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79results about How to "Effective complexation" patented technology

High-salinity non-aqueous electrolyte and use thereof

The invention discloses a high-salinity non-aqueous electrolyte. The high-salinity non-aqueous electrolyte comprises a lithium salt and a non-aqueous organic solvent, and the concentration of the lithium salt is 2-10mol / L. The invention also discloses a use of the high-salinity non-aqueous electrolyte in a lithium or sodium cell system. The high-salinity non-aqueous electrolyte has the advantages of high thermal stability, low volatility, high safety, electrochemical widow and aluminum foil corrosivity, and lithium or sodium dendrite overcoming.
Owner:INST OF PHYSICS - CHINESE ACAD OF SCI

Composite soil adsorbent for preventing high-content soil in concrete from adsorbing poly-carboxylic water reducer, and preparation method and using method of composite soil adsorbent

The invention provides a composite soil adsorbent for preventing high-content soil in concrete from adsorbing a poly-carboxylic water reducer, and a preparation method and using method of the composite soil adsorbent. The composite soil adsorbent is prepared from the following raw materials by mass percent: 10 to 20% of a dispersion thinner, 5 to 10% of a retarder, 0.5 to 2.5% of an ion complexing agent, 0.2 to 0.5% of a surfactant and the balance of water. The preparation method comprises the following steps: stirring the dispersion thinner and water in a reaction kettle until the dispersion thinner is dissolved completely to obtain an even solution; adding the retarder and the ion complexing agent, and stirring until the retarder and the complexing agent are dissolved completely; finally, adding the surfactant, heating by a water bath, and stirring uniformly, so as to obtain a product. The using method comprises that the mixing amount of the composite soil adsorbent which is used cooperatively with a poly-carboxylic water reducer mother solution or replaces a part of the poly-carboxylic water reducer mother solution is 0.2 to 0.5% of that of a cementing material. By adoption of the composite soil adsorbent, the preparation method and the using method, the adsorbing of the soil to the poly-carboxylic water reducer is reduced, therefore, the comprehensive properties of the concrete are improved remarkably, and the problem of poor usability of the poly-carboxylic water reducer in the concrete with high soil content is solved.
Owner:SHIJIAZHUANG CHANGAN YUCAI BUILDING MATERIALS

Method for preparing white carbon black and manganese fertilizer from manganese leaching residue

The invention discloses a method for preparing white carbon black and manganese fertilizer from manganese leaching residue. The method comprises the following steps: 1, washing the manganese leaching residue with dilute sulphuric acid solution and running water in turn to obtain the residue; 2, conducting reaction between the residue and 25 to 40% strong base solution by mass at 90 to 120 DEG C for 2 to 5 h, and filtering to obtain filtrate; 3, decoloring the filtrate with active carbon and then carboxyl-terminated hyperbranched polyester at 100 to 120 DEG C to obtain the aqueous solution of silicate; 4, adding water and then inorganic acid and carboxyl-terminated hyperbranched polyester for reaction at 40 to 90 DEG C for 0.5 to 2 h to obtain the white carbon black; and 5, drying and dehydrating the residue obtained in step 2 and adding into a high-speed mixer, adding phosphoric acid, anticaking agent and manganese sulfate into the high-speed mixer, and mixing at room temperature for 10 to 20 min to obtain the manganese fertilizer. The method is simple in process and low in cost and is suitable for industrial production; and the silicon dioxide content of the prepared white carbonblack is more than 95% by mass, the specific area is more than 270 m<2> / g and the particle size is less than 50 nm.
Owner:SOUTH CENTRAL UNIVERSITY FOR NATIONALITIES

Boron-containing gel polymer electrolyte and preparation method and application thereof

