Application of dendranthema morifolium volatile oil and composition thereof in preparation of product for treating glucose and lipid metabolism comprehensive disorder
A technology of golden silk chrysanthemum and glucose and lipid metabolism, applied in the fields of application, metabolic diseases, drug combination, etc., can solve problems that do not involve hypoglycemic and hypolipidemic activity, component efficacy testing, etc. Achieving low cost, good hypoglycemic and hypolipidemic activity, and favorable preservation effects
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Embodiment 1
[0066] Optimization of a method for extracting volatile oil from Chrysanthemum chrysanthemum:
[0067] Extraction rate of volatile oil from Chrysanthemum chrysanthemum under different conditions in table 1
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[0069]
[0070] It can be known from Table 1 that the extraction rate is higher when the extraction solvent in the volatile oil extractor and post-treatment is ether, and the extraction rate is the highest when the heating temperature of the external bath is 150°C and the extraction time is 9 hours.
Embodiment 2
[0072] A process for extracting the volatile oil of Chrysanthemum chrysanthemum:
[0073] S1 adopts the steam distillation extraction method, weighs a certain amount of Chrysanthemum chrysanthemum flowers and leaves, carries out superfine grinding, transfers them to a round bottom flask, adds deionized water with a material-to-liquid ratio of 1:10, and then adds zeolite to connect the volatile oil Extractor, and add ether in the volatile oil extractor, connect the decompression device on the upper part of the reflux condenser, and connect the reflux condenser to the low-temperature constant temperature circulation condenser for condensation.
[0074] S2 Under reduced pressure, heat the water to boiling, reflux and extract for 3-9 hours, collect the ether layer, extract the water layer twice with ether, combine the ether layers, dry over anhydrous sodium sulfate, and distill off the ether to obtain light yellow gold wire The volatile oil of Huang chrysanthemum flowers and leave...
Embodiment 3
[0078] Liquid-mass spectrometry analysis of the extracted volatile oil of Chrysanthemum chrysanthemum:
[0079] According to the "National Pharmacopoeia of the People's Republic of China 2010 Edition" volatile oil assay method, the chemical composition analysis adopts gas chromatography-mass spectrometry detection (GC-MS) analysis, and the analysis conditions are as follows:
[0080] Detection instrument: American Agilent 5975C+7890A gas chromatography-mass spectrometer.
[0081] Chromatographic conditions: HP-5MS elastic quartz capillary column (0.25μm×30m×0.25mm), the initial temperature of the programmed temperature rise is 40°C, keep for 3min, rise to 160°C at 4°C / min, keep for 3min, and keep at 6°C / min Rise to 280°C, hold for 10min, use high-purity helium (99.99%) as carrier gas, volume flow rate is 1.0mL / min, split ratio is 50:1, and injection volume is 1.0μL.
[0082] Mass spectrometry conditions: electron bombardment (EI) ion source, electron energy 70eV, solvent dela...
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