Chuanxiong tea preparation
A Chuanxiong tea preparation, the technology of Chuanxiong, applied in anti-inflammatory agents, non-central analgesics, medical preparations of non-active ingredients, etc.
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preparation example Construction
[0107] Preparation of reference substance solution: Take an appropriate amount of ferulic acid reference substance, weigh it accurately, add 45% ethanol-glacial acetic acid (20:1) mixed solution to make a solution containing 10 μg per 1 ml, and obtain it.
[0108] Preparation of the test solution: Take the product under the difference in loading amount, grind it finely, take about 1.5g, accurately weigh it, add 25ml of 45% ethanol-glacial acetic acid (20:1) mixed solution, weigh it, Heat and reflux for extraction for 30 minutes, let cool, weigh again, make up the lost weight with 45% ethanol-glacial acetic acid (20:1) mixed solution, shake well, centrifuge (4000 rpm) for 10 minutes, and take the supernatant Liquid, that is.
[0109] Determination method: Precisely draw 10 μl each of the reference substance solution and the test solution, inject it into the liquid chromatograph, measure it, and obtain it.
[0110] Generally speaking, each bag of this product is required to con...
preparation example 1
[0120] Composition of raw materials:
[0121]
[0122] Preparation method:
[0123] (a) Add the water extracts of Chuanxiong, Angelica dahurica, Notopterygium, Licorice, Fangfeng, and Asarum to decoct twice, add 8 times the amount of water for the first time, decoct for 1.5 hours, and add 6 times for the second time Measure the water, decoct for 1 hour, filter the decoction, combine the filtrates, and obtain the water extract;
[0124] (b) adding 8 times the amount of water to both Peppermint and Schizonepeta, and extracting the volatile oil by steam distillation for 2.5 hours to obtain two parts of volatile oil and water extract (filtered);
[0125] (c) Combine the water extract obtained in step (a) with the water extract obtained in step (b), add 10 parts by weight of maltodextrin, concentrate to an extract with a relative density of 1.12-1.16 (80°C), and spray dry (air inlet temperature 230 ℃, air outlet temperature 110 ℃), obtain extract powder;
[0126] (d) adding t...
preparation example 2
[0141] Composition of raw materials:
[0142]
[0143]
[0144] Preparation method: basically the same as Preparation Example 1, but 7.5 parts by weight of maltodextrin are used in step (c), and lactose and dextrin are used in a weight ratio of 1:0.5 in step (d) and an appropriate amount is added to make the material The total weight amounts to 375 parts by weight. The obtained sample is designated as Ex2. The glycyrrhizic acid yield of the granule preparation sample obtained in this preparation example was measured with reference to the glycyrrhizic acid yield assay method in Preparation Example 1 to be 98.7%. Referring to the glycyrrhizic acid stability assay method in Preparation Example 1, the glycyrrhizic acid residual rate of the granule preparation sample obtained in this preparation example after high temperature treatment was determined to be 98.1%. The dissolution rate of the granule preparation sample obtained in this preparation example after high temperatu...
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