Hydrophobic waterproof emulsion and preparation method thereof

A waterproof emulsion and hydrophobic technology, which is used in the addition of water repellents, textiles and papermaking, papermaking, etc. It can solve the problems that the water resistance effect cannot be maintained for a long time, the lotus leaf effect without hydrophobicity, and the system stability is poor, and achieves excellent hydrophobic effect. , high stability, simple and easy-to-control process

Pending Publication Date: 2022-04-12
佛山市桥通新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, most manufacturers currently use polyurethane emulsion, which not only has no hydrophobic lotus leaf effect, but also has poor system stability, and

Method used

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  • Hydrophobic waterproof emulsion and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0024] Example 1

[0025] This embodiment provides a method of preparing a hydrophobic waterproof emulsion, comprising the steps of:

[0026] (1) 60kg water, 8kg emulsifier (BASF fat alcohol polyoxyether ether sodium sulfate), 11kg natural wax, 10 kg acrylic resin, 6kg palmitic acid (imported first-level acid) into emulsion, heating and 80R / The rotational speed of MIN was stirred to give mixture a;

[0027] (2) 0.5 kg of antifoaming agent (BYK024) was added to the mixture A, and the homogenized machine was emulsified under 80 r / min to obtain a mixture B;

[0028] (3) 0.1 kg of preservatives (OT-45) were added to the mixture B, and the pH to 6 of the emulsified system was adjusted using DMEA and the ternary copolyte, and the hydrophobic emulsion was obtained.

Example Embodiment

[0029] Example 2

[0030] This embodiment provides a method of preparing a hydrophobic waterproof emulsion, comprising the steps of:

[0031] (1) 58kg water, 8kg emulsifier (BASF fatty polyoxyethylene ether sulfate), 10 kg natural wax, 12 kg acrylic resin, 6kg palmitic acid (imported acetal acid) is put into emulsion, heating and 100R / The rotational speed of MIN was stirred to give mixture a;

[0032] (2) 0.8 kg of antifoaming agent (BYK024) was added to the mixture A, and the homogenized machine was emulsified under 100R / min for 2 h, resulting in a mixture B;

[0033] (3) 0.15 kg of preservatives (OT-45) were added to the mixture B, and the pH to 6.5 of the emulsification system was adjusted using DMEA and ternary copolyte, and the hydrophobic emulsion was obtained.

Example Embodiment

[0034] Example 3

[0035] This embodiment provides a method of preparing a hydrophobic waterproof emulsion, comprising the steps of:

[0036] (1) 55kg water, 8kg emulsifier (BASF fat alcohol polyoxyethylene ether sulfate), 9kg natural wax, 15kg acrylic resin, 5kg palmitic acid (imported-level acid) into emulsion, heating and 90R / The rotational speed of MIN was stirred to give mixture a;

[0037] (2) 1 kg of antifoaming agent (BYK024) was added to the mixture A, and the homogenized machine was emulsified under 90r / min to give a mixture B;

[0038] (3) 0.2 kg of preservative (OT-45) was added to the mixture B, and the pH to 7 of the emulsification system was adjusted using DMEA and ternary copolyte, and the hydrophobic emulsion was obtained.

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Abstract

The invention relates to a hydrophobic waterproof emulsion and a preparation method thereof. The hydrophobic waterproof emulsion is prepared from the following raw materials in parts by weight: 10-26 parts of acrylic resin, 5-11 parts of beewax, 7-8 parts of an emulsifier, 3-6 parts of palmitic acid, 0.5-1 part of a defoaming agent, 0.1-0.2 part of a preservative and 40-60 parts of water. The hydrophobic waterproof emulsion is scientific and reasonable in component proportion and free of alkylphenol, and the system is low in odor and environmentally friendly. After testing, centrifugation, standing and lotus leaf hydrophobic effects are excellent, and the highest water resistance time can reach more than 7 days. The emulsion is high in stability, can be coated by a coating machine, can also be dip-coated and sprayed, and is suitable for producing corrugated paper, kraft paper, cardboard paper and the like with high hydrophobic and waterproof requirements; the process is simple and easy to control, and large-scale production is facilitated.

Description

technical field [0