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Bis(1,5-nitroaminotetrazole)-potassium ferrous oxide tetrahydrate

A technology of potassium ferrous tetrahydrate and nitroaminotetrazole, which is applied in the fields of nitrated acyclic/alicyclic/heterocyclic amine explosive composition and organic chemistry, and can solve the problems of low detonation velocity and small detonation volume

Active Publication Date: 2019-10-29
XIAN MODERN CHEM RES INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the compound has a smaller detonation volume and a lower detonation velocity

Method used

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  • Bis(1,5-nitroaminotetrazole)-potassium ferrous oxide tetrahydrate
  • Bis(1,5-nitroaminotetrazole)-potassium ferrous oxide tetrahydrate
  • Bis(1,5-nitroaminotetrazole)-potassium ferrous oxide tetrahydrate

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Embodiment 1

[0021] (1) Synthesis of 1,5-Dinitroaminotetrazole Potassium Salt

[0022] At room temperature, sequentially add 0.17g (0.89mmol) 1,5-dinitroaminotetrazole and 3.0mL methanol into the reaction flask, cool in an ice-water bath to 0-5°C, add dropwise 3.0mL containing 0.112g (2mmol) hydrogen The methanol solution of potassium oxide was continued to react at 0-5°C for 0.5 h, filtered, washed with methanol, and dried in vacuum to obtain 0.19 g of white solid with a yield of 79.8%.

[0023] Structure Identification:

[0024] Infrared Spectrum: IR(KBr,cm -1 ), υ: 1510, 1439, 1412, 1367, 1291, 1236, 1228, 1099, 1034, 912, 856

[0025] NMR spectrum: 13 C NMR (DMSO-d 6 ,125MHz), δ: 154.42

[0026] Elemental analysis: Molecular formula CK 2 N 8 o 4

[0027] Theoretical value: C 4.51, N 42.08

[0028] Found: C 4.62, N 42.03.

[0029] The above structural identification data confirmed that the obtained substance was indeed 1,5-dinitroaminotetrazole potassium salt.

[0030] (2) S...

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Abstract

The invention discloses a bis(1,5-nitroaminotetrazole)-potassium ferrite tetrahydrate compound of which the structural formula is as shown in (I) in the description. The compound disclosed by the invention is mainly used for the field of initiating explosives.

Description

technical field [0001] The invention relates to an energetic material, in particular to a bis(1,5-nitroaminotetrazole)-potassium ferrous tetrahydrate compound. Background technique [0002] The primary explosive is the most sensitive chemical energy, with the characteristics of high sensitivity, high promptness, and high power. When excited by external small initial impulse energy such as impact, friction, acupuncture, flame, etc., it will produce detonation and trigger The secondary charge exploded. At present, lead azide and lead styphate are widely used in the military and civilian fields as the primary explosives. Because these two primary explosives contain the toxic heavy metal element-lead, the use of this type of primary explosives will cause serious pollution to personnel and the environment. With the improvement of people's requirements for the safety of weapons and ammunition and the quality of the environment, the performance defects of lead azide and lead styph...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C07D257/06C06B25/34
CPCC06B25/34C07D257/06
Inventor 李亚南陈涛胡建建张红武尉涛熊存良
Owner XIAN MODERN CHEM RES INST
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