Synthesis method for producing potassium titanate series crystal whisker and titanium dioxide crystal whisker products

Abstract

The invention provides a potassium titanate series whisker by slow cooling sintering crystallization method and a synthetic method of titanium dioxide whisker. First, the titanium raw materials, the kalium raw materials and the cosolvent are mixed into the crucible, and the crucible puts into the kiln gradually warming up 600-1300[deg.] C sintering; it which of temperature is slow cooling following the kiln temperature is formed the crystallization spot adjunct; the crystallization spot adjunct is decomposed naturally 2-10 days in the drying room of the humidity 50-100% and the temperature 50-300[deg.] C, to form the complete uniform acicular fibrous; it puts into the 80-102[deg.] C hot-water reactor, by adjusting the pH value of control response solution and the reaction time, then obtains a variable conversion stereotypia of two, four, six or eight potassium titanate whisker or titanium dioxide whisker after washing, dehydration and drying; it is placed into the crucible, then gradually warming up to 600-1300[deg.] C high temperature sintering in the kalium, obtains a finished product of variable conversion stereotypia of two, four, six or eight potassium titanate whisker or titanium dioxide whisker about the length of 50-100 micron and the diameter of 5-10 micron.

Description

technical field [0001] The invention belongs to a synthetic preparation method which is generally applicable to the production of inorganic salt series whiskers. The invention particularly provides a synthesis and preparation method for producing potassium titanate series whiskers and titanium dioxide whiskers. Background technique [0002] With the continuous deepening of research on potassium titanate whiskers, people are more interested in the excellent mechanical, physical and chemical properties of potassium titanate whiskers, as well as their high infrared reflectivity, low thermal conductivity at high temperatures, high temperature resistance, and corrosion resistance. Resistance, wear resistance and other characteristics, with a more in-depth understanding and mastery. At present, Japan has not only produced potassium titanate whisker series products on an industrial scale, but also used potassium titanate whisker as a resin-based and ceramic-based toughening and re...

AI Technical Summary

Problems solved by technology

This method not only reduces the production cost of potassium titanate series whiskers and titanium dioxide whiskers, but also has simple production process and safe operation, and also solves the quality problem of incomplete and uniform whiskers in industrial production