Liposomal formulations
A technology of liposomes and compositions, which is applied in liposome delivery, antibody medical components, viruses/phages, etc., and can solve problems such as reducing liposome efficiency
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[0218] The preparation of liposomes is well known in the art. In general, liposomes have been prepared by a number of different techniques, including ethanol infusion (Batzri et al., Biochem. Biophys. Acta. 298:1015, 1973); ether infusion (Deamer et al., Biochem. Biophys. Acta. 443 Schieren et al., Biochem.Biophys.Acta.542:137,1978); Detergent removal (Razin, Biochem.Biophys.Acta.265:241972); Solvent evaporation (Matsumato et al., J.Colloid Interface Sci .62:149,1977); evaporation of organic solvents (REV) from aqueous emulsions of chloroform (Szoka Jr. et al., Proc.Natl.Acad.Sci.USA,75:4194,1978); Extrusion of MLV or EUV (Olson et al., Biochem. Biophys. Acta. 557:9, 1979); freeze-thawing of phospholipid mixtures (Pick, Arch. Biochem. Biophys., 212:186, 1981) and sonication and homogenization. By convention, liposomes are classified by size and a 3-letter acronym is used to designate the type of liposome in question. Multilamellar vesicles are often designated "MLV". Small ...
Embodiment 1
[0238] Embodiment 1. Influenza A virus materials and methods
[0239] A. IAVM2e1-HDpET28a vector
[0240] The IAVM2e1-HD pET28a plasmid design has been described previously [Ernst et al., 2006].
[0241] B. IAVM2e1-HD pEV vector
[0242] Table 1. Peptide and oligonucleotide sequences of the different IAVM2e1 sequences evaluated
[0243]
[0244] To generate the IAVM2e1-HD protein, a 5' oligonucleotide primer (Integrated DNA Technologies) encoding the IAVM2el gene containing a Bgl II restriction enzyme site and an enterokinase (EK) site was synthesized. To generate the LDR-IAVM2e1-HD protein, a 5' oligonucleotide primer (Integrated DNA Technologies) encoding the IAVM2e1 gene containing the Bgl II restriction enzyme site, the EK site and the LDR sequence of the pET28a vector was synthesized. Similarly, a 3' oligonucleotide primer encoding a hydrophobic domain gene containing an Xho I restriction enzyme site was synthesized. To generate the IAVM2e1-HD gene, primers were us...
Embodiment 2
[0291] Example 2. Results
[0292] In this study, in addition to pET28a-IAVM2e1-HD, we constructed four new IAVM2e1-HD constructs: (i) pEVlIAVM2e1-HD with the above LDR sequence, (ii) pEVl-IAVM2e1(C16S,C18S) -HD, (iii) pEV1-IAVM2e1(C16S)-HD, (iv) pEV1-IAVM2e1(C18S)-HD and (v) pEV1-IAVM2e1(1-15)-HD. All new plasmids were sequenced and confirmed to be in frame and contain the correct sequence. PCR products for each IAVM2e1-HD construct indicated that each PCR product corresponded to the expected size of the corresponding IAVM2e1-HD insert. The plasmid was transformed into E. coli strain C-43 and expressed. Small scale expression studies were performed to confirm that the construct expressed the protein. Unlike the original pET28a-IAVM2e1-HD construct, the pEV-containing IAVM2e-HD construct showed high levels of protein expression compared to the corresponding uninduced controls. To confirm expression of the target M2e protein, Western blot analysis was performed. The IAVM2e...
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