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32results about How to "Pure hair color" patented technology

Process for preparing spherical nanometer spinel zaffre by hydrothermal method

The invention discloses a process for preparing spherical nanometer spinel zaffre by the hydrothermal method. The process comprises the following steps: weighing and putting cobalt chloride and aluminum chloride according to a mol ratio of Co<2+> : Al <3+> = 1:2, putting the materials into a beaker, adding a proper amount of deionized water and carrying out uniform stirring on a magnetic stirrer;adding a sodium hydroxide solution drop by drop until the pH value of the mixture in the beaker is 13 and continuing stirring; adding mixed liquor of triethanolamine and glycerol with a volume fraction of 6 to 18% and resuming stirring; carrying out hydrothermal cultivation on the mixed solution at a temperature of 245 DEG C for 20 to 40 hours and taking the mixed solution out for natural coolingat room temperature; repeatedly rinsing the hydrothermal cultivation resultant material in liquid phase until the pH value equals 7 and putting the resultant material into a baking oven for drying attemperature of 60 DEG C so as to obtain spherical products with particle size less than 100 nm. The advantages of the invention are as follows: liquid phase hydrothermal cultivation is employed and composite organic matters are added; therefore, nanometer spherical powder is formed directly without calcining, energy consumption is relatively low, and no environmental pollution is generated.
Owner:JINGDEZHEN CERAMIC INSTITUTE

Method for preparing zirconium silicate coated carbon nanosphere ceramic black pigment

ActiveCN107189494AGood dispersionHigh negative potentialPigmenting treatmentDispersityOxygen
The invention discloses a method for preparing a zirconium silicate coated carbon nanosphere ceramic black pigment. The method is characterized in that carbon nanospheres prepared from a biomass raw material by a hydrothermal method replace a traditional carbon source, the hydrophilicity is improved by use of rich oxygen-containing functional groups on the surfaces of the carbon nanospheres and the negative potential state, and the dispersity of the carbon source is enhanced; the thickness of wrappers of the carbon nanospheres and the electrostatic adsorption capability are adjusted and controlled to enable a zirconium silicate precursor to tightly wrap the carbon nanospheres; and under the action of a mineralizer, the ceramic black pigment in which zirconium silicate wraps the carbon nanospheres is prepared after high-temperature calcination. In the experiment process, through optimization and control of such conditions as the addition of glucose, the hydrothermal temperature, the hydrothermal time, the silicon-zirconium ratio, the stirring time of the precursor, type and consumption selection of the mineralizer and a firing system, the synthesized black pigment is pure in color, uniform in particle size and stable in performance, can be used in various high-temperature ceramic glazes, and has a high economical value.
Owner:JINGDEZHEN CERAMIC INSTITUTE

A kind of preparation method of zirconium silicate wrapped nano-carbon sphere ceramic black material

ActiveCN107189494BGood dispersionHigh negative potentialPigmenting treatmentDispersityOxygen
The invention discloses a method for preparing a zirconium silicate coated carbon nanosphere ceramic black pigment. The method is characterized in that carbon nanospheres prepared from a biomass raw material by a hydrothermal method replace a traditional carbon source, the hydrophilicity is improved by use of rich oxygen-containing functional groups on the surfaces of the carbon nanospheres and the negative potential state, and the dispersity of the carbon source is enhanced; the thickness of wrappers of the carbon nanospheres and the electrostatic adsorption capability are adjusted and controlled to enable a zirconium silicate precursor to tightly wrap the carbon nanospheres; and under the action of a mineralizer, the ceramic black pigment in which zirconium silicate wraps the carbon nanospheres is prepared after high-temperature calcination. In the experiment process, through optimization and control of such conditions as the addition of glucose, the hydrothermal temperature, the hydrothermal time, the silicon-zirconium ratio, the stirring time of the precursor, type and consumption selection of the mineralizer and a firing system, the synthesized black pigment is pure in color, uniform in particle size and stable in performance, can be used in various high-temperature ceramic glazes, and has a high economical value.
Owner:JINGDEZHEN CERAMIC UNIV

Process for preparing spherical nanometer spinel zaffre by hydrothermal method

The invention discloses a process for preparing spherical nanometer spinel zaffre by the hydrothermal method. The process comprises the following steps: weighing and putting cobalt chloride and aluminum chloride according to a mol ratio of Co<2+> : Al <3+> = 1:2, putting the materials into a beaker, adding a proper amount of deionized water and carrying out uniform stirring on a magnetic stirrer;adding a sodium hydroxide solution drop by drop until the pH value of the mixture in the beaker is 13 and continuing stirring; adding mixed liquor of triethanolamine and glycerol with a volume fraction of 6 to 18% and resuming stirring; carrying out hydrothermal cultivation on the mixed solution at a temperature of 245 DEG C for 20 to 40 hours and taking the mixed solution out for natural coolingat room temperature; repeatedly rinsing the hydrothermal cultivation resultant material in liquid phase until the pH value equals 7 and putting the resultant material into a baking oven for drying attemperature of 60 DEG C so as to obtain spherical products with particle size less than 100 nm. The advantages of the invention are as follows: liquid phase hydrothermal cultivation is employed and composite organic matters are added; therefore, nanometer spherical powder is formed directly without calcining, energy consumption is relatively low, and no environmental pollution is generated.
Owner:JINGDEZHEN CERAMIC UNIV
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