Doped neodymium lithium lanthanum barium tungstate laser crystal and its preparation method and usage
A laser crystal, neodymium lithium tungstate technology, applied in the direction of crystal growth, chemical instruments and methods, single crystal growth, etc., can solve the problems of narrow absorption spectrum line, unsuitable for LD pumping, etc., and achieve moderate crystal hardness and excellent optics Features, Ease of Processing
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[0011] Example: Czochralski method growth doping concentration is 1.22at.% Nd 3+ Nd 3+ :BaLaLiWO 6 Laser crystal.
[0012] BaCO will be accurately weighed according to the proportioning 3 , Li 2 CO 3 , La 2 O 3 , WO 3 And Nd 2 O 3 Mix and grind evenly, after pressing the tablets, put in Ф80×80mm 3 In the corundum crucible, the solid-phase reaction was carried out at 1100°C in a muffle furnace for 24 hours, and then the temperature was raised to 1300°C for 48 hours, repeated twice. Load the synthesized samples above Ф40×35mm 3 In the iridium crucible, put it into the pulling furnace, using the pulling method, in the N 2 In the atmosphere, the growth temperature is 1410°C, the crystal rotation speed is 20 rpm, and the pulling speed is 2 mm / hour, the size of the growth is φ20×19mm 3 Nd 3+ :BaLaLiWO 6 Crystal. The plasma element analysis shows that Nd in the crystal 3+ The ion content is 1.22at.%.
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