Detection method of yupingfeng oral liquid

A technology of Yupingfeng oral liquid and quality control method, which is applied in the directions of measuring devices, instruments, scientific instruments, etc., can solve the problems that the quality of preparations cannot be controlled quickly and easily, the requirements for instruments and equipment are high, and the costs of consumables and reagents are high. The effect of identification time, strong specificity, and easy judgment

Active Publication Date: 2013-09-18
BAODING JIZHONG PHARMA
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Problems solved by technology

Yupingfeng oral liquid is composed of Astragalus, Atractylodes macrocephala (stir-fried) and Fangfeng three herbs. The identification of Astragalus and Fangfeng in the quality standard is completed by thin-layer chromatography and high-performance liquid chromatography, and high-performance liquid chromatography is used for The qualitative identification of traditional Chinese medicine preparations has the problems of high requirements for equipment, long time consumption, high cost of consumables and reagents, and the quality of preparations cannot be controlled quickly and easily.

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  • Detection method of yupingfeng oral liquid

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[0014] Below in conjunction with the examples, the present invention is further described, the following examples are illustrative, not limiting, and the protection scope of the present invention cannot be limited by the following examples.

[0015] A kind of quality control method of Yupingfeng oral liquid, the steps of its method are:

[0016] Identification of Radix Astragali and Fangfeng by Thin Layer Chromatography

[0017] ①Preparation of the test solution: Take 10 ml of Yupingfeng oral liquid sample, extract by shaking with water-saturated n-butanol 3 times, 20 ml each time, combine n-butanol solution, wash 3 times with ammonia test solution, each time 20 ml, evaporate the n-butanol solution to dryness, add 1 ml of methanol to the residue to dissolve, and use it as the test solution;

[0018] ② Preparation of reference substance solution: take astragaloside IV reference substance and 5- 0 - Take an appropriate amount of methyl visamidol glycoside reference substance, ...

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Abstract

The invention relates to a detection method of a yupingfeng oral liquid. A thin layer chromatography is adopted, the same sample pretreatment method and the same chromatographic condition are used, and astragali radix and saposhnidoviae radix in a yupingfeng oral liquid prescription are simultaneously identified on the same thin layer plate. The method of identifying the astragali radix and the saposhnidoviae radix by the thin layer chromatography comprises the steps of (1) test solution preparation, (2) reference solution preparation, and (3) thin layer chromatography conditions and result. According to the detection method, the quality standard of the yupingfeng oral liquid is improved and perfected, and the identification of the saposhnidoviae radix is revised from a high performance liquid chromatography to a thin layer identification method, so that the identification time is greatly shortened, and the detection cost is lowered. Compared with a method in the prior art, the detection method is simpler, more convenient, rapider and more economical; the quality is easier to control; and the detection method is more suitable for industrial production.

Description

technical field [0001] The invention belongs to the technical field of traditional Chinese medicines, and relates to a detection method of traditional Chinese medicines, in particular to a quality control method of Yupingfeng oral liquid. Background technique [0002] Yupingfeng Oral Liquid is a preventive and therapeutic drug widely used in humans and animals. Among them, the quality standard of Yupingfeng Oral Liquid for human use is recorded in the 2010 edition of "Chinese Pharmacopoeia" on page 615; in terms of veterinary drugs, Yupingfeng Oral Liquid is approved by Baoding Jizhong Pharmaceutical Co., Ltd. and Hebei Tianxiang Biological Pharmaceutical Co., Ltd. For new veterinary drugs jointly declared and registered, the new veterinary drug certificate number is: (2010) New Veterinary Drug Zhengzi No. 03, and its quality standards are published in Announcement No. 1322 of the Ministry of Agriculture of the People's Republic of China. Yupingfeng oral liquid is composed ...

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/90
Inventor 许冠英李定刚雷思琦
Owner BAODING JIZHONG PHARMA
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