Method of synthesizing onium salt type condensation agent on the basis of WK reaction and VHA reaction
A condensing agent and reaction technology, which is applied in the field of synthesizing onium salt condensing agents, achieves the effects of stable and reliable methods, rich functional groups, and good controllability
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[0030] In order to make the purpose, technical solution and advantages of the present invention clearer, the embodiments of the present invention will be further described below in conjunction with the accompanying drawings.
[0031] Please refer to figure 1 , the embodiment of the present invention provides a kind of method based on Willgerodt-Kindler reaction and Vilsmeier-Haack-Arnold reaction synthesis onium salt condensing agent, comprises the following steps:
[0032] S1. Using acyl compounds as raw materials to synthesize carboxylic acid compounds through Willgerodt-Kindler reaction;
[0033] Please refer to figure 2 , the specific method is:
[0034] S1.1. React the acyl compound, sulfur and morpholine under the protection of nitrogen for 24 hours, and the reaction temperature is 140°C;
[0035] S1.2. Cool, add 1.4-dioxane, react at room temperature for 30 minutes, pour the obtained reaction solution into a beaker filled with water, filter and wash;
[0036] S1.3....
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