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A processing method for leaf-shaped glass with surface

A processing method and leaf-like technology, applied in chemical instruments and methods, surface etching compositions, etc., can solve the problems of cumbersome process flow, high maintenance cost, irregular surface morphology of glass, etc., and achieve a high level of acid etching efficiency. Effect

Active Publication Date: 2022-06-24
(CNBM) BENGBU DESIGN & RES INST FOR GLASS IND CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But so far, the controllable synthesis of glass surface microstructures requires expensive lithography, etching, nanoimprinting and other technologies. Due to the expensive equipment itself, the disadvantages of high follow-up maintenance costs seriously restrict the special glass with surface microstructures. industrial application of
[0003] There are also many problems in the research of preparing anti-glare glass by ordinary acid etching method. For example, in the Chinese patent of "Preparation Method of Anti-glare Glass" (publication number CN101314522B), the acid etching solution needs to be aged for more than 6 hours. It is suitable for large-scale industrial production, and the surface of the prepared glass has irregular morphology and low haze, only 2%-8%
The Chinese patent of "A Frosting Liquid, Its Preparation Method, Application, and Method for Preparing Anti-Glare Glass" (publication number CN108191253A) requires gas to be introduced during the preparation process, and the process is relatively complicated, and the surface of the prepared anti-glare glass Irregular shape, low haze
All in all, there are currently problems in this field such as complex acid etching solution formula, cumbersome process flow, uncontrollable surface morphology, and low haze.

Method used

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  • A processing method for leaf-shaped glass with surface
  • A processing method for leaf-shaped glass with surface
  • A processing method for leaf-shaped glass with surface

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] The present invention provides a method for processing leaf-shaped glass on the surface, comprising the following steps:

[0025] S1. Take float glass and clean it; use 5% surfactant to clean first, then use deionized water and ethanol to clean in turn; the surfactant is sodium dodecyl benzene sulfonate; air dry naturally after cleaning dry spare;

[0026] S2. Encapsulate the cleaned float glass on one side to prevent acid corrosion protection;

[0027] S3. Immerse the encapsulated float glass in the acid etching solution, and the liquid level between the float glass and the acid etching solution is 45º;

[0028] The etching solution comprises 40% of ammonium bifluoride, 8% of sulfuric acid, 14% of potassium chloride, 3% of ammonium sulfate and 35% of water by weight percentage;

[0029] S4. Take out the acid-etched float glass, wash it with a brush, dry it after cleaning, remove the anti-acid-etching protective layer on the encapsulated surface, and obtain an unencap...

Embodiment 2

[0032] The present invention provides a method for processing leaf-shaped glass on the surface, comprising the following steps:

[0033] S1. Take float glass and clean it; use 10% surfactant to clean first, then use deionized water and ethanol to clean in turn; the surfactant is sodium dodecyl benzene sulfonate; air dry naturally after cleaning dry spare;

[0034] S2. Encapsulate the cleaned float glass on one side to prevent acid corrosion protection;

[0035] S3. Immerse the encapsulated float glass in the acid etching solution, and the liquid level of the float glass and the acid etching solution is 90º;

[0036] The etching solution comprises 30% of ammonium bifluoride, 10% of sulfuric acid, 15% of potassium chloride, 5% of ammonium sulfate and 40% of water by weight percentage;

[0037] S4. Take out the acid-etched float glass, wash it with a brush, dry it after cleaning, and remove the acid-etching protection layer on the encapsulated surface to obtain an unencapsulate...

Embodiment 3

[0040] The present invention provides a method for processing leaf-shaped glass on the surface, comprising the following steps:

[0041] S1. Take float glass and clean it; use 5% surfactant to clean first, then use deionized water and ethanol to clean in turn; the surfactant is sodium dodecyl benzene sulfonate; air dry naturally after cleaning dry spare;

[0042] S2. Encapsulate the cleaned float glass on one side to prevent acid corrosion protection;

[0043] S3. Immerse the encapsulated float glass in the acid etching solution, and the liquid level of the float glass and the acid etching solution is 60º;

[0044] The etching solution comprises 50% of ammonium bifluoride, 4% of sulfuric acid, 11% of potassium chloride, 5% of ammonium sulfate and 30% of water by weight percentage;

[0045] S4. Take out the acid-etched float glass, wash it with a brush, dry it after cleaning, remove the acid-etching protective layer on the package surface, and obtain an unpackaged surface wit...

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PUM

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Abstract

The invention discloses a method for processing leaf-shaped glass on the surface, which comprises the following steps: S1, taking float glass and cleaning it; S2, encapsulating the cleaned float glass on one side to prevent acid corrosion protection; S3 1. Immerse the encapsulated float glass in the acid etching solution, the liquid level of the float glass and the acid etching solution is 45-90°; the acid etching solution contains 30-50% ammonium bifluoride, 4-10% Sulfuric acid, 10-18% potassium salt, 1-5% ammonium salt, and 30-40% water; S4, take out the float glass after acid etching, clean it, remove the sealing surface after cleaning, and obtain the unpackaged Leaf-shaped glass on the surface; the method can prepare high haze glass with microstructure on the surface, and the process is simple and the surface morphology is easy to control.

Description

technical field [0001] The invention relates to the technical field of glass processing, in particular to a method for processing leaf-shaped glass on the surface. Background technique [0002] With the rapid development of science and technology, people have higher and higher requirements for the functions carried by glass. From frosted glass used in privacy places to anti-glare glass for vehicle / electronic product screens, researchers try to realize and endow glass with more functions and applications through the regulation of glass surface microstructure. However, so far, the controllable synthesis of glass surface microstructures requires expensive lithography, etching, nanoimprinting and other technologies to achieve, because the equipment itself is expensive, the follow-up maintenance costs are high, and the shortcomings seriously restrict the special glass with surface microstructures. industrial application. [0003] There are also many problems in the research on ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C03C15/00C03C23/00C09K13/08
CPCC03C15/00C03C23/0075C09K13/08
Inventor 王金磊甘治平李刚金克武杨扬
Owner (CNBM) BENGBU DESIGN & RES INST FOR GLASS IND CO LTD