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Dry recovery system and method of reduction tail gas produced in polysilicon production process

A dry recovery and production process technology, applied in the directions of hydrogen separation, using liquid contact hydrogen separation, using solid contact hydrogen separation, etc., can solve the problems of product quality decline, difficult maintenance, expensive bag filter, etc., and achieve simple molding. , the effect of low price

Active Publication Date: 2012-12-12
CHINA ENFI ENGINEERING CORPORATION
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] 1. The bag filter has poor high temperature resistance
Especially in the synthesis system of trichlorosilane and the hydrogenation of silicon tetrachloride to produce trichlorosilane, it was found that the bag filter was very prone to damage, resulting in a serious decline in the filtering effect and eventually causing blockage of the subsequent system;
[0005] 2. The bag filter is easily damaged, which will cause a large increase in the amount of dust in the gas, and eventually cause a sharp decline in product quality;
[0006] 3. Cloth bag filter is expensive. At present, the imported filter material is converted to the finished filter bag, and the price per square meter reaches more than 1,000 yuan;
[0007] 4. The filter material of the cloth bag filter has poor corrosion resistance, and at the same time, the support is easy to corrode during the maintenance process, resulting in difficult maintenance and high maintenance costs

Method used

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  • Dry recovery system and method of reduction tail gas produced in polysilicon production process
  • Dry recovery system and method of reduction tail gas produced in polysilicon production process
  • Dry recovery system and method of reduction tail gas produced in polysilicon production process

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Embodiment 1

[0079] Such as Figure 6 As shown, firstly, the reduction tail gas is bubbled and washed through the washing tower 40 to remove the high-chlorosilane and solid impurities in the reduction tail gas. The components of the reduction tail gas are chlorosilane, hydrogen and a small amount of hydrogen chloride.

[0080] Pass the rinsed reduction tail gas into the absorption system 50 for absorption and desorption, so as to absorb the rinsed reduction tail gas, remove the chlorosilane and hydrogen chloride in it, and obtain hydrogen (which contains a trace amount of hydrogen chloride and a trace amount of chlorosilane). The absorbed chlorosilanes and hydrogen chloride can be further separated to obtain chlorosilanes and hydrogen chloride respectively. The separated chlorosilane can participate in the reduction reaction again after purification, and the reduction tail gas after the reaction is recovered through the dry recovery system again to form a recycling. The separated hydrogen...

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Abstract

The invention discloses a dry recovery system and a dry recovery method of reduction tail gas produced in a polysilicon production process. The system comprises a leaching tower, an absorption system, an absorption device, and a first filtering device. The absorption system is used for carrying out an absorption treatment upon leached reduction tail gas, such that chlorosilane and hydrogen chloride in the leached reduction tail gas can be removed, and hydrogen can be obtained. An adsorbentused for carrying out an absorption treatment upon the hydrogen is arranged in the absorption device, such that residual chlorosilane and hydrogen chloride in hydrogen can be further removed by adsorption. The first filtering device is used for filtering the hydrogen processed through the absorption treatment, such that high-purity hydrogen is obtained. A ceramic filter core is arranged in the first filtering device. According to the dry recovery system provided by the invention, a gas filtering device provided with the ceramic filter core is adopted. The filtering device has excellent properties of high-temperature resistance and corrosion resistance. Therefore, no influence is caused upon polysilicon product quality.

Description

technical field [0001] The invention relates to the technical field of polysilicon production technology, and more specifically, the invention relates to a dry recovery system and method for reducing tail gas generated in the polysilicon production process. Background technique [0002] More than 85% of the process technology of polysilicon projects in my country at this stage belongs to Siemens process technology. In the process of this process, there are many systems that need to carry out gas filtration. Specifically: hydrogenation of silicon tetrachloride to produce trichlorosilane system, trichlorosilane synthesis system, reduction tail gas dry recovery system, etc. [0003] At present, the filters generally used are cloth bag filters, but in the production process, it is found that the cloth bag filters have the following disadvantages: [0004] 1. The bag filter has poor high temperature resistance. Especially in the synthesis system of trichlorosilane and the hydro...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B3/52C01B3/56
Inventor 万烨严大洲毋克力肖荣晖汤传斌
Owner CHINA ENFI ENGINEERING CORPORATION
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