Blasting bead for herba houttuyniae essential oil cigarette and preparation method thereof

A technology for Houttuynia cordata and oil fume, applied in the directions of essential oils/spice, tobacco, application, etc., can solve the problems of low extraction rate, uncommon application, solvent residue and the like

Inactive Publication Date: 2017-12-15
YUNNAN TOBACCO BIOLOGICAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The cost of solvent extraction is high, it is easy to introduce impurities, the process is complicated and it is easy to cause the loss of volatile oil, and it is easy to have solvent residues, so it is generally not used; steam distillation, the extraction rate is low; CO 2 Supercritical fluid extraction method has simple process, high extraction efficiency, no solvent residue, and low temperature, which is beneficial to protect the biological activity of the target substance. However, this process requires high-pressure equipment, high technical requirements, large investment in equipment costs, and is not widely used.
CO 2 The main disadvantage of supercritical extraction is that the operating pressure is too high

Method used

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  • Blasting bead for herba houttuyniae essential oil cigarette and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0071] Example 1: Preparation of Houttuynia cordata essential oil cigarette popping beads

[0072] The implementation steps of this embodiment are as follows:

[0073] A. Houttuynia cordata pretreatment

[0074] Houttuynia cordata is dried in the shade to a water content of 3.8% by weight, pulverized, sieved, and the collected Houttuynia cordata powder is put into an extraction kettle sold under the trade name Supercritical Extractor by Applied Company of the United States, and then vacuumed to achieve a vacuum The degree is -0.01MPa;

[0075] B. Extraction

[0076] According to the ratio of Houttuynia cordata in grams to extraction solvent in milliliters is 1:38; add 1,1,1,2-tetrafluoroethane extraction solvent and Houttuynia cordata powder to the extraction kettle, under the pressure of 1.4MPa and The extraction was carried out at 40°C for 2.0 hours, and left to stand for separation for 8 minutes to obtain the extract and Houttuynia cordata extract;

[0077] C. Separatio...

Embodiment 2

[0085] Example 2: Preparation of Houttuynia cordata essential oil cigarette popping beads

[0086] The implementation steps of this embodiment are as follows:

[0087] A. Houttuynia cordata pretreatment

[0088] Houttuynia cordata is dried in the shade to a water content of 3.4% by weight, pulverized, sieved, and the collected Houttuynia cordata powder is put into an extraction kettle sold under the trade name Supercritical Extractor by U.S. Applied Company, and then vacuumed to achieve a vacuum The degree is -0.02MPa;

[0089] B. Extraction

[0090] According to the ratio of Houttuynia cordata in grams to extraction solvent in milliliters is 1:20; add 1,1,1,2-tetrafluoroethane extraction solvent and Houttuynia cordata powder to the extraction kettle, under the pressure of 1.2MPa and Extract at 60°C for 0.5h, stand and separate for 5min to obtain the extract and Houttuynia cordata extract;

[0091] C. Separation

[0092] Use a booster pump to introduce the extract obtaine...

Embodiment 3

[0098] Example 3: Preparation of Houttuynia cordata essential oil smoke popping beads

[0099] The implementation steps of this embodiment are as follows:

[0100] A. Houttuynia cordata pretreatment

[0101] Houttuynia cordata is dried in the shade to a water content of 3.1% by weight, pulverized, sieved, and the collected Houttuynia cordata powder is put into an extraction kettle sold under the trade name Supercritical Extractor by U.S. Applied Company, and then vacuumed to achieve a vacuum The degree is -0.05MPa;

[0102] B. Extraction

[0103] According to the ratio of Houttuynia cordata in grams to extraction solvent in milliliters is 1:32; add 1,1,1,2-tetrafluoroethane extraction solvent and Houttuynia cordata powder to the extraction kettle, under the pressure of 1.5MPa and The extraction was performed at a temperature of 46°C for 1.6 hours, and left to separate for 10 minutes to obtain the extract and Houttuynia cordata extract;

[0104] C. Separation

[0105] Use ...

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Abstract

The invention relates to a blasting bead for a herba houttuyniae essential oil cigarette and a preparation method thereof. The preparation method comprises steps of pretreatment of herba houttuyniae, extraction, separation, dropping preparation and the like. According to the preparation method, herba houttuyniae essence is abstracted by using a subcritical fluid abstraction technique; the preparation method has the advantages of high abstraction efficiency, easy separation, non-thermal processing, energy conservation, low cost and the like. The improvement effects, on the smoking quality of the cigarette, of the essence for the blasting bead for the cigarette is more obvious and completer compared with that of a control sample; the blasting bead is abundant in aroma and carries with a spicy aroma and a herbal aroma; the oral irritation is weakened; meanwhile, the laryngeal discomfort feeling is relieved; the saliva secretion feeling is obviously increased, and the overall smoking quality is obviously promoted.

Description

【Technical field】 [0001] The invention belongs to the technical field of tobacco essence extraction. More specifically, the present invention relates to a popping bead for smoking Houttuynia essential oil, and also relates to a preparation method of the popping bead for smoking Houttuynia essential oil. 【Background technique】 [0002] Houttuynia cordata is a wild plant with the same source of medicine and food. It has the functions of clearing heat and detoxifying, reducing swelling and discharging pus, relieving cough and reducing phlegm. Volatile oil is the main functional substance of Houttuynia cordata, which has good curative effect on upper respiratory tract infection, bronchitis, pneumonia, chronic bronchitis, pertussis, etc.; oxalin), 2-undecanone (methyl nonanone), lauric aldehyde, capric aldehyde and other aldehydes and ketones are closely related to terpenoids. Houttuynia cordata can be processed to produce high-quality volatile oils. These volatile oils can be ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/02A24D3/14
CPCA24D3/14C11B9/022C11B9/025C11B9/027
Inventor 杨紫刚周军杨涛洪学晖陈小东
Owner YUNNAN TOBACCO BIOLOGICAL TECH CO LTD
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