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53results about How to "Product Quality Impact" patented technology

Energy-saving and yield-improving production method of ethyl acetate

The invention discloses an energy-saving and yield-improving production method of ethyl acetate. The production method comprises the following steps of: heating and gasifying raw material acetic acid and ethanol and then feeding into a reaction kettle to react; recovering a bottom material in the reaction kettle according to a certain proportion with the total amount of fed materials to an evaporator to perform flash evaporation, wherein most of ester and alcohol in the bottom material which is subjected to flash evaporation are returned to the bottom of an esterification tower, and the ester phase of the rest bottom material is a large amount of acid and a part of water and is discharged through a pump from the bottom of the evaporator; conveying the treated bottom material to a heat exchanger through the pump for heating and then directly feeding into a dehydration tower to perform dehydration treatment; performing azeotropic distillation and recovering azeotrope formed by water and a dehydrant from the top of the esterification tower; condensing to split phase; discharging the water phase to a recovery tower for treatment; reflowing the oil phase to a dehydration tower; and newly returning acid which is discharged from the bottom of the dehydration tower to the reaction kettle to participate in esterification reaction. After the process is implemented, the water in the kettle is effectively reduced to further reduce the corrosion condition of the equipment, the energy of an esterification section is saved by 5-10 percent, the capacity can be increased by 10-20 percent, and the economic benefit is obvious.
Owner:JINJIANG TAIXING CHEM IND CO LTD

Method for extracting and separating tungsten and molybdenum from molybdenum-contained ammonium tungstate solution

The invention discloses a method for extracting and separating tungsten and molybdenum from a molybdenum-contained ammonium tungstate solution. The method comprises the steps that bicarbonate containing trialkyl methyl ammonium and an organic phase of a carbonate composite extractant of the bicarbonate are used for making contact with molybdenum-contained ammonium tungstate feed liquid subjected to vulcanization and an ammonium bicarbonate-ammonium carbonate mixed detergent correspondingly for performing fractional extraction, the molybdenum is made to enter the organic phase, the tungsten remains in a water phase, and a high-purity ammonium tungstate aqueous solution and an organic phase loaded with pure molybdenum are obtained; and then, the organic phase loaded with the pure molybdenumis oxidized through a hydrogen peroxide solution, reextraction is performed by adopting an ammonium bicarbonate-ammonium carbonate mixed solution, a high-purity ammonium molybdate solution is obtained, and an organic phase after reextraction can directly return back to extraction for repeated use without needing treatment. The method has the characteristics that the tungsten and molybdenum mutualseparation depth is high, no detrimental impurity is introduced, and high-purity tungsten and molybdenum product liquid can be obtained simultaneously.
Owner:CENT SOUTH UNIV

Dry recovery system and method of reduction tail gas produced in polysilicon production process

The invention discloses a dry recovery system and a dry recovery method of reduction tail gas produced in a polysilicon production process. The system comprises a leaching tower, an absorption system, an absorption device, and a first filtering device. The absorption system is used for carrying out an absorption treatment upon leached reduction tail gas, such that chlorosilane and hydrogen chloride in the leached reduction tail gas can be removed, and hydrogen can be obtained. An adsorbentused for carrying out an absorption treatment upon the hydrogen is arranged in the absorption device, such that residual chlorosilane and hydrogen chloride in hydrogen can be further removed by adsorption. The first filtering device is used for filtering the hydrogen processed through the absorption treatment, such that high-purity hydrogen is obtained. A ceramic filter core is arranged in the first filtering device. According to the dry recovery system provided by the invention, a gas filtering device provided with the ceramic filter core is adopted. The filtering device has excellent properties of high-temperature resistance and corrosion resistance. Therefore, no influence is caused upon polysilicon product quality.
Owner:CHINA ENFI ENGINEERING CORPORATION

Method for preparing cobalt oxalate by pulse electromagnetic field

The invention relates to a method for preparing cobalt oxalate by a pulse electromagnetic field, which solves the problems in the prior cobalt powder manufacture of complex process, high cost and large particle size and irregular shape of cobalt powder. The method comprises the following steps: acidulating (NH4)2C2O4 solution and controlling the pH value of the (NH4)2C2O4 solution at 4-6; dripping the acidulated (NH4)2C2O4 solution into CoCl2 solution, wherein the mol ration of (NH4)2C2O4 solution to CoCl2 solution is 1:1-2:1, and the dripping speed is controlled to be 100-200 ml / min; reacting in thermostatic water-circulator bath at 20-45 DEG C; mechanically stirring during reaction; processing the reaction system by a pulse electromagnetic field, wherein the pulse voltage is 1-1000V, and the pulse frequency is 1-100Hz; carrying out filtration, washing, vacuum drying at normal temperature after the reaction is completed to obtain a cobalt oxalate sample; and putting the cobalt oxalate sample into a tube-type resistance furnace to perform thermolysis reaction, cooling to room temperature in the furnace to obtain cobalt powder as a thermolysis product of cobalt oxalate. The invention has the advantages of simple process, low production cost, good quality, no pollution to treated objects or surrounding environment and wide application range, and can obtain products with different shapes and particle sizes.
Owner:LIAONING UNIVERSITY OF TECHNOLOGY

