Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Method for detecting organic matter content of soil

A technology of organic matter content and detection method, which is applied in the preparation of test samples, material analysis by observing the effect on chemical indicators, and analysis by chemical reaction of materials, etc. Complexity, analysis errors and other problems, to achieve the effect of improving stability and accuracy, simplifying analysis operation steps, and enhancing analysis capabilities

Inactive Publication Date: 2020-06-30
SHANGHAI BAOSTEEL IND TECHNOLOGICAL SERVICE
View PDF4 Cites 1 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The existing heating and digestion methods mainly include (1) electric heating plate and electric sand bath reflux heating, which are difficult to control the temperature of such methods; (2) oil bath reflux heating, which is troublesome to clean and pollutes the analysis environment
Moreover, the above heating methods all have problems such as low heating efficiency, difficulty in batch analysis, complicated procedures, acid mist pollution to the environment, and easy introduction of analysis errors.
[0004] In the existing ferrous sulfate titration method, the color end point of some complex samples is not clear during ferrous sulfate titration, and errors are prone to occur, and ferrous sulfate is easily oxidized, so ferrous sulfate needs to be calibrated before each titration
Therefore, the traditional organic matter content detection pretreatment operation is complicated, the accuracy is poor, and the detection efficiency is low.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Method for detecting organic matter content of soil
  • Method for detecting organic matter content of soil
  • Method for detecting organic matter content of soil

Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0014] The method for detecting soil organic matter content of the present invention includes the following steps:

[0015] Step 1. Pre-treatment of soil heating digestion. Accurately weigh 0.1000~0.2000g air-dried soil sample to a digestion tube containing 3ml 0.4000mol / L potassium dichromate-sulfuric acid and 0.1g silver sulfate digestion solution, and add 2ml distilled water. The total volume is controlled to 5ml, and the digestion tube is placed in a COD digester preheated to 150°C for airtight digestion for 10 minutes;

[0016] Step 2. Draw the standard curve. Pipette 2000mg / L potassium hydrogen phthalate 0ml, 0.1ml, 0.2ml, 0.5ml, 1.0ml, 1.5ml to the digestion tube, add distilled water to 2ml, and configure it to 0mg / L. Organic carbon standard curve of L, 100mg / L, 200mg / L, 500mg / L, 1000mg / L, 1500mg / L, the correlation coefficient of the standard curve is r = 0.9994, the intercept a = 1.77×10 -2 , The slope b=2.93×10 -4 , Where the organic carbon digestion method is the same as ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses a method for detecting the organic matter content of soil, which comprises: carrying out soil heating digestion pretreatment, placing a sample in a digestion tube containing apotassium dichromate-sulfuric acid digestion solution, and carrying out sealed digestion for 10 min in a preheated COD digester; taking potassium hydrogen phthalate to prepare an organic carbon standard curve; then carryng out colorimetric analysis by adopting a spectrophotometric method, and multiplying the content of organic carbon read from a standard curve by an empirical coefficient to obtainthe content of organic matters in the soil. The method overcomes the defects of a traditional detection mode, adopts a closed digestion mode, improves the stability and accuracy of content detection,improves the digestion efficiency, has no environmental pollution, simplifies the analysis operation steps, enhances the analysis capability of complex samples, and is suitable for batch analysis.

Description

Technical field [0001] The invention relates to a method for detecting the content of soil organic matter. Background technique [0002] Soil organic matter generally refers to the material derived from life in the soil. Soil organic matter is an important component of the solid part of the soil and one of the main sources of plant nutrition. It can promote the growth and development of plants, improve the physical properties of the soil, and promote microorganisms and The activities of soil organisms promote the decomposition of nutrient elements in the soil, and improve the fertility retention and buffering properties of the soil; the content of soil organic matter is an important index to measure soil fertility, and has certain guidance for understanding the status of soil fertility, fertilizing and improving soil significance. [0003] At present, the detection method of organic matter content is heating digestion, then ferrous sulfate titration is used to determine the organi...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/78G01N1/44
CPCG01N1/44G01N21/78
Inventor 李静蒋文捷陈震芳金婷
Owner SHANGHAI BAOSTEEL IND TECHNOLOGICAL SERVICE
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products