereutectic melt is rapidly cooled to form ribbons of a hypereutectic alloy having the same atomic percentages.

[0067]The ribbons of the hypereutectic alloy are subjected to a heat treatment at 500° C. for 4 hours to produce an annealed hypereutectic alloy. The annealed hypereutectic alloy is digested using hydrochloric acid. After treatment with hydrochloric acid, the resultant powder includes aluminum in an amount of 0.30 atomic percent on a basis of all atoms in the powder, silicon in an amount of 95.70 atomic percent on a basis of all atoms in the powder, and copper in an amount of 4.00 atomic percent on a basis of all atoms in the powder. The p...

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Abstract

Systems, methods and compositions to produce fine powders are described. These include forming a hypereutectic melt including a target material, a sacrificial-matrix material, and an impurity, rapidly cooling the hypereutectic melt to form a hypereutectic alloy having a first phase and a second phase, annealing the hypereutectic alloy to alter a morphology of the target material to thereby produce target particles, and removing the sacrificial matrix to thereby produce a fine powder of the target particles. The first phase is defined by the target material and the second phase is defined by the sacrificial-matrix material. The sacrificial-matrix material forms a sacrificial matrix having the target material dispersed therethrough.

Description

INTRODUCTION[0001]The disclosure relates to the field of metallurgy and, more specifically, to systems and methods for producing high-purity fine powders, such as substantially pure silicon, from metallurgical-grade powders.[0002]Advanced technologies, such as high energy-density batteries and electronics, employ fine powders of high-purity materials, such as silicon. However, production of such high-purity fine powders generally requires complex, energy-intensive processes. For example, purification of silicon may require formation of nanosized particles and chemical treatments, or may involve chemical conversion, distillation, and deposition. Such processes are overly burdensome, particularly when nanosized particles are not desired.SUMMARY[0003]It is desirable to form high-purity fine powders without employing high-energy and / or low-efficiency processes. Beneficially, processes described herein may be used to produce high-purity fine powders from low-cost raw materials, such as l...

Claims

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Application Information

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IPC IPC(8): C01B33/021C01B33/037
CPCC01B33/021C01B33/037C01P2006/40C01P2004/61C01P2004/62C01P2004/03C01B33/039
Inventor ABD ELHAMID, MAHMOUDBOBEL, ANDREW C.SACHDEV, ANIL K.VERBRUGGE, MARK W.PIECZONKA, NICHOLAS P.SALVADOR, JAMES R.
Owner GM GLOBAL TECH OPERATIONS LLC
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