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40results about How to "Operating parameters are easy to control" patented technology

Carbon dioxide subcritical extraction, recycling and reusing method for electrolyte of waste lithium ion battery

The invention provides a carbon dioxide subcritical extraction, recycling and reusing method for the electrolyte of a waste lithium ion battery, belonging to the field of recycling and reusing of solid waste. The method comprises the following steps: after complete discharging of the waste lithium ion battery, dismounting the waste lithium ion battery and removing a shell, positive and negative terminals, sealing rings and cover plates; transferring the electrolyte, current collectors with positive and negative electrode materials and a diaphragm into a supercritical extraction apparatus; adjusting the temperature, pressure, extraction time and flow of a supercritical carbon dioxide fluid and extracting an organic solvent and an additive; and subjecting the obtained solvent to component analysis, supplementing electrolyte salt, the organic solvent and the additive according to analysis results and adjusting a ratio to prepare electrolytes with different functions. The method effectively prevents degradation and dissipation of heat-sensitive substances; operation parameters are easy to control; extraction, separation and recovery are integrated together; later complicated treating procedures are omitted; and the utilization rate of resources is higher.
Owner:HARBIN INST OF TECH

Whey protein active peptide with antioxidant activity and preparation method thereof

The invention discloses a whey protein active peptide with antioxidant activity and a preparation method thereof. The preparation method comprises the following steps: (1) adding protease into whey protein solution for enzymolysis, wherein the enzymolysis temperature is 40-60 DEG C, and the pH value is 6.0-8.0; (2) after enzymolysis, inactivating the protease; (3) precipitating the whey protein not hydrolyzed in enzymolysis solution, and removing the whey protein to take supernatant; (4) carrying out ultrafiltration on the supernatant by an ultrafiltration membrane the cut-off molecular weight of which is less than or equal to 10,000 dalton, collecting filter liquor of peptide the molecular weight of which is less than or equal to 10,000 dalton; (5) concentrating the filter liquor; (6) desalting the concentrated liquor; and (7) concentrating the desalted solution, and then freezing and drying. In the invention, the obtained whey protein active peptide has significant antioxidant property and specific functional characteristics and stable quality, and can be widely applied to the fields of food, cosmetics, medicine and the like. The production technology is simple and is convenientfor scale production, the raw material whey protein has high use ratio, and the production cost is low.
Owner:BRIGHT DAIRY & FOOD

A method for preparing straw particle board

The invention discloses a straw particle board manufacture method, which relates to a particle board manufacture method. The invention solves the problem that the straw surface includes a plurality of waxy layers and SiO2 substance, common urea formaldehyde resin glue and phenolic resin are hard to wet the straw surface to cause a plurality of gluing difficulty. The invention has the method that: the straw is cut into pieces and performed ash removal at first, and straw crushed aggregates which are performed with the pretreatment through the blending ratio of the 1:4 to 5.0 according to the mass ratio of the straw and alkali liquor is soaked in the alkali liquor of 1.4 to 1.6 wt percent (mass) for 10 to 15 hours, and the straw particle board can be manufactured after drying, glue applying, paving, pre-pressing, hot pressing, and cooling. The equipment performance request of the straw particle board manufacture through the invention is low, the method is simple, and the operation parameter is easy to control. The method of the invention for performing chemical treatment to the straw raw material surface improves the wetting property of the raw material, greatly enhances the inner combination intensity, enlarges the application scope of the straw, releases the lack of the timber resources, and the invention has great economic and social efficiency in the situation that the conflict between supply and demand becomes more prominent.
Owner:NORTHEAST FORESTRY UNIVERSITY

Welding system and welding method of metal piece and coaxial cable

ActiveCN106112163AGood thermal conductionReliable brazing connection structureLine/current collector detailsHeating appliancesEngineeringFiller metal
The invention discloses a welding system of a metal piece and a coaxial cable. The welding system comprises a heating device which is arranged at a processing station and is in contact with the metal piece or the coaxial cable to carry out heating, a solder feeding device which is arranged adjacent to the heating device and is used for adding brazing filler metal at a connecting part of the metal piece and the coaxial cable and a moving and positioning device which is used for separately clamping and transferring the metal piece and the coaxial cable to the processing station. The invention also discloses a welding method of the metal piece and the coaxial cable. The welding method comprises the following steps: preparing the metal piece and the coaxial cable, and transferring the metal piece and the coaxial cable to the processing station; adding the brazing filler metal at the connecting part of the metal piece and the coaxial cable at the processing station, and carrying out contact heating on the metal piece or the coaxial cable to realize welding; and transferring the welded metal piece from the processing station. According to the welding system and the welding method, the brazing reliability and conduction ratio of the metal piece and the coaxial cable can be well solved, the production efficiency can also be improved, and the production cost is lowered.
Owner:COMBA TELECOM TECH (GUANGZHOU) CO LTD +2

