Method for recycling waste polyurethane foam and application
A polyurethane foam and calcination technology, applied in the field of polyurethane foam, can solve the problems of complex process and difficult industrialization, and achieve the effects of high specific capacity, good cycle stability and wide source of raw materials
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Embodiment 1
[0058] Using waste polyurethane rigid foam as raw material, it was soaked in ethanol and ultrasonically cleaned to remove mechanical impurities without other pretreatment. It is first cut into a fixed shape suitable for the size of the tube furnace, and its mass is said to be 200 mg. Put the waste polyurethane foam in a porcelain boat, place the porcelain boat in a tube furnace, and heat it at 5°C min under a nitrogen protective atmosphere. -1 The heating rate (i.e. the heating rate of the low-temperature section) was raised to 400°C (i.e. the temperature of the low-temperature section) and calcined for 2 hours (i.e. the constant temperature time of the low-temperature section), and the temperature was naturally cooled to room temperature to obtain a pre-carbonized carbon material;
[0059] Then, under the protection of nitrogen, continue at 6°C·min -1 The heating rate (that is, the heating rate of the high temperature section) is raised to 1000°C (ie, the temperature of the ...
Embodiment 2-4
[0062] The raw material of embodiment 2-4 is consistent with embodiment 1. The difference lies in the heating rate of the low temperature section, the temperature of the low temperature section, the constant temperature time of the low temperature section, the heating rate of the high temperature section, the temperature of the high temperature section and the constant temperature time of the high temperature section, see Table 1 for details.
Embodiment 5-11
[0063] Embodiment 5-11 (comparison)
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