Electrolyte and preparation method thereof and lithium-sulfur battery
An electrolyte and electrolyte technology, applied in the field of lithium battery electrode material preparation, can solve the problems of low coulombic efficiency of lithium-sulfur batteries, loss of positive active material, low conductivity of organic all-solid-state electrolytes, etc., to improve the Coulombic efficiency and capacity retention rate , the effect of inhibiting solubility
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[0025] 1. Preparation of electrolyte materials
[0026] Lithium reference preparation of perfluoroalkylsulfonylimides. Preparation of ionic liquids containing ether functional groups.
[0027] 2. Preparation of electrolyte
[0028] In an argon atmosphere glove box (H2O<1ppm), dissolve 1M lithium trifluoromethanesulfonyl imide in N,N-diethyl-N,N-di(methoxyethyl)ammonium-tris In the fluoromethylsulfonylimide salt, fully stir evenly to obtain the lithium-sulfur battery electrolyte (free acid<5ppm, moisture<10ppm) of the present invention.
[0029] 3. Preparation of lithium-sulfur battery
[0030] Place the sulfur-based positive pole piece, the separator, and the lithium metal sheet in the battery case, add the electrolyte solution prepared in this example dropwise, and seal it to prepare a CR2025 button battery.
[0031] 4. Test method for flame retardant performance of electrolyte
[0032] Soak an equal weight of glass wool in the electrolyte solution for 10 minutes, then t...
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