The invention belongs to the technical field of polymer electrolytes, and particularly relates to a boron-containing gel polymer electrolyte and a preparation method and application thereof. The gel polymer electrolyte is prepared from lithium salt, an organic solvent, a photoinitiator, boron-containing heterocyclic photosensitive monomers and acrylate monomers in a copolymerization mode. The preparation method of the gel polymer electrolyte includes the steps that a compound containing boric acid groups and an alkene compound with a diol structure are esterified to obtain boron-containing heterocyclic alkene monomers, and the boron-containing heterocyclic alkene monomers, the acrylate monomers, the photoinitiator, the lithium salt and the organic solvent are uniformly dispersed; a mould containing the mixed solution is irradiated by an LED lamp for surface photo-initiated polymerization, and the boron-containing gel polymer electrolyte is obtained. The boron-containing gel polymer electrolyte has high ionic conductivity and a high cationic transference number, effectively solves the problems of liquid leakage, corrosion, poor mechanical performance and the like of a liquid electrolyte in traditional lithium-ion batteries and can be applied to preparation of supercapacitors, lithium-ion batteries, hybrid supercapacitors and the like.
Owner:FUDAN UNIV

Boron-containing solid polymer electrolyte and preparation method and application thereof

The invention belongs to the technical field of an electrolyte material, especially a boron-containing solid polymer electrolyte and a preparation method and application thereof. The polymer electrolyte provided by the invention comprises high molecular polymer matrix and electrolyte salt. The preparation method comprises the steps of esterifying boric acid-containing compounds and alkene compounds with diol structures, thereby obtaining boron heterocycle-containing vinyl monomer, uniformly dispersing the boron heterocycle containing vinyl monomer, initiator, the electrolyte salt and organic solvent, carrying out free radical polymerization, and drying obtained mixture, thereby obtaining the boron-containing solid polymer electrolyte. The boron-containing solid polymer electrolyte has the advantages of high ion conductivity, high cation transference number, good mechanical property and excellent electrode / electrolyte interface interaction and can be applied to fields such as a supercapacitor, a lithium ion battery, a hybrid supercapacitor and a fuel battery. The supercapacitor assembled with the polymer electrolyte has the advantages of wide electrochemical window, long cycle life and high security.
Owner:FUDAN UNIV

Method for measuring free acid concentration in acid liquid

The invention provides a fast and accurate method for measuring free acid concentration in acid liquid. An automatic potentiometric titrator is used to measure total acidity of the acid liquid. EDTA (ethylene diamine tetraacetic acid) which prevents iron ions, aluminum ions and the like from hydrolyzing is used as a screening agent to eliminate influence of hydrolysis of the iron ions, the aluminum ions and the like to free acid measurement. The defect that pH jump of the free acid is fully or partially covered during automatic potentionmetric titration is avoided. Jump of equivalent point is increased, and accuracy of the measurement is increased. An analysis result is automatically calculated according to an input formula. Operation time from analysis to result obtaining is shortened to less than 10 minutes. In addition, the method is low in sampling amount, fine in reproducibility, and accurate in analysis results. By the method, labor intensity of analysts is reduced, and labor productivity is emancipated.
Owner:武钢集团有限公司

Copper cleaning agent and preparation method thereof

The invention discloses a copper cleaning agent and a preparation method thereof. The copper cleaning agent disclosed by the invention consists of an inorganic acid, an organic acid, a surfactant, a penetrating agent, an emulsifier, a defoaming agent, a complexing agent and water. The inorganic acid and the organic acid are compounded, the hazards to health of cleaning workers caused by individual use of the inorganic acid in the traditional cleaning agent are avoided, over etching of a copper workpiece is also avoided, the copper cleaning agent is an environmental-friendly cleaning agent and has a certain oiliness, an effect of cleaning dirt such as oil attached to the surface of a copper part is improved by using the cleaning agent, the cleaning agent solution is acidic, and the oxide skin on the surface of the copper part can be well removed. The cleaning agent prepared by the invention is simple in using method, the copper part only needs to be soaked at normal temperature for 2-5 minutes so as to be cleaned, no greasy dirt residue is left on the cleaned copper part, the color of the surface of the copper part is the copper base color, and the cleaning effect is obvious. The copper cleaning agent disclosed by the invention is simple in preparation method, low in cost and obvious in effect and is suitable for industrial production and application.
Owner:PINGGAO GRP +1

