The invention discloses antique
ceramic mulberry purple black
glaze and a preparation method thereof, and belongs to the technical field of
ceramic glaze. The
glaze comprises the following components in percentage by
mass: basic glaze (40-50% of
potassium feldspar, 20-30% of
quartz, 10-15% of kaolin and 5-10% of
calcite), a composite color former (3-6% of
ferric oxide, 2-4% of
manganese oxide and 0.1-0.5% of
cobalt oxide) and an antique additive (2-5% of
bone ash and 1-3% of
plant ash). The preparation method comprises the steps of
raw material crushing, wet ball milling,
glazing, segmented firing and the like. The antique glaze with mulberry fruit characteristic purple black gradient tone and natural silver
crystal spots is successfully prepared through the synergistic effect of an iron-
manganese-
cobalt composite color development
system, in combination with regulation and control of natural additives on the
microstructure of the glaze, and by adopting a segmented firing process of firstly oxidizing, then reducing and controlling
slow cooling. The glaze surface is simple and natural in texture, unique in color development, rich in layer, good in
sintering stability and high in yield, and can meet the requirements of art ceramics and archaized artware on high-quality characteristic black glaze.