Preparation method of flat plate microfiltration membrane for biological detection
A microbial detection and microfiltration membrane technology, applied in chemical instruments and methods, membranes, ultrafiltration, etc., can solve the problems of weak anti-pollution ability, large adsorption capacity, low flux, etc., and achieve strong retention capacity and high separation efficiency , excellent structural properties
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[0023] Example 1
[0024] A method for preparing a flat microfiltration membrane for biological detection, including the following steps:
[0025] 1) Mix the components of the casting solution uniformly, and set aside; the composition and weight percentage of the casting solution are: polyethersulfone 12.5%, sulfonated polyethersulfone 1.5%, polyvinylpyrrolidone-k30 11%, diethylene glycol 30 %, N-methylpyrrolidone 45%;
[0026] 2) Put the film casting liquid in step 1) to degas by standing: put the film casting liquid in a closed container and let it stand for degassing at 30°C;
[0027] 3) Steam induced film formation: Take a clean glass plate and place it on the film scraper horizontally, cast the film casting solution on one end of the glass plate, spread the film casting solution evenly on the glass plate with a 150μm scraper, stay for 90s, in the air The water vapor initially contacts with the casting liquid, exchanges with the solvent, and microphase separation occurs. Then, th...
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[0028] Example 2
[0029] A method for preparing a flat microfiltration membrane for biological detection, including the following steps:
[0030] 1) Mix the components of the casting solution uniformly and prepare for use; the composition and weight percentage of the casting solution are: polyethersulfone 11%, sulfonated polyethersulfone 2%, polyvinylpyrrolidone-k30 12%, diethylene glycol 20 %, N-methylpyrrolidone 55%;
[0031] 2) Put the film casting liquid in step 1) to degas by standing: put the film casting liquid in a closed container and let it stand for degassing at 30°C;
[0032] 3) Steam induced film formation: Take a clean glass plate and place it on the film scraping machine horizontally, cast the film casting solution on one end of the glass plate, spread the film casting solution evenly on the glass plate with a 150μm scraper, stay in the air for 60s Preliminary contact between the water vapor and the casting liquid, exchanges with the solvent, and microphase separation...
Example Embodiment
[0033] Example 3
[0034] A method for preparing a flat microfiltration membrane for biological detection, including the following steps:
[0035] 1) Mix the components of the casting liquid uniformly, and set aside; the composition and weight percentage of the casting liquid are: polyethersulfone 13.5%, sulfonated polyethersulfone 0.5%, polyvinylpyrrolidone-k30 9%, diethylene glycol 30 %, N-methylpyrrolidone 47%;
[0036] 2) Put the film casting liquid in step 1) to degas by standing: put the film casting liquid in a closed container and let it stand for degassing at 30°C;
[0037] 3) Steam induced film formation: Take a clean glass plate and place it horizontally on the film scraper, cast the casting film on one end of the glass plate, spread the casting film evenly on the glass plate with a 150μm scraper, stay for 120s, in the air Preliminary contact between the water vapor and the casting liquid, exchanges with the solvent, and microphase separation occurs, and then the glass pla...
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