Method of measuring and monitoring weight of UO2 pellets in single fuel rod in real time

ActiveCN106782706AImprove the degree of weighing informationRealize data traceabilityNuclear energy generationNuclear monitoringMonitor weightBarcode
The invention provides a method of measuring and monitoring weight of UO2 pellets in a single fuel rod in real time. The method comprises the following steps: (1) automatically reading, by a barcode reading device, a barcode on a cladding tube, and then comparing the barcode with welding information in a database to determine whether the cladding tube is already welded; (2) automatically weighing the determined welded cladding tube by means of a weighing system; (3) conveying the cladding tube already loaded with pellets to a weighing position again, automatically reading, by the barcode reading device, the barcode on the cladding tube, and then comparing the barcode with weighing information in the database; (4) automatically weighing the cladding tube determined as being filled with pellets by means of the weighing system; and (5) assembling a fuel assembly, inquiring about the barcodes on the cladding tubes, and automatically reading and counting up the weight of the loaded UO2 pellets. The method in the invention increases the level of informationization of fuel rod weighing, achieves data tracing in weight data storage, and can achieve immediate obtaining of the weight of UO2 pellets in a single fuel rod and real-time monitoring on consumption fluctuation of UO2 pellets during the production of the fuel rods.
Owner:CHINA NORTH NUCLEAR FUEL

Light environmental-friendly brick based on building waste and production process of light environmental-friendly brick

ActiveCN109516735AImprove structural strengthAffect the normal service lifeCement mixing apparatusCeramicwareBrickSlag
The invention discloses a light environmental-friendly brick based on building wastes and a production process of the light environmental-friendly brick. The light environmental-friendly brick comprises the following raw materials in percentage by weight: 30-50% of water, 15-25% of Portland cement, 5-15% of a ceramic waste, 5-15% of a brick waste, 6-8% of river sand, 3-7% of bits of wood, 3-7% offurnace cinder and 2-4% of modified foaming aids. Due to adoption of the ceramic waste, the brick waste, the bits of wood and the furnace cinder in the raw materials, building wastes and slag materials can be reasonably recycled, environment influence caused by casual treatment can be avoided, the production cost can be reduced, and meanwhile the environment protection is greatly improved; and dueto adoption of the modified foaming aids, under coactions of final products, namely calcium dodecyl benzene sulfonate and sodium dodecyl benzene sulfonate generated in mutual reactions of raw materials in the modified foaming aids, and under the synergetic effect of a silicon resin polyether emulsion, a foaming effect is improved, and the consequence that bricks have unequal and too large self weights since air pores are unequal in size and non-uniform in distribution can be avoided.
Owner:湖南钰龙建材有限公司

Reactor cap for manufacturing titanium sponge

The invention provides a cover of a reactor used for producing sponge titanium. The cover comprises a barrel, a panel arranged on the upper part of the barrel, a bottom plate arranged on the lower part of the barrel; and a channel sleeve, a feeder sleeve and a vacuum piping sleeve are arranged on the cover of the reactor. The cover is characterized in that a cavity enclosed by the panel, the bottom plate and the barrel is filled with a heat insulating material-serra cotton containing zirconium, the bottom plate of the cover of the reactor is arched spherical, a sleeve barrel is arranged below the bottom plate of the reactor cover, the channel sleeve and the feeder sleeve are arranged inside the sleeve barrel, the vacuum piping sleeve is arranged outside the sleeve barrel. The reactor cover has the advantages of simple structure, easy manufacturing, light weight, safety and reliability and hard deformation, and can effectively avoid distilled materials from being directly pumped out by a vacuumizer and simultaneously does not affect the completion of the reduction reaction. The reactor cover has the functions of universal interchangeability, and can ensure the normal operation of production, and the product quality is not threatened, so that the main equipment problem of producing the sponge titanium by the combined method is radically solved.
Owner:CITIC JINZHOU METAL

