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Flavor and fragrance composition

A kind of composition and aroma technology, which is applied in the direction of essential oil/fragrance, food science, perfume formulation, etc. It can solve the problem of no sensory stimulation effect, achieve excellent storage stability, improve the quality of fragrance and fragrance, and increase the diffusivity and long-lasting effects

Inactive Publication Date: 2008-08-06
SHANGHAI TAKASAGO-UNION FRAGRANCES & FLAVORS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Furthermore, there is also no report on any identification of sensory stimulating effects such as cooling effects of 1-(2-hydroxy-4-methylcyclohexyl)ethanone

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0095] Example 1 (sensory stimulation)

[0096] The aqueous solution of (1R, 2R, 4R)-1-(2-hydroxy-4-methylcyclohexyl)ethanone obtained in Synthesis Example 1 was subjected to oral evaluation by a panel of 7 experts. The results of the oral evaluation are as follows.

[0097] Odor quality: sweet acetophenone odor.

[0098] The cooling and refreshing sensation of the aqueous solution: the cooling and refreshing sensation is equivalent to 10 ppm menthol at a concentration of 50 ppm; the refreshing sensation appears relatively quickly, with a clear refreshing sensation without unpleasant taste.

Embodiment 2

[0099] Example 2 (Synergy with menthol)

[0100] Mix 1-menthol and (1R, 2R, 4R)-1-(2-hydroxy-4-methylcyclohexyl)ethanone obtained in Synthesis Example 1 in a ratio of 100:0 to 0:100, The synergy of the cool and refreshing sensation of the mixture was studied.

[0101] As a result, a 70:30 mixture of 1-menthol and (1R, 2R, 4R)-1-(2-hydroxy-4-methylcyclohexyl) ethanone showed about 40% stronger than menthol alone. Cool and refreshing feeling.

[0102] It is obvious from Examples 1 and 2, that the evaluation of (1R, 2R, 4R)-1-(2-hydroxy-4-methylcyclohexyl)ethanone alone and the evaluation of its mixture with menthol are excellent.

Embodiment 3

[0103] Example 3 (body shampoo)

[0104] From 35 parts of (1R, 2R, 4R)-1-(2-hydroxy-4-methylcyclohexyl) ethyl ketone obtained in Synthesis Example 1 and 65 parts of citrus herb fragrance (from TAKASAGO INTERNATION Production) to prepare perfume compositions. By using the above fragrance composition, a body shampoo was prepared according to the following formula. In this formula, the mixing amount is based on "parts by weight".

[0105] Through the bath of ten ordinary group members aged 20-40, each person uses 5g of the body shampoo prepared above to evaluate the cooling sensation effect and the long-lasting performance of the obtained shampoo. As a result, all ten panelists replied that the shampoo has a cooling sensation and the cooling sensation effect is long-lasting.

[0106] Formula of body shampoo

[0107] Component amount

[0108] Triethanolamine 9.00

[0109] Lauric acid 6.00

[0110] Myristic acid 9.00

[0111] Disodium lauryl polyoxyethylene sulfosuccinate (1E.O.) (42%)...

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PUM

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Abstract

A flavor and fragrance composition with a cooling sensation effect comprising 1-(2-hydroxy-4-methylcyclohexyl)ethanone represented by the formula (1). The flavor and fragrance composition is added to a beverage or food product, a fragrance or cosmetic product, a daily utensil product, an oral composition, or a pharmaceutical product in the range of 0.0001 to 20wt% by weight to the total weight of the flavor and fragrance composition added.

Description

Technical field [0001] The present invention relates to a flavor and fragrance composition comprising 1-(2-hydroxy-4-methylcyclohexyl) ethyl ketone, and preferably to a flavor and fragrance composition comprising 1-(2-hydroxy-4-methylcyclohexyl) ethyl A fragrance and aromatic composition that is ketone and has a cooling effect. The present invention also relates to beverages or foods, fragrances or cosmetics, daily necessities, oral compositions, or medicines in which the fragrance and fragrance composition are mixed, and the production method thereof. Background technique [0002] Substances that give the skin, mouth, nose, and throat a cool and refreshing sensation (cooling sensation) or so-called cooling sensation agents have been used in various products such as toothpaste, candy (such as chewing gum and candy), tobacco, paste, bathing Agents and cosmetics. As a typical cooling sensation agent, 1-menthol (L-menthol) is well known, and it is widely used as a fragrance and arom...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A23L1/226A61Q13/00A23L27/00A23L27/20
CPCA23L1/2265A23L2/56A61K8/35A61K2800/244A61Q5/02A61Q11/00A61Q19/00A61Q19/10A23L27/203A61Q13/00A23L27/20C11B9/00
Inventor 相田高石田贤哉
Owner SHANGHAI TAKASAGO-UNION FRAGRANCES & FLAVORS CO LTD
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