High-voltage lithium-ion battery with Si/C composite anode

The invention discloses a high-voltage lithium-ion battery with a Si / C composite anode. The high-voltage lithium-ion battery comprises a cathode, an anode as well as a separator and a non-aqueous electrolyte placed between the cathode and the anode, wherein the active substance of the cathode is lithium transition metal oxide; the active substance of the anode is a Si-based substance; the separator is a ceramic separator; the non-aqueous electrolyte comprises a non-aqueous organic solvent, lithium salt and an additive, the additive comprises FEC (fluoroethylene carbonate) and isocyanurate compounds in the mass ratio being (6-36):1. Compared with the prior art, the lithium-ion battery using the electrolyte has excellent normal-temperature cycle performance, high-temperature cycle performance and high-temperature storage life, and the gas output in the high-temperature storage process can be remarkably reduced.
Owner:GUANGZHOU TINCI MATERIALS TECH

Processing method capable of preventing abalone soup cans from blackening

The invention discloses a processing method capable of preventing abalone soup cans from blackening. The method comprises the following steps: timely performing anti-blackening color protection process treatment for three times during fishing of abalone, workshop pretreatment and pre-boiling and soup-loading process, and then performing sterilization and storage. Through the three times of timely continuous anti-oxidation and anti-blackening color protection treatment with seamless oxygen contact, the original color, luster and quality of products can be effectively kept.
Owner:福州日兴水产食品有限公司

Heteroatom-doped carbon-based non-noble metal compound electrocatalyst and preparation method thereof

The invention provides a preparation method of a heteroatom-doped carbon-based non-noble metal compound electrocatalyst. The preparation method comprises the following steps of A) mixing a carbon precursor obtained by oxidization processing on a carbon raw material and acidulated graphite-phase carbon nitride in an aqueous solution, and then adding a transition metal salt and a precipitant to obtain a composite precursor; and B) performing thermal processing on the composite precursor to obtain the heteroatom-doped carbon-based non-noble metal compound electrocatalyst, wherein different-polarity charges are carried on a surface of the carbon precursor and a surface of the acidulated graphite-phase carbon nitride in the aqueous solution. By the method for processing the composite precursorby one step, effective control on types and content of heteroatom doping and types, morphology and dispersibility of metal compound constituents is simply and effectively achieved, very high mutual bonding force and synergic effect are achieved among the heteroatom-doped carbon-based non-noble metal compound composite material constituents, and excellent performance is shown when the heteroatom-doped carbon-based non-noble metal compound electrocatalyst is used as an electrocatalytic oxidization-reduction catalyst.
Owner:SAIC MOTOR

Tin dioxide/porous carbon composite lithium battery negative electrode material and preparation method

The invention discloses a tin dioxide / porous carbon composite lithium battery negative electrode material and a preparation method. The preparation method comprises the following steps: with fibroin and a high molecular polymer PAMAM as precursors, soaking a fibroin / PAMAM composite material after freeze drying treatment in a stannous sulfate aqueous solution for sufficient adsorption; performing high-temperature calcination to obtain the lithium battery negative electrode material. Sn<2+> and amino groups (mainly tertiary amino groups) in the PAMAM dendrimer can generate an effective complexing action so that the SnO2 nanoparticles are in-situ compounded on the surface of the fibroin / PAMAM; therefore, the yield of tin dioxide / porous carbon compound is higher, the uniform stability is better, and a lithium ion battery negative electrode material with high specific capacity and long cycle life is prepared finally.
Owner:赵兵

Mercury ion rapidly absorbing composite sponge absorbent and preparation and application methods thereof