Production device and production method of caprolactam

PendingCN112079759AEfficient evaporationHigh Efficiency in Evaporation and GasificationLactams preparationLactams separation/purificationPtru catalystFluidized bed
The invention relates to the field of caprolactam production, in particular to a caprolactam production device and method, and the device comprises a cyclohexanone-oxime evaporation and gasification system, a mist separation system, a fluidized bed reaction system and a moving bed reaction system which are connected in series; the device further comprises a reaction solvent recycling system and acarrier gas recycling system. The method comprises the following steps: (1) evaporating and gasifying carrier gas, ethanol and cyclohexanone-oxime in a cyclohexanone-oxime evaporation and gasificationsystem; (2) feeding a gas-phase material flow obtained in the step (1) into a mist separation device to gasify cyclohexanone-oxime which is not completely gasified in a cyclohexanone-oxime evaporation and gasification system; (3) feeding the material flow obtained in the step (2) into a fluidized bed reaction system and a moving bed reaction system in sequence for gas-phase Beckmann rearrangementreaction; and (4) recovering ethanol and carrier gas in the material flow obtained in the step (3). By adopting the device and the method, the high conversion rate of cyclohexanone-oxime can be obtained, the problem of catalyst discharge is avoided, and the production is not interrupted.
Owner:ZHEJIANG HENGYI PETROCHEMICAL RES INST CO LTD

Anti-blocking powder discharging device and method for low-loose-density metal powder products

The invention discloses an anti-blocking powder discharging device and method for low-loose-density metal powder products. The device comprises a decomposer, a middle bin and a produced powder material bin, and the decomposer, the middle bin and the produced powder material bin are sequentially connected from top to bottom; the tops of the middle bin and the produced powder material bin are each provided with an exhausting port; the bottom of the middle bin is provided with a discharging valve; the device further comprises a decomposed gas dust remover, a disinfecting replacement gas dust remover and a dust collecting powder material bin; an inlet of the decomposed gas dust remover is connected with the exhausting port of the middle bin and the exhausting port of the produced powder material bin through pipelines; the top of the dust collecting powder material bin is provided with a dust collecting port and a disinfecting port; an inlet of the disinfecting replacement gas dust remover is connected with the exhausting port of the produced powder material bin and the disinfecting port through pipelines; and the dust collecting port is connected with an outlet of the decomposed gas dust remover and an outlet of the disinfecting replacement gas dust remover through pipelines. The device and method are good in powder discharging smoothness and high in powder product quality.
Owner:JINCHUAN GROUP LIMITED

A method for preparing needle coke

The invention discloses a method and a device of preparing a needle coke, and belongs to the technical field of needle coke preparation. The method disclosed by the invention is characterized by comprising the following steps: separating an asphalt raw material by virtue of a degasification column and a molecular distillation column, preheating the asphalt raw material, pumping the asphalt raw material in the degasification column and carrying out degasification treatment at a degasification temperature of 250-330 DEG C under an in-column pressure of 100-1000Pa, then pumping the degasified materials to the molecular distillation column, controlling a distillation temperature in the molecular distillation column to 300-400 DEG C and controlling a pressure to 0.01-100Pa, separating the materials into a light-phase component and a heavy-phase component in the molecular distillation column through a short-path distillation action, carrying out delayed coking on the light-phase component to obtain green coke, and calcining the green coke to obtain the needle coke. The method disclosed by the invention is capable of stably and accurately controlling the cutting amounts of the raw material components, thus flexibly adjusting the product quality, and furthest reserving ideal components. Moreover, the method is low in treatment temperature, rapid in material separation, and free from forming secondary quinoline undissolved substances.
Owner:乔光明

Thin-wall veneer reeling machine with adjustable roll shaft diameter

The invention belongs to the technical field of veneer reeling machines, and particularly relates to a thin-wall veneer reeling machine with an adjustable roll shaft diameter. The machine comprises aveneer reeling machine body, the veneer reeling machine body comprises an end shaft, a diameter-adjustable mechanism is arranged on the inner wall of the end shaft, the diameter-adjustable mechanism comprises a disc, and the inner wall of the end shaft is fixedly sleeved with the outer surface of the disc. According to the thin-wall veneer reeling machine with the adjustable roll shaft diameter, when two specifications of veneer reeling plates with the same veneer reeling diameter but different wall thicknesses are required, the distance between an upper roll shaft and two lower roll shafts onthe veneer reeling machine body is automatically adjusted, the action of adjusting while veneer reeling during veneer reeling is achieved, meanwhile, The differential connection mode that an oil inlet pipe and an oil outlet pipe of a hydraulic cylinder are communicated is adopted, the outward extending movement speed of a piston rod of the hydraulic cylinder can be conveniently achieved on the premise that the flow of a hydraulic pump is not increased, and the effect that the quality of plate products after veneer reeling is affected is avoided.
Owner:NANTONG CHAOLI ROLLING MACHINE PRODUCING

