A kind of tomato ubiquitin ligase gene and application
A technology of ubiquitin ligase, tomato, applied in the field of plant genetic engineering
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Embodiment 1
[0014] Embodiment 1: SlSINAL gene cloning and Escherichia coli expression vector construction
[0015] Total RNA was extracted from tomato leaves, reverse transcription-PCR (reverse transcription-PCR, RT-PCR), and cloned to obtain the SISINAL gene.
[0016] 1. Reagents
[0017] Plant RNA extraction reagent Trizol was purchased from Invitrogen; DNase I (Dnase I) was purchased from Takara; reverse transcriptase (TransScript Reverse Transcriptase), Pfu high-fidelity DNA polymerase, and T4 DNA ligase were purchased from Beijing Quanshijin Technology Co., Ltd.; restriction endonucleases EcoR I and Sal I were purchased from Fermentas; plasmid extraction kits and gel recovery kits were purchased from Omega; primers were synthesized by Shanghai Yingjun Biotechnology Co., Ltd.; other reagents were imported packaged or domestically produced analytically pure products.
[0018] 2. Escherichia coli strains, vectors and plant material
[0019] Escherichia coli (Escherichia coli) strain ...
Embodiment 2
[0102] Example 2: Expression and purification of SlSINAL tagged protein
[0103] The Escherichia coli with the pMAL-SINAL vector obtained in Example 1 was subjected to induced expression of the SISINAL gene, and then the induced expression of the SISINAL protein was purified to obtain a recombinant SISINAL with the MBP (maltose binding protein, maltose binding protein) tag protein.
[0104] 1. Reagents
[0105]Starch resin was purchased from NEB Company; maltose and IPTG (Isopropylβ-D-Thiogalactoside) were purchased from Sigma Company; other reagents were imported or domestically produced analytically pure products.
[0106] 2. Medium and solution
[0107] The preparation method of LB medium and 1000× ampicillin (Amp) is as described in Example 1.
[0108] Extraction buffer: 1M Tris (pH 7.5) 2mL, 5M NaCl 4mL, 0.5M EDTA 200μL, add sterilized deionized water to 100mL.
[0109] Elution buffer: Add 36 mg maltose to 10 mL extraction buffer.
[0110] 5×SDS-PAGE loading buffer: ...
Embodiment 3
[0130] Example 3: In vitro ubiquitination activity detection of SlSINAL protein
[0131] Add the purified SISINAL protein prepared in Example 2 above to the reagents required for the ubiquitination reaction to detect the ubiquitin ligase activity of the SISINAL protein.
[0132] 1. Reagents
[0133] Creatine phosphocreatine, creatine phosphokinase, ATP (inosine triphosphate), flag-labeled ubiquitin molecule Flag-Ub were purchased from Sigma; ubiquitin activating enzyme (E1), ubiquitin conjugating enzyme (E2 ) was purchased from R&D Systems; PVDF membrane was purchased from Merck Millipore; mouse Flag tag monoclonal antibody anti-Flag and anti-mouse antibody anti-mouse were purchased from Sigma; ECL western blotting substrate was purchased from GE; other reagents All are imported repackaged or domestically produced analytically pure products.
[0134] 2. Solution
[0135] 20×Reaction Buffer: 9.52mg MgCl, 24.2mg ATP, 7.65mg phosphocreatine, 1 mg phosphocreatine kinase, add 1M...
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