A kind of preparation method of tobacco guarana extract
A technology for extracts and cigarettes, applied in the field of preparation of guarana extracts for cigarettes, can solve the problems of high cost and low recovery rate, and achieve the effects of dry and plump flue gas, high extraction rate, elegant and natural fragrance
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Embodiment 1
[0018] A preparation method of guarana extract for tobacco, comprising the following steps:
[0019] S1: Purification of guarana fruit: Clean the guarana, then crush it and place it in a tank, and add a soaking liquid with a mass of 9 times the guarana. Methyl chloride, tetraethyl orthosilicate, rhamnolipid, ultrasonic leaching, ultrasonic leaching time 30min, leaching temperature 30℃, ultrasonic power 350w, filter to obtain the leaching solution;
[0020] S2: Add the extracting liquid to the extracting liquid for extraction, the volume ratio of the extracting liquid and the soaking liquid is 0.5:1, and the extracting liquid includes octylphenol polyoxyethylene ether, sorbitol, 25% in a mass ratio of 1:1.2:5 Mass fraction of sodium sulfate aqueous solution, extraction temperature is 40 ℃, extraction time is 0.6h, then the upper layer is taken and filtered to obtain guarana filtrate;
[0021] S3: the guarana filtrate is placed in a drying box for drying, the drying temperature...
Embodiment 2
[0023] A preparation method of guarana extract for tobacco, comprising the following steps:
[0024] S1: Purification of guarana fruit: Clean the guarana, then crush it and place it in a tank, add a soaking solution with a mass of 10 times the guarana, and the soaking solution includes two 15:3:8 mass ratio Methyl chloride, tetraethyl orthosilicate, rhamnolipid, ultrasonic extraction, ultrasonic extraction time 20min, extraction temperature 45 ℃, ultrasonic power 300w, filter to obtain extract;
[0025] S2: Add the extracting liquid to the extracting liquid for extraction, the volume ratio of the extracting liquid and the soaking liquid is 0.4:1, and the extracting liquid includes octylphenol polyoxyethylene ether, sorbitol, 25% in mass ratio of 1:1.5:5 The mass fraction of sodium sulfate aqueous solution, the extraction temperature is 45 ° C, the extraction time is 0.5 h, and then the upper layer is taken and filtered to obtain the guarana filtrate;
[0026] S3: the guarana ...
Embodiment 3
[0028] A preparation method of guarana extract for tobacco, comprising the following steps:
[0029] S1: Purification of guarana fruit: clean the guarana, then pulverize it and place it in a tank, add a soaking solution with a mass of 9.5 times the guarana, and the soaking solution includes two parts with a mass ratio of 22:3:3. Methyl chloride, tetraethyl orthosilicate, rhamnolipid, ultrasonic extraction, ultrasonic extraction time 40min, extraction temperature 25 ℃, ultrasonic power 400w, filter to obtain extract;
[0030] S2: Add the extracting liquid to the extracting liquid for extraction, the volume ratio of the extracting liquid and the soaking liquid is 0.4:1, and the extracting liquid includes octylphenol polyoxyethylene ether, sorbitol, 25% octylphenol ethoxylate with a mass ratio of 1:1:6 The mass fraction of sodium sulfate aqueous solution, the extraction temperature is 30 ° C, the extraction time is 1 h, and then the upper layer is taken and filtered to obtain the...
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