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96results about How to "High in silica" patented technology

Nano-material mixed modified superhigh-temperature high-performance well cementing slurry system and preparation method thereof

The invention relates to a nano-material mixed modified superhigh-temperature high-performance well cementing slurry system and a preparation method thereof. The slurry system comprises the followingingredients in parts by weight: 100 parts of oil well cement, 15-25 parts of coarse silica sand, 15-20 parts of fine silica sand, 1-10 parts of nano-silicon dioxide, 1-10 parts of nano-calcium carbonate, 0.2-1 part of a defoaming agent, 4-10 parts of a fluid loss agent, 0-3 parts of a drag reduction agent, 0.5-4 parts of a retarder and 30-100 parts of water. In the slurry system, set cement has excellent compressive strength and toughness under superhigh temperature, and the compressive strength and the elasticity modulus cannot be obviously changed as the maintenance time is prolonged. The slurry system has good rheological property, lower water loss and proper thickening time, and the comprehensive properties of the slurry system can completely meet the related requirements of site wellcementing construction, so that the technical support is provided for well cementing under high temperature. A nano-material obtained by mixing the nano-silicon dioxide and the nano-calcium carbonateis added, and micropores of the set cement can be effectively filled, so that the system becomes denser. Therefore, the volume shrinkage of the set cement is relieved.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Method for preparing white carbon black and manganese fertilizer from manganese leaching residue

The invention discloses a method for preparing white carbon black and manganese fertilizer from manganese leaching residue. The method comprises the following steps: 1, washing the manganese leaching residue with dilute sulphuric acid solution and running water in turn to obtain the residue; 2, conducting reaction between the residue and 25 to 40% strong base solution by mass at 90 to 120 DEG C for 2 to 5 h, and filtering to obtain filtrate; 3, decoloring the filtrate with active carbon and then carboxyl-terminated hyperbranched polyester at 100 to 120 DEG C to obtain the aqueous solution of silicate; 4, adding water and then inorganic acid and carboxyl-terminated hyperbranched polyester for reaction at 40 to 90 DEG C for 0.5 to 2 h to obtain the white carbon black; and 5, drying and dehydrating the residue obtained in step 2 and adding into a high-speed mixer, adding phosphoric acid, anticaking agent and manganese sulfate into the high-speed mixer, and mixing at room temperature for 10 to 20 min to obtain the manganese fertilizer. The method is simple in process and low in cost and is suitable for industrial production; and the silicon dioxide content of the prepared white carbonblack is more than 95% by mass, the specific area is more than 270 m<2> / g and the particle size is less than 50 nm.
Owner:SOUTH CENTRAL UNIVERSITY FOR NATIONALITIES

Method for low-cost synthesis of ZSM-5 molecular sieve

The invention belongs to the technical fields of molecular sieve and preparation method thereof, and specifically relates to a process for synthesis of a ZSM-5 molecular sieve by using a hydrothermal method and taking natural minerals diatomite and kaolin as raw materials for providing all aluminum sources and silicon sources required for synthesis of the ZSM-5, and particularly, relates to a method for low-cost synthesis of the ZSM-5-5 molecular sieve. The natural minerals diatomite and kaolin as the raw materials provide all the silicon sources and aluminum sources required for synthesis of the ZSM-5 molecular sieve, the use of any chemical silicon or aluminum products are not required, the ways of diatomite low temperature liquid alkali dissolving and kaolin low temperature solid alkali melting are provided for achieving low temperature high-efficiency activation of natural mineral silicon and aluminum 'nutrients', at the same time, inert impurities in the raw materials are removed, and crystallinity and purity of a crystallized product are improved. The method has obvious advantages in aspects of expanding the range of molecular sieve synthetic raw materials, increasing the added value of the natural mineral products, reducing the production cost of molecular sieve, reducing the environmental pollution and the like.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Method for manufacturing high temperature resisting and high pressure resisting oil well cementation briquette through silicon bauxite ceramic microbeads

InactiveCN104478418AChange the dependence of floating beadsLow densityWell cementingPulverized fuel ash
A method for manufacturing a high temperature resisting and high pressure resisting oil well cementation briquette through silicon bauxite ceramic microbeads comprises the steps that the silicon bauxite closed-hole hollow ceramic microbeads are manufactured, burdening, mixing, stirring and size mixing are carried out, 55-65wt percent of G-class oil well cement, 25-35wt percent of the silicon bauxite closed-hole hollow ceramic microbeads with the grain size of five microns to 50 microns, five to seven wt percent of pulverized fuel ash with the loss on ignition of 1.1 percent and the grain size of 20 microns to 50 microns, 1.5 to two wt percent of calcium oxide with the purity of 99.9 percent, 0.5-1.0wt percent of sodium sulfate and one to three wt percent of micro-silicon with the grain size of five microns to 20 microns are mixed, size mixing is carried out according to the water cement ratio of 0.5 to 0.7, the mixtures are poured into a set of two briquette molds with the length of 53 mm, the width of 53 mm and the height of 53 mm, are maintained in a water bath maintenance box for 24 hours and 48 hours respectively at the constant temperature of 52 DEG C, and are soaked in cold water for one hour after demolding, and a performance index test is carried out.
Owner:SHANDONG UNIV OF TECH