Method for preparing and separating enkaurane-16-alkene-19-acid from wedelia trilobata

The invention relates to the technical field of extracting of plant active ingredients and discloses a method for preparing and separating enkaurane-16-alkene-19-acid from wedelia trilobata. The method comprises the following steps of: drying, crushing and sieving the wedelia trilobata; putting the wedelia trilobata powder to an extraction kettle of a supercritical extractor for extracting, wherein an entrainer is alcohol, the extracting pressure is 20MPa-25MPa, the extracting temperature is 40 DEG C to 60 DEG C, the CO2 flow rate is 30L / h to 40L / h, and the extracting time is two hours to three hours; concentrating the extract under reduced pressure to obtain total extract, dissolving the total extract in water, extracting the solution for three times by using ethyl acetate and concentrating the organic phase under reduced pressure to remove ethyl acetate to obtain the extract; loading the extract to D101 macroreticular resin, eluting using alcohol aqueous solution, collecting the eluate, and concentrating under reduced pressure to obtain a crude crystal; and re-crystallizing the crude crystal by petroleum ether to obtain the product. The method disclosed by the invention is high in extracting speed, high in efficiency, less in energy consumption, and high in yield and purity of the obtained product.
Owner:NINGBO INST OF TECH ZHEJIANG UNIV ZHEJIANG

Supercritical CO2 process for extracting effective medicinal components from Chinese angelica

The invention discloses a method for extraction of medicinal available composition from Chinese angelica with a supercritical carbon dioxide, belonging to the technique of extracting the medicinal available composition from Chinese angelica. The method contains the following process: adding the root of Chinese angelica into extraction kettle after disintegrating or cutting, and adding CO2 into extraction kettle after condensation and booster, the operation pressure of extraction being 10- 50MPa and the temperature being 32- 90 Deg. C, the mass ratio of entrainer ethanol to material being 0.5: 1- 3: 1, the entrainer being mixed and soaked with raw material or pumped by the entrainer pump and separated from solute and CO2 in separator after extraction, the pressure of the first stage separator being 3- 15MPa and temperature being 25- 40Deg. C, and the pressure of second stage separator being 3- 15MPa and temperature being 20- 30Deg. C, the product or solvent dissolved product being received from receiver, the solvent being evaporated and dried to prepare the final product, CO2 used circularly, and the whole extraction time being 0.5- 5 hours. The method has merits as the following: the energy consumption small, the operation simple, the extraction condition mild, the extraction time short, and so on.
Owner:TIANJIN UNIV

Medicinal composition soft capsules for improving anoxia tolerance and preparation method for medicinal composition soft capsules

The invention provides medicinal composition soft capsules for improving anoxia tolerance and a preparation method for the medicinal composition soft capsules, and belongs to the technical field of health-care products and the fields of medicines, food and the health-care products. The preparation method comprises the following steps of: putting crushed integripetal rhodiola herb rhizomes and bee glue into a supercritical kettle, and extracting at the temperature of between 20 and 80 DEG C under the pressure of between 20 and 80 MPa for 1 to 6 hours to obtain a composition extract; dissolving 3 grams of composition extract subjected to supercritical extraction in edible oil in an amount which is 0.5 to 1.5 times that of the composition extract in a constant volume mode, adding a preservative and an antioxidant, and mixing uniformly; and loading the uniformly-mixed medicines into a soft capsule machine to obtain the soft capsules. According to the preparation method, an extraction process is simple, the quality is controllable, the content of active ingredients of the extract is high, and the cost is low, so the preparation method is suitable for industrial production; and the medicinal composition soft capsules are convenient to take, and have an effect of improving sleep.
Owner:JILIN UNIV

