A method for preparing a series of products from the whole pomelo peel without residue
A series of products, residue-free technology, applied in botany equipment and methods, chemical instruments and methods, compositions for inhibiting chemical changes, etc., can solve the problems of lack of deep processing, etc., achieve strong anti-oxidation performance, simple process, reduce environmental pollution pollution effect
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Embodiment 1
[0024] Step (1) Antibacterial oil extraction: Weigh 200g of untreated pomelo peel, wash it with deionized water, crush it to 10-20 mesh, put it in a large flask of a simultaneous distillable extraction device, add deionized After the water reaches a height of 2 cm above the pulverized powder, heat it to boiling; add pure diethyl ether into the small flask at the other end of the distillable and extraction device, and slowly heat it until the diethyl ether boils, stop heating after 3 hours, and cool it down; dilute the diethyl ether extract at 40 0 C obtained after distillation.
[0025] Step (2) Extract antioxidants with water: filter and separate the residue in the large flask in step (1) from the solution, add the filter residue to the reflux device at a ratio of mass number to water volume of 1g:30mL, 0 Reflux for 2 hours at a temperature of C and then filter, and the filter residue is continuously extracted with the same proportion of water as above, and the parallel opera...
Embodiment 2
[0029] Step (1) Antibacterial oil extraction: Weigh 200g of untreated pomelo peel, wash it with deionized water, crush it to 10-20 mesh, put it in a large flask of a simultaneous distillable extraction device, add deionized After the water reaches a height of 2 cm above the pulverized powder, heat it to boiling; add pure diethyl ether into the small flask at the other end of the simultaneous distillable and extraction device, and slowly heat until the diethyl ether boils, stop heating after 2 hours, and cool it down; dilute the diethyl ether extract at 35 0 C obtained after distillation.
[0030] Step (2) Extract antioxidants with water: filter and separate the residue in the large flask in step (1) from the solution, add the filter residue to the reflux device at a ratio of mass number to water volume of 1g:20mL, 0 Reflux at a temperature of C for 1.5 h and then filter, and the filter residue is continuously extracted with the same proportion of water as above, and the parall...
Embodiment 3
[0034] Step (1) Antibacterial oil extraction: Weigh 200g of untreated pomelo peel, wash it with deionized water, crush it to 10-20 mesh, put it in a large flask of a simultaneous distillable extraction device, add deionized After the water reaches a height of 2 cm above the pulverized powder, heat it to boiling; add pure diethyl ether into the small flask at the other end of the distillable and extraction device, slowly heat until the diethyl ether boils, stop heating after 2.5 hours, and cool down; distill the diethyl ether extract in 40 0 C obtained after distillation.
[0035] Step (2) Extract antioxidants with water: filter and separate the residue in the large flask in step (1) from the solution, add the filter residue to the reflux device at a ratio of mass number to water volume of 1g:50mL, and 0 Reflux for 3 hours at a temperature of C and then filter, and the filter residue is extracted with the same proportion of water as above, and the parallel operation is perform...
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