Method for preparing ultra-fine active white carbon black by using manganese leached slag and manganese electrolysis waste acid

The invention relates to a method for preparing ultra-fine active white carbon black by using manganese leached slag and manganese electrolysis waste acid. According to the invention, first, manganese leached slag is washed and neutralized by diluted acid and alkaline aqueous solution; the obtained filter residue strong alkaline solution is reacted and filtered, such that a filtrate is obtained; the filtrate is sequentially decolorized by using amino-terminated hyperbranched polyester and polyacrylamide with a number-average molar mass above 1000000 g/mol, such that a decolorized silicate aqueous solution is obtained; a particle activator is added to the solution, then decolorized manganese electrolysis waste acid is dropped to the solution; the obtained solution is reheated, reacted, filtered, washed, and dried, such that white carbon black is obtained. According to the present invention, white carbon black with a high added value can be produced by using waste slag and waste liquid discharged from a manganese mine enterprise, such that environment protection and comprehensive utilization of resources can be realized. The method also has advantages of simple technology, low cost,high added value, and is suitability for industrialized productions.
Owner:DAXIN MANGANESE MINE BRANCH OF CITIC DAMENG MINING IND +1

Method for preparing oil well cementing test block resistant to high temperatures and high pressures from aluminum diatomite ceramic microspheres

InactiveCN104592963AChange the dependence of floating beadsLow densityDrilling compositionCeramicwareMicrosphereSlurry
The invention provides a method for preparing an oil well cementing test block resistant to high temperatures and high pressures from aluminum diatomite ceramic microspheres. The method comprises the preparation of aluminum diatomite closed-pore hollow ceramic microspheres, burdening, blending and stirring for slurry mixing. Specifically, the method comprises the steps that 55-65wt% of G-grade oil-well cement, 25-35wt% of aluminum diatomite closed-pore hollow ceramic microspheres having the particle size of 10-50 microns, 5-7wt% of coal ash having the ignition loss of 1.1% and the particle size of 20-50 microns, 1.5-2wt% of calcium oxide having the purity of 99.9%, 0.5-1.0wt% of sodium sulfate, and 1-3wt% of micro-silicon having the particle size of 5-20 microns are mixed to obtain a mixture; the mixture is mixed with water in the water cement ratio of 0.5-0.7 to obtain the slurry; one part of the slurry is poured into a group of two test molds which are 53mm long, 53mm wide and 53mm high, and maintained in a constant-temperature water bath curing box at 52 DEG C for 24 hours and 48 hours, respectively; next, the stripped product is soaked in cold water for 1 hour, and then a performance index test is performed.
Owner:SHANDONG UNIV OF TECH

Equipment for continuous acid leaching treatment of high silica glass fiber cloth

The invention discloses equipment for continuous acid leaching treatment of high silica glass fiber cloth. The equipment comprises an acid leaching slot; the acid leaching slot comprises a presoaking acid slot, a thermal acid slot I, a thermal acid slot II and a thermal acid slot III; the glass fiber cloth arranged on an unwinding machine enters the presoaking acid slot, the thermal acid slot I, the thermal acid slot II, the thermal acid slot III, a water washing slot I, a water washing slot II and a water washing slot III in sequence by a cloth feeding machine, pickling and washing are finished, the glass fiber cloth is dried and flattened by drying and flattening equipment, and is wound by a winding machine beside the drying and flattening equipment, and the production line operation is finished. The equipment is a piece of production line equipment, the content of SiO2 in the glass fiber cloth can be improved from 70% to be over 96% by controlling the process parameters through the process steps, the temperature resistance performance of grey cloth is improved to 100 DEG C, the continuous production line acid leaching production efficiency is high, the SiO2 content of obtained grey cloth is stable, the comprehensive performance of the product is greatly improved, and benefits are increased for an enterprise.
Owner:JIANGSU HENGZHOU SPECIAL GLASS FIBER MATERIAL

Granite waste rock powder ceramsite pervious concrete and preparation method thereof