Method for harvesting dunaliella salina by using waste spirulina culture liquid

The invention discloses a method for harvesting dunaliella salina by using a waste spirulina culture liquid, and relates to a dunaliella salina harvesting method. The method comprises the following steps: 1) collecting supernate after spirulina is harvested, and testing the pH value; 2) adding the supernate collected in the step 1) into dunaliella salina, leaving to stand, and testing the harvesting rate; and 3) mixing the supernate obtained in the step 2) with a dunaliella salina culture medium, inoculating dunaliella salina cells, performing circulation culture, and testing the growth curve of dunaliella salina. By making full use of characteristics that the pH of the culture liquid used in the growth process of spirulina is alkali and dunaliella salina can be automatically flocculated under a high pH value, the supernate of spirulina can be sufficiently utilized, the supernate obtained after dunaliella salina is harvested can be continuously adopted for dunaliella salina culture, and the production cost is low. The harvested dunaliella salina is free of organic test agent or toxic or harmful substance, influence to the quality of an algae paste product in the harvesting process can be avoided, the waste supernate can be sufficiently utilized, and secondary pollution can be prevented.
Owner:XIAMEN UNIV

Automatic film tearing machine

The invention relates to the technical field of film tearing machines, in particular to an automatic film tearing machine. The automatic film tearing machine comprises an air blowing mechanism, a waste suction pipe, a hot pressing mechanism, an automatic feeding mechanism, an automatic discharging mechanism, a fixing mechanism and a machine frame, the air blowing mechanism, the hot pressing mechanism and the waste suction pipe are arranged on the fixing mechanism in a sleeving mode through fixing plates, the air blowing mechanism is located on one side of the hot pressing mechanism, the waste suction pipe is located on one side of the air blowing mechanism, the automatic feeding mechanism is arranged on one side of the machine frame, and the automatic discharging mechanism is arranged on the other side of the machine frame. According to the film tearing machine, the air blowing mechanism, the waste suction pipe and the hot pressing mechanism are arranged on the machine frame and matched with one another for film tearing, the product quality is not affected due to the fact that products are not in contact, the film tearing machine can achieve automatic feeding and discharging due to the arrangement of the automatic feeding mechanism and the automatic discharging mechanism, the film tearing machine can work automatically after the automatic feeding mechanism is full of label paper, and the film tearing machine automatically works in the whole process, does not need manual operation, and is high in working efficiency, simple and clear to operate and stable in running performance.
Owner:深圳市恒兴安实业有限公司

Anti-clogging powder feeding device and method for low bulk ratio metal powder products

ActiveCN107262736BGuaranteed patencyAvoid tappingMetal powderDecomposer
The invention discloses an anti-blocking powder discharging device and method for low-loose-density metal powder products. The device comprises a decomposer, a middle bin and a produced powder material bin, and the decomposer, the middle bin and the produced powder material bin are sequentially connected from top to bottom; the tops of the middle bin and the produced powder material bin are each provided with an exhausting port; the bottom of the middle bin is provided with a discharging valve; the device further comprises a decomposed gas dust remover, a disinfecting replacement gas dust remover and a dust collecting powder material bin; an inlet of the decomposed gas dust remover is connected with the exhausting port of the middle bin and the exhausting port of the produced powder material bin through pipelines; the top of the dust collecting powder material bin is provided with a dust collecting port and a disinfecting port; an inlet of the disinfecting replacement gas dust remover is connected with the exhausting port of the produced powder material bin and the disinfecting port through pipelines; and the dust collecting port is connected with an outlet of the decomposed gas dust remover and an outlet of the disinfecting replacement gas dust remover through pipelines. The device and method are good in powder discharging smoothness and high in powder product quality.
Owner:JINCHUAN GROUP LIMITED

Raw material sieving machine for production of calculus bovis factitius

The invention discloses a raw material sieving machine for production of calculus bovis factitius. The raw material sieving machine comprises a sieving machine main body, a feeding inlet is formed inthe upper end of the sieving machine main body, and two sets of symmetrical supporting plates are arranged in the sieving machine main body; springs are arranged above the two sets of supporting plates correspondingly and fixedly connected with a first sieving plate through connecting blocks; the upper side of the first sieving plate is fixedly connected with the lower side of a second sieving plate through connecting rods; and a vibrating motor is arranged on the lower portion of one end of the first sieving plate, and one end of an output shaft of the vibrating motor is fixedly connected with the lower portion of one end of the first sieving plate through a connecting block. According to the raw material sieving machine for production of the calculus bovis factitius, the vibrating motoris utilized to provide vibration force for the two sieving plates, sieving operation of raw materials is achieved, the first sieving plate and the connecting block are fixed by adopting a clamping connection mode, and an operator can conveniently dismount and mount the sieving plates for clearing the sieving plates through the position of a mounting door; and a spraying head is arranged in the sieving machine, and the interior of the sieving machine is flushed through the spraying head.
Owner:武汉百草园生化药业有限公司
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