Positive-working lithographic printing plate precursor and method for preparing same
A technology of lithographic printing plate and original plate, applied in lithographic printing equipment, printing, printing technology, etc., can solve the problems of printing operation obstacles, image density drop, etc., and achieve the effect of good image contrast
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[0151] Hereinafter, the present invention will be described in more detail based on examples. However, the present invention is not limited to these Examples.
[0152] Synthesis of materials for hydrophilization of substrates
[0153] Vinylphosphonic acid / acrylamide copolymer (molar ratio 1:9)
[0154] Add 3500 g of ethanol to a 10-liter flask equipped with a stirrer, a condenser, and a dropping device, and heat to 70° C. 231.1 g (2.14 mol) of vinylphosphonic acid monomers, 1368.9 g (19.26 mol) of acrylamide, and 52 g of AIBN were dissolved in 1000 g of ethanol, and the solution was added dropwise to the reaction device over 4 hours. During the dropwise addition of the monomer solution, a white precipitate was formed. After further heating and stirring at 70° C. for 2 hours, the heating was stopped and cooled to room temperature. The precipitated white powder was isolated by filtration, washed with 1000 g of ethanol and dried.
[0155] Substrate Manufacturing
[0156...
Synthetic example
[0159] Add 2990 g of dimethylacetamide to a 10-liter flask equipped with a stirrer, a condenser, and a dropping device, and heat to 90° C. Make 740.5g phenylmaleimide, 1001g methacrylamide, 368g methacrylic acid, 643g acrylonitrile, 203.6g Phosmer M (United Chemicals), 222.5g styrene, 10.6g AIBN, 16g n-decyl Dialkylmercaptan was dissolved in 2670 g of dimethylacetamide, and this solution was added dropwise to the reaction device over 2 hours. After completion of the dropwise addition, 5.3 g of AIBN was added, the temperature was raised to 100° C., and stirring was continued for 4 hours. During this period, 5.3 g of AIBN was added every 1 hour to make it react.
[0160] After the reaction, stop heating and cool to room temperature. The reaction solution was poured into 50 liters of water, and the generated precipitate was collected by filtration under reduced pressure, washed with water, and vacuum-dried at 50° C. for 24 hours to obtain resin 1 . The yield was 2873g (yield 9...
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