The invention relates to a composite sponge absorbent capable of rapidly and efficiently absorbing mercury ions in aqueous solution and preparation and application methods thereof. The preparation method comprises taking cellulose, lignin and wheat protein powder, which are low in price and easy to acquire, as base materials, performing high-speed dispersion to obtain a suspension, then adding inchitosan, chitin and polyvinyl alcohol or polyethylene glycol of different quantities, and through a simple crosslinking and freeze-drying combined method, preparing the compound sponge absorbent. Overall preparation processes are implemented in aqueous solution and accordingly are simple in processes and operation without special technical equipment, thereby being low in cost. The prepared compound sponge absorbent is rapid in absorbing speed, high in selective absorption to mercury ions, low in influence of pH, recyclable, green and environmentally friendly, thereby having a good applicationprospect during practical heavy metal wastewater treatment.
Owner:XINJIANG TECHN INST OF PHYSICS & CHEM CHINESE ACAD OF SCI

Viscosity stabilizing agent used for polymer flooding

ActiveCN103275679AImprove field application effectHigh viscosityDrilling compositionIsothiazolinoneEthylene diamine
A viscosity stabilizing agent used for polymer flooding is characterized by comprising components in percentage by mass as follows: 5%-8% of 2-mercapto benzimidazole, 2%-3% of hydroquinone, 10%-15% of sodium thiosulfate, 10%-15% of isothiazolinone, 5%-10% of glutaraldehyde, 6%-10% of isopropanol, 1%-2% of EDTA (ethylene diamine tetraacetic acid), and the balance of water. The viscosity stabilizing agent used for polymer flooding can improve viscosity stability of a polymer flooding system, the viscosity maintaining time is long, so that on the condition of oilfield wastewater preparation, the viscosity of the polymer flooding system maintains stable and is improved in a certain range, the field application effect of the polymer flooding is improved, the effect is remarkable, and the viscosity stabilizing agent is suitable for popularization and application.
Owner:DAQING HUAYING CHEM IND

Non-aqueous electrolyte and lithium ion battery

The invention provides a non-aqueous electrolyte and a lithium ion battery. The non-aqueous electrolyte comprises a solvent, an electrolyte lithium salt and a functional additive, wherein the functional additive comprises 4,4'-dipinacol borate diphenyl sulfone, dipyridyl carbonate and lithium difluorophosphate. When the electrolyte provided by the invention is applied to a lithium ion battery of ahigh-nickel ternary material / graphite system, the impedance of the lithium ion battery can be remarkably reduced, the power performance of the lithium ion battery can be improved, gas production of the lithium ion battery in circulation and storage processes can be remarkably inhibited, and the rate capability, the normal-temperature cycle performance, the high-temperature cycle performance, thehigh-temperature storage performance and the safety performance of the lithium ion battery are remarkably improved.
Owner:DONGGUAN DONGYANG SOLAR SCI RES & DEV CO LTD

Method for recovering gold from gold-containing barren solution and purifying gold-containing barren solution

The invention discloses a method for recovering gold from gold-containing barren solution and purifying the barren solution. In the method, sulfuric acid is added into gold-containing cyanide barren solution to perform acidification precipitation, pH value of the solution is regulated to be less than or equal to 2, ferrocyanide, copper, zinc and lead in the gold-containing cyanide barren solution are separated and removed from the gold-containing cyanide barren solution in a precipitate mode; lime is added into the separated acidic supernatant for neutralizing until the pH value is between 10 and 12, and formed calcium sulfate precipitate is removed; and a calcium removing agent is added into the separated basic supernatant, the formed precipitate is removed, and the separated supernatant is returned to the gold leaching process, wherein before the acidification precipitation step, a bactericide is added to the gold-containing cyanide barren solution, and the gold-containing cyanide barren solution is subjected to multi-medium filtration, microfiltration and first nano-filtration in sequence. According to the method for recovering gold from the gold-containing barren solution and purifying the barren solution, the dosage of acid agent is greatly reduced, and the treatment cost for the barren solution is reduced.
Owner:FUJIAN SHUANGQISHAN MINING