Preparation method and application of N-doped FeMnO3 electrode material

The invention discloses a preparation method and application of an N-doped FeMnO3 electrode material. The preparation method comprises the following steps: Mixing ferrous sulfate heptahydrate and manganese sulfate monohydrate according to the molar ratio of iron to manganese of 1:1, adding distilled water for dissolving, and preparing an iron-manganese mixed solution; carrying out a coprecipitation reaction at a constant temperature of 25 DEG C by taking an ammonia water solution as a precipitant, and carrying out aging, filtering, washing and freeze-drying operations after the reaction is finished, so as to obtain a precursor; and weighing 0-1.5 g of analytically pure NH4HCO3, dissolving the analytically pure NH4HCO3 in 15 mL of an ethanol aqueous solution, adding 0.1 g of the precursor into the ethanol aqueous solution, uniformly stirring the mixture, transferring the mixture into a crucible, putting the crucible into a muffle furnace, and carrying out annealing treatment at 1000 DEG C to prepare the N-doped FeMnO3 electrode material. The N-doped FeMnO3 electrode material is applied to a lithium ion battery negative electrode material, the cycle performance and the rate capability of the N-doped FeMnO3 electrode material are remarkably superior to those of the FeMnO3 electrode material, and the N-doped FeMnO3 electrode material has very excellent lithium storage performance. The preparation method has the advantages of simple steps, easily available raw materials, low cost and easily controlled operation parameters, and is convenient for large-scale production.
Owner:GUILIN UNIVERSITY OF TECHNOLOGY

Whey protein active peptide with antioxidant activity and preparation method thereof

The invention discloses a whey protein active peptide with antioxidant activity and a preparation method thereof. The preparation method comprises the following steps: (1) adding protease into whey protein solution for enzymolysis, wherein the enzymolysis temperature is 40-60 DEG C, and the pH value is 6.0-8.0; (2) after enzymolysis, inactivating the protease; (3) precipitating the whey protein not hydrolyzed in enzymolysis solution, and removing the whey protein to take supernatant; (4) carrying out ultrafiltration on the supernatant by an ultrafiltration membrane the cut-off molecular weight of which is less than or equal to 10,000 dalton, collecting filter liquor of peptide the molecular weight of which is less than or equal to 10,000 dalton; (5) concentrating the filter liquor; (6) desalting the concentrated liquor; and (7) concentrating the desalted solution, and then freezing and drying. In the invention, the obtained whey protein active peptide has significant antioxidant property and specific functional characteristics and stable quality, and can be widely applied to the fields of food, cosmetics, medicine and the like. The production technology is simple and is convenient for scale production, the raw material whey protein has high use ratio, and the production cost is low.
Owner:BRIGHT DAIRY & FOOD CO LTD

Carbon dioxide subcritical extraction and recycling method of waste lithium-ion battery electrolyte

The invention provides a carbon dioxide subcritical extraction, recycling and reusing method for the electrolyte of a waste lithium ion battery, belonging to the field of recycling and reusing of solid waste. The method comprises the following steps: after complete discharging of the waste lithium ion battery, dismounting the waste lithium ion battery and removing a shell, positive and negative terminals, sealing rings and cover plates; transferring the electrolyte, current collectors with positive and negative electrode materials and a diaphragm into a supercritical extraction apparatus; adjusting the temperature, pressure, extraction time and flow of a supercritical carbon dioxide fluid and extracting an organic solvent and an additive; and subjecting the obtained solvent to component analysis, supplementing electrolyte salt, the organic solvent and the additive according to analysis results and adjusting a ratio to prepare electrolytes with different functions. The method effectively prevents degradation and dissipation of heat-sensitive substances; operation parameters are easy to control; extraction, separation and recovery are integrated together; later complicated treating procedures are omitted; and the utilization rate of resources is higher.
Owner:HARBIN INST OF TECH

Method for purifying sodium dehydroacetate

The invention discloses a process for purifying sodium dehydroacetate by using supercritical fluid crystallization. The process comprises the following steps: (1) spraying neutralized impurity-containing 90 DEG C sodium dehydroacetate solution from the top of an extraction tower by using a feedstock pump, feeding supercritical fluid to the bottom portion of the extraction tower, and controlling the temperature of the supercritical fluid to be 33 to 36 DEG C, the pressure to be 9 to 11MPa and the flow to be 15 to 30m<3>/min; (2) reducing the pressure of high-pressure supercritical fluid containing dissolved sodium dehydroacetate to be below the critical pressure of the supercritical fluid through a throttling valve, and then enabling the supercritical fluid to enter a separation kettle; (3) after extraction of sodium dehydroacetate, enabling the product to sequentially pass through dehydration and drying processes. The process for purifying sodium dehydroacetate has the advantages that the process is simple and the equipment structure is compact; since the crystal layer is formed on the heat transfer surface but is not suspended in liquid during the process, the blockage of the equipment and pipes is avoided, the production faults are reduced, the purity of the product produced by using the process is high, the bioactivity is good and the grain size is uniform.
Owner:曹海涛
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