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Multifunctional vegetable regenerated cellulose fibers and preparation method thereof

A regenerated cellulose, plant-based technology, applied in the direction of microsphere preparation, microcapsule preparation, etc., can solve the problems of difficult industrial production, complicated preparation process, poor functionality, etc., achieve reduced volatile loss, excellent functionality, The effect of ensuring stability

Inactive Publication Date: 2019-10-18
顾翚
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The present invention provides a multifunctional plant-based regenerated cellulose fiber and its preparation method, which can solve the problems of the existing functional regenerated cellulose when the function is single or multifunctional, its functionality is not good, the preparation process is complicated, and it is not easy for industrial production.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0040] A specific technical plan for the preparation of a multifunctional plant-based regenerated cellulose fiber with a specification of 1.33dtex*38mm:

[0041] Preparation of sweet basil extract solution: Weigh sweet basil extract, dissolve it in deionized water with a bath ratio of 1:4 at a speed of 500r / min, and dissolve it in deionized water at a temperature of 40°C for 40 minutes to obtain sweet basil extract substance solution.

[0042] (Peppermint essential oil + wormwood essential oil and lavender essential oil) preparation of compound plant essential oil microcapsules: add peppermint essential oil, wormwood essential oil, and lavender essential oil into a vacuum mixing kettle according to the mass ratio of 1.0:1.0:0.5 and fully stir. The time is about 20 minutes, the temperature is 15°C, and it is mixed uniformly to form a stable oil phase system.

[0043] The plant essential oil oil phase system prepared above was adjusted to a pH value of 3.0 with acetic acid, and...

Embodiment 2

[0049] A specific technical plan for the preparation of a multifunctional plant-based regenerated cellulose fiber with a specification of 1.56dtex*38mm:

[0050] Preparation of sweet basil extract solution: Weigh sweet basil extract, dissolve it in deionized water with a bath ratio of 1:5 at a speed of 615r / min, and dissolve it in deionized water at a temperature of 48°C for 31 minutes to obtain sweet basil extract substance solution.

[0051] (Peppermint essential oil + wormwood essential oil and lavender essential oil) preparation of compound plant essential oil microcapsules: add peppermint essential oil, wormwood essential oil and lavender essential oil into the vacuum mixing kettle according to the mass ratio of 1.0:1.0:0.5 and fully stir, stirring The time is about 30 minutes, the temperature is 10°C, and it is mixed uniformly to form a stable oil phase system.

[0052] Adjust the pH value of the plant essential oil oil phase system prepared above to 4.0 with acetic aci...

Embodiment 3

[0058] A specific technical plan for the preparation of a multifunctional plant-based regenerated cellulose fiber with a specification of 1.67dtex*38mm:

[0059] Preparation of sweet basil extract solution: Weigh sweet basil extract, dissolve it in deionized water at a temperature of 55°C at a bath ratio of 1:4.5 at a speed of 706r / min, and dissolve it for 26 minutes to obtain sweet basil extract substance solution.

[0060] (Peppermint essential oil + wormwood essential oil and lavender essential oil) preparation of compound plant essential oil microcapsules: add peppermint essential oil, wormwood essential oil and lavender essential oil into the vacuum mixing kettle according to the mass ratio of 1.0:1.0:0.5 and fully stir, stirring The time is about 35 minutes, the temperature is 13°C, and it is mixed uniformly to form a stable oil phase system.

[0061]Adjust the pH value of the plant essential oil oil phase system prepared above to 5.0 with acetic acid, add ethanol and p...

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PUM

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Abstract

The invention provides multifunctional vegetable regenerated cellulose fibers and a preparation method thereof, belongs to the technical field of functional regenerated cellulose fibers, and can solvethe problems that an existing functional regenerated cellulose fiber is single in function or multifunctional, is poor in functionality, complex in preparation process, difficult in industrial production and the like. The multifunctional vegetable regenerated cellulose fibers comprise the following components in percentages by weight: 3.0-8.0wt% of a sweet basil extract and 1.72-5.22wt% of complex plant essential oil, wherein the complex plant essential oil comprises 0.69-2.09wt% of mint oil, 0.69-2.09wt% of folium artemisiae argyi essential oil and 0.34-1.04wt% of lavender essential oil. Thepreparation method disclosed by the invention can be applied to preparation of multifunctional vegetable regenerated cellulose fibers integrating functions of antibiosis, mosquito repelling, skin protection and the like, and is further applied to textiles prepared from the multifunctional vegetable regenerated cellulose fibers.

Description

technical field [0001] The invention belongs to the technical field of functional cellulose fibers, and in particular relates to a multifunctional antibacterial and mosquito repelling fiber prepared from cellulose pulp, sweet basil extract, peppermint essential oil, mugwort essential oil and lavender essential oil as raw materials. Vegetable regenerated cellulose fiber and its preparation method. Background technique [0002] In real life, people will inevitably come into contact with various bacteria, fungi and other microorganisms, and textiles are a good place for these microorganisms to live and a source of disease transmission. Mosquitoes are one of the "four pests" and the main insects that threaten public health. They have many types, reproduce quickly, and are widely distributed, and can transmit various diseases. As people pay more and more attention to health, more and more functional fibers and their textiles are constantly coming out, and functional regenerated ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F1/10D01F2/10B01J13/14
CPCB01J13/14D01F1/103D01F2/10
Inventor 顾翚其他发明人请求不公开姓名
Owner 顾翚
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