Preparation method of calcium, strontium and barium scale inhibitor

InactiveCN104045172AEffective complexationSolve the problem of high phosphorusScale removal and water softeningSulfateRoom temperature
The invention relates to a preparation method of a calcium, strontium and barium scale inhibitor. The method comprises the following steps: adding 80-120kg of organic acid anhydrides, 15-35kg of acetate and 150-250kg of deionized water into a 500L reaction kettle, adding 0.5-1kg of an initiator, heating to 80-100DEG C, adding 30-80kg of an organic acid in a dropwise manner, and reacting for 6-8h; and adding 5-25kg of sodium hydroxide, cooling to room temperature, adding 50-100kg of a complexing agent, stirring for 30min, filtering, and discharging. The introduction of the complexing agent with a high complexation effect enables barium and strontium ions in oilfield produced water to be effectively complexed, and the generation of sulfate scales is prevented by using complexation solubilizing, dispersion and crystal distortion effects.
Owner:JIANGSU JIAHUA ADVANCED MATERIALS TECH

Special foam-free composite bactericide for shale gas well pipeline, and preparation method thereof

The invention provides a special foam-free composite bactericide for shale gas well pipelines, and a preparation method thereof, and solves the use defects of low effective concentration, large foam amount, certain corrosivity, toxicity and weak irritation of quaternary ammonium salt bactericides in the prior art, and the technical problems of secondary pollution to the environment and drug resistance of microorganisms due to long-term large-scale use. The composite bactericide is prepared from the following raw materials in parts by weight: 1-6 parts of iodine, 1-5 parts of a stabilizer, 18-40 parts of short-chain tertiary amine, 10-51 parts of a solvent, 16-51 parts of hydrogen peroxide, 1-5 parts of a pH regulator and 2-20 parts of a synergist. According to the invention, the special foam-free composite bactericide is used for sterilizing by using iodine, and is an efficient, rapid, broad-spectrum, high-bactericidal-power, low-toxicity and environment-friendly bactericide; and due to the non-foaming property of the stabilizer, the gas production rate of shale gas exploitation is not influenced.
Owner:四川长宁天然气开发有限责任公司 +2

Host-guest assembled supramolecular gel based on functionalization of trimesoyl chloride and its preparation method and use

The invention designs and synthesizes host-guest assembled supramolecular gel based on the functionalization of trimesoyl chloride. N-amino-1, 8-naphthalic anhydride functionalized trimesoyl chlorideas a main body and 4-amino pyridine-functionalized trimesoyl chloride as a guest are complex and assembled into the gel in a H2O-DMSO system. The supramolecular gel has good fluorescence emission properties and emits yellow-green fluorescence when the excitation wavelength is 380nm. A series of aqueous cationic solutions are added to the supramolecular gel, and only Fe<3+> can quench the fluorescence of the supramolecular gel. In the metal gel TG-Fe formed by coordination of the supramolecular gel and Fe<3+>, a series of anions are added respectively. Only H2PO4<-> can restore the fluorescenceof the metal gel TG-Fe. This competitive coordination recognition property has an important application value in the field of ion identification.
Owner:NORTHWEST NORMAL UNIVERSITY