The invention provides granite waste rock powder ceramsite pervious concrete and a preparation method thereof. The granite waste rock powder ceramsite pervious concrete is prepared from the following ingredients in percentage by weight: 60 to 75 percent of granite waste rock powder ceramsite, 10 to 25 percent of cement, 6 to 20 percent of pulverized fuel ash, 0.1 to 0.5 percent of water reducing agents and 7 to 8 percent of water, wherein the granite waste rock powder ceramsite has the grain diameter being 10 to 20mm, and is prepared from the following ingredients in percentage by weight: 50 to 80 percent of granite waste rock powder, 4 to 15 percent of clay tailings, 10 to 20 percent of waste porcelain powder, 5 to 10 percent of clay and 1 to 5 percent of coal dust. A large amount of granite waste rock powder ceramsite is used for replacing natural aggregate; the surface of the granite waste rock powder ceramsite is hard; fine and fine honeycomb micropores are formed at the inside; the characteristics of small density, low heat conductivity, high strength and good water permeability are realized. Meanwhile, the fireproof performance of the ceramsite sintered through high temperature is excellent; the consistency with the concrete is good; the performance of the pervious concrete can be obviously improved.
Owner:UNIV OF JINAN

Method for manufacturing high temperature and high pressure resisting oil well cementing test block through silicon kaolin ceramic microbeads

InactiveCN104531111AChange the dependence of floating beadsLow densityDrilling compositionCeramicwareKaolin clayMixed materials
Disclosed is a method for manufacturing a high temperature and high pressure resisting oil well cementing test block through silicon kaolin ceramic microbeads. The method comprises the steps of the silicon kaolin blind hole hollow ceramic microbeads are prepared, batched, mixed and stirred for size mixing, 55 wt% to 65 wt% of G-level oil well cement, 25 wt% to 35 wt% of the silicon kaolin ceramic microbeads with the particle size of five microns to 50 microns, 5 wt% to 7 wt% of coal ash with the ignition loss of 1.1 percent and the particle size of 20 microns to 50 microns, 1.5 wt% to 2 wt% of calcium oxide with the purity of 99.9 percent, 0.5 wt% to 1.0 wt% of sodium sulfate and 1 wt% to 3 wt% of micro-silicon with the particle size of five microns to 20 microns are mixed, size mixing is carried out on the mixed materials according to the water cement ratio of 0.5-0.7, the mixed materials are poured into a set of two test molds with the length of 53 mm, the width of 53 mm and the height of 53 mm, the test molds are maintained in water bath maintenance boxes at the constant temperature of 52 DEG C for 24 hours and 48 hours respectively, the mixed materials are soaked in cold water for one hour after demolding, and a performance index test is carried out.
Owner:SHANDONG UNIV OF TECH

Nickel oxide high-temperature purple silk-gloss ceramic glaze and preparation method thereof

The invention provides nickel oxide high-temperature purple silk-gloss ceramic glaze and a preparation method thereof, and belongs to the field of ceramic. The nickel oxide high-temperature purple silk-gloss ceramic glaze is obtained by firstly preparing a nickel oxide high-temperature purple silk-gloss ceramic glaze material, and then glazing and sintering at high temperature, wherein the nickeloxide high-temperature purple silk-gloss ceramic glaze material is prepared from the following raw materials according to the mass percent of each raw material: 45 percent to 35 percent of potassium feldspar powder, 4.5 percent to 6 percent of silicon dioxide, 4.5 percent to 10 percent of kaolin, 10 percent to 20 percent of zinc oxide, 30 percent to 40 percent of a frit and 1 percent to 2 percentof nickel oxide. The frit is prepared from the following raw materials according to the mass percent of each raw material: 1 percent to 3 percent of potassium oxide, 12 percent to 20 percent of sodiumoxide, 2 percent to 8 percent of calcium oxide, 10 percent to 35 percent of barium carbonate and 40 percent to 60 percent of silicon dioxide. By adopting the method provided by the invention, a phenomenon in a firing process of a traditional glaze material that a lot of poisonous heavy metal is volatilized is overcome; meanwhile, phenomena that needle holes and cracks are formed in the surface ofa fired product are effectively prevented.
Owner:SHENYANG JIANZHU UNIVERSITY

Preparation method of macrocrystalline magnesia with low silicon dioxide content

The invention discloses a preparation method of macrocrystalline magnesia with low silicon dioxide content, and belongs to the technical field of mineral resource processing. The method comprises thefollowing steps: (1) fine selection: taking low-grade magnesite as a raw material, and finely selecting magnesite with the magnesium oxide content of 40%-45%; (2) cleaning: cleaning magnesite; (3) refining: refining the magnesite; (4) roasting: feeding the concentrate powder into a rotary kiln or a fluidized bed furnace for roasting, and cooling to room temperature to obtain light calcined magnesia; (5) dry pressing: feeding the light calcined magnesia into a ball press machine for dry pressing to obtain balls; and (6) electric melting: feeding the spheres prepared in the step (5) into an electric arc furnace for electric melting, and carrying out heat preservation, cooling and crystallization. The prepared macrocrystalline magnesia has good performance advantages, the test parameters suchas the particle volume density, the magnesium oxide content, the silicon dioxide content, the calcium oxide content, the iron oxide content, the aluminum oxide content and the yield show significantdifferences, and the macrocrystalline magnesia is high-quality macrocrystalline magnesia.
Owner:LIAONING DONGHE NEW MATERIAL CO LTD
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