Hydrophobic waterproof emulsion and preparation method thereof
A waterproof emulsion and hydrophobic technology, which is used in the addition of water repellents, textiles and papermaking, papermaking, etc. It can solve the problems that the water resistance effect cannot be maintained for a long time, the lotus leaf effect without hydrophobicity, and the system stability is poor, and achieves excellent hydrophobic effect. , high stability, simple and easy-to-control process
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Example Embodiment
[0024] Example 1
[0025] This embodiment provides a method of preparing a hydrophobic waterproof emulsion, comprising the steps of:
[0026] (1) 60kg water, 8kg emulsifier (BASF fat alcohol polyoxyether ether sodium sulfate), 11kg natural wax, 10 kg acrylic resin, 6kg palmitic acid (imported first-level acid) into emulsion, heating and 80R / The rotational speed of MIN was stirred to give mixture a;
[0027] (2) 0.5 kg of antifoaming agent (BYK024) was added to the mixture A, and the homogenized machine was emulsified under 80 r / min to obtain a mixture B;
[0028] (3) 0.1 kg of preservatives (OT-45) were added to the mixture B, and the pH to 6 of the emulsified system was adjusted using DMEA and the ternary copolyte, and the hydrophobic emulsion was obtained.
Example Embodiment
[0029] Example 2
[0030] This embodiment provides a method of preparing a hydrophobic waterproof emulsion, comprising the steps of:
[0031] (1) 58kg water, 8kg emulsifier (BASF fatty polyoxyethylene ether sulfate), 10 kg natural wax, 12 kg acrylic resin, 6kg palmitic acid (imported acetal acid) is put into emulsion, heating and 100R / The rotational speed of MIN was stirred to give mixture a;
[0032] (2) 0.8 kg of antifoaming agent (BYK024) was added to the mixture A, and the homogenized machine was emulsified under 100R / min for 2 h, resulting in a mixture B;
[0033] (3) 0.15 kg of preservatives (OT-45) were added to the mixture B, and the pH to 6.5 of the emulsification system was adjusted using DMEA and ternary copolyte, and the hydrophobic emulsion was obtained.
Example Embodiment
[0034] Example 3
[0035] This embodiment provides a method of preparing a hydrophobic waterproof emulsion, comprising the steps of:
[0036] (1) 55kg water, 8kg emulsifier (BASF fat alcohol polyoxyethylene ether sulfate), 9kg natural wax, 15kg acrylic resin, 5kg palmitic acid (imported-level acid) into emulsion, heating and 90R / The rotational speed of MIN was stirred to give mixture a;
[0037] (2) 1 kg of antifoaming agent (BYK024) was added to the mixture A, and the homogenized machine was emulsified under 90r / min to give a mixture B;
[0038] (3) 0.2 kg of preservative (OT-45) was added to the mixture B, and the pH to 7 of the emulsification system was adjusted using DMEA and ternary copolyte, and the hydrophobic emulsion was obtained.
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