Anti-seismic prefabricated house

The invention discloses an anti-seismic prefabricated house, comprising a plurality of steel plates, wherein the outer side of each steel plate is treated by a phosphating solution to form a phosphating film, and the phosphating solution comprises the following components in parts by weight: 35-45 parts of phosphoric acid, 0.2-0.4 parts of copper nitrate, 20-25 parts of zinc oxide, and 10-15 partsof compound accelerant. The anti-seismic prefabricated house provided by the invention has the advantages: as the main film-forming materials, the phosphoric acid and zinc oxide can form a continuous and uniform phosphating film on the surface of the processed. Meanwhile, the addition of the compound accelerator further improves the film forming speed and film forming quality of the phosphatingfilm. In addition, because the electrode potential of copper is higher than that of iron, copper ions are reduced and deposited on the surface of a phosphated hinge body, so the cathode area on the surface is increased; the electrochemical reaction of phosphating is further promoted, the formation of phosphating crystal nucleus is accelerated, crystal grains are refined, and the phosphating film is compact and uniform; meanwhile, the phosphating speed is improved, the phosphating temperature is reduced, and finally the phosphating film has the advantages of compact film formation and strong adhesive force.
Owner:浙江华锦建筑装饰设计有限公司

Environmental-friendly solution capable of inhibiting generation rate of tetravalent tin

The invention discloses an environmental-friendly solution capable of inhibiting the generation rate of tetravalent tin. The solution is prepared from the following components according to the concentration: 10 to 30g / L of stannous ion, 70 to 130g / L of thiourea, 30 to 70g / L of methanesulfonic acid, 10 to 50mg / L of interfacial agent, 30 to 60g / L of sodium hexametaphosphate, 20 to 30g / L of ethylenediamine tetra sodium, 10 to 30g / L of sodium oxalate, 0 to 10g / L of cysteine, and 0 to 20g / L of ascorbic acid. The components are uniformly mixed so as to be prepared into a chemical solution; and thechemical solution has the characteristics that under the conditions of ensuring the good stability of the solution and the stable tin deposition rate, the rate for oxidizing divalent tin into the tetravalent tin is effectively inhibited, and substances and byproducts contained in the formula are safe, environmental-friendly and friendly to the environment. According to the environmental-friendly solution capable of inhibiting the generation rate of the tetravalent tin provided by the invention, multiple complexing agents are contained in the formula, the stannous ions cannot be easily oxidizedinto the tetravalent tin, and the oxidation of oxygen dissolved in a plating solution on the stannous ions can be removed by utilizing a reducing agent.
Owner:SHENZHEN CHENGGONG CHEM

Modification method of humic acid and application of product thereof in soil remediation

The invention relates to a modification method of humic acid and an application of a product thereof in soil remediation and belongs to the technical fields of surfactants and soil remediation. Therefore, the problems of poor surface activity and poor polluted soil remediation capability of the humic acid in the prior art can be solved. The method comprises the following steps: performing alkylation reaction on the humic acid and an alkylation reagent, namely halogenated alkane to get alkylated humic acid; and then performing sulfomethylation reaction with a sulfomethylation reagent so as to get a final humic acid modified product. The method disclosed by the invention is simple in technological process and easy to operate, and the obtained humic acid modified product is higher in surface activity and enables the strength of hydrophilicity to be matched with that of lipophilicity; and the humic acid modified product can also better remedy the polluted soil and particularly has the remediation capability in the aspects of remedying the soil polluted by heavy metals and the soil polluted by organic matters.
Owner:杭州韦尔茂通环境技术有限公司

Method for preparing polycrystalline SnSe2 material by solution method

The invention discloses a method for preparing a polycrystalline SnSe2 material by a solution method. The method comprises the steps that selenium powder is dispersed in an oleic acid solution to obtain a precursor solution A of a selenium source; then water vapor of the precursor solution A is removed under vacuuming conditions to obtain an environment without oxygen or water vapor; then the temperature rises, heating and heat preservation are conducted, and the precursor solution A is sucked to be added into a mixed solution B composed of a stannum source and ethanol to obtain a mixed solution C, wherein the volume ratio of the precursor solution A to the mixed solution B is (5-7):(25-30); then the mixed solution C is subjected to an alcohol thermal reaction, and drying is conducted to obtain SnSe2 powder. The preparation method is simple, the repeatability is high, the addition of any catalyst is not needed, expensive and complicated equipment is not involved, waste liquid generatedby the reaction is easy to handle, and the method is friendly to the environment and an operator.
Owner:广州新致信息科技有限公司

Preparation method for acidic fertilizer

The invention relates to a preparation method for an acidic fertilizer. The preparation method comprises the following steps: mixing of phosphoric acid with urea; reaction after completion of mixing;and granulating and drying. The acidic fertilizer provided by the invention comprises urea phosphate and ammonium bisulfate and has a pH value of 2.5 to 3.5, so the pH value of alkaline soil can be reduced, and the volatilization loss of ammonium nitrogen in the alkaline soil is reduced; in addition, the stability of amide nitrogen can be increased, and activation effects can be exerted on phosphorus and medium-trace elements; meanwhile, the phosphorus can be avoided from fixation by elements like calcium and magnesium, and the moving ability of the phosphorus is improved; when the pH value ofthe acidic fertilizer is lower than 2.5, the acidic fertilizer has too great viscosity and is easy to absorb moisture; and when the pH value of the acidic fertilizer is excessively high, the pH valueof soil can not be effectively reduced, and the purpose of activating the phosphorus and the medium-trace elements can not be achieved.
Owner:菏泽金正大生态工程有限公司 +2

Preparation method of reverse osmosis membrane antisludging agent with high iron content

The invention relates to a preparation method of a reverse osmosis membrane antisludging agent with the high iron content. The preparation method comprises the following steps: firstly placing 50g of diethylenetriamine pentaacetic acid ammonium salt in a 250mL beaker, and stirring until the diethylenetriamine pentaacetic acid ammonium salt dissolves to obtain a solution; secondly adding 50g of polyaspartic acid into the solution, and carrying out water-bath stirring for 60 minutes at the temperature of 45 DEG C to obtain a mixture; and finally, cooling the mixture to the room temperature to obtain a finished product. The preparation method has beneficial effects that the diethylenetriamine pentaacetic acid ammonium salt and the polyaspartic acid are compounded to form a novel reverse osmosis membrane antisludging agent, the antisludging agent can be effectively complexed with iron ions in water and is high in antisludging capability for calcium carbonate and calcium sulfate, the cost is low, and the secondary pollution on a membrane can be avoided.
Owner:WEIHAI XIANGYU TECH

Lithium ion battery electrolyte, preparation method and lithium ion battery

The invention provides a lithium ion battery electrolyte, a preparation method thereof and a lithium ion battery. The lithium ion battery electrolyte comprises a solvent, an electrolyte lithium salt and an additive, the electrolyte lithium salt and the additive are dispersed in the solvent, and the additive is pentafluorophenyltriethoxysilane. The pentafluorophenyltriethoxysilane is used as an additive, so that the pentafluorophenyltriethoxysilane can be oxidized earlier than other materials of the electrolyte, and an oxidation product can form a more stable film with lower internal resistanceon an interface so as to inhibit decomposition of the electrolyte; meanwhile, pentafluorophenyltriethoxysilane can effectively adsorb byproducts hydrogen fluoride and hydrogen ions and fluorine ionsformed by ionization of the byproducts hydrogen fluoride, stripping of active substances caused by corrosion of the byproducts is prevented, and the long-cycle stability of the battery is guaranteed.
Owner:SOUTH CHINA NORMAL UNIVERSITY

Composite adsorption material for removing hypochlorite from water and preparation method for adsorption material

The invention discloses an adsorption material for hypochlorite and a preparation method for the adsorption material, and belongs to the field of material preparation. The preparation method comprises the following steps of: cooking timothy hay serving as a raw material, adding a sulfuric acid solution at certain mass concentration, and stirring; treating suspension by using an ultrasonic oscillator, performing centrifugal precipitation, and filtering; and mixing a product and K2CO3 in a mass ratio of 1:1, activating under the protection of N2, cooling, washing until the solution is neutral, and drying to obtain the adsorption material with high adsorption property. The preparation method is innovative, novel and unique, and the prepared material has a good adsorption effect on the hypochlorite in water.
Owner:CHANGZHOU UNIV

Preparation method of biomass source N/P co-doped carbon aerogel/cross-linked chitosan composite membrane electrode

According to the preparation method of the biomass source N / P co-doped carbon aerogel / crosslinked chitosan composite membrane electrode, cheap natural biomass with a natural plant fiber sponge structure, such as shaddock peel and bagasse, which are agricultural processing wastes, is used as a raw material, and the N / P co-doped carbon aerogel with a developed mesoporous structure is prepared through the processes of pre-carbonization, high-temperature carbonization and the like; furthermore, the N / P co-doped carbon aerogel and chitosan are compounded to prepare an electro-adsorption membrane electrode for electro-adsorption separation of uranium in uranium-containing wastewater, so that the production cost is reduced and the material performance is improved. The biomass source N / P co-dopedcarbon aerogel / chitosan composite membrane electrode has a high specific surface area, good conductivity and chemical stability and is suitable for industrial production. When used for electro-adsorption separation of uranium in uranium-containing wastewater, the composite membrane electrode has high uranium recovery rate and adsorption capacity, and can meet industrial production requirements.
Owner:EAST CHINA UNIV OF TECH

Titanium seed etching liquid for wafer level package

The invention discloses titanium seed etching liquid for wafer level package. The etching liquid is formed by mixing a component A and a component B according to the size proportion before use. The proportion of the component A and the component B is (0.8-1):1. The component A is hydrogen peroxide. The component B comprises, by concentration, 40-80 g / L of citric acid, 0.1-10 g / L of hydrogen peroxide stabilizer, 0.1-10 g / L of lateral erosion preventing agent, 30-90 g / L of dipotassium phosphate, 2-6 g / L of monopotassium phosphate and 0.1-10 g / L of surface activator. After being prepared according to the component proportion, the component B is mixed with the component A uniformly according to the proportion. After the component A and the component B are mixed uniformly, pH buffering liquid is added according to needs to adjust the pH value to be controlled within 8-9, and thus the titanium seed etching liquid is formed. The titanium seed etching liquid needs to be used when the temperature is between 30 DEG C and 60 DEG C. The titanium seed etching liquid has the characteristics of being stable in performance, suitable for super-thin line, and small in lateral erosion, and nearly having no corrosion to copper and aluminum.
Owner:成功环保科技(南通)有限公司

Reclaimed water recycling reverse osmosis membrane cleaning agent

The invention discloses a reclaimed water recycling reverse osmosis membrane cleaning agent, and belongs to the technical field of membrane element cleaning. The cleaning agent comprises an acidic cleaning agent and an alkaline cleaning agent. The acidic cleaning agent comprises the following main components in percentage by weight: 0.02-0.2% of hydrochloric acid, 0.1-0.2% of organic acid and thebalance of water. The alkaline cleaning agent comprises the following main components in percentage by weight: 0.05-0.2% of sodium hydroxide, 0.01-0.1% of biosurfactant, 0.02-0.2% of metal complexingagent, 0.01-0.1% of bactericide, and the balance of water. A use method comprises the following steps: cleaning the reverse osmosis membrane with the acidic cleaning agent, then cleaning the reverse osmosis membrane with the alkaline cleaning agent, and washing the reverse osmosis membrane with clear water after cleaning with the acidic cleaning agent and the alkaline cleaning agent, wherein during on-line cleaning, a part of concentrated water and produced water need to be discharged into a wastewater pool at the initial stage of cleaning. The reverse osmosis membrane cleaning agent disclosedby the invention is an environment-friendly composite formula which is easy to biodegrade, all the components play a role in coordination and synergy during cleaning, the cleaning agent has excellentcleaning performance on a reverse osmosis membrane which is seriously polluted during reclaimed water recycling, and the usage amount of the cleaning agent is small.
Owner:HIGH & NEW TECH RES CENT OF HENAN ACAD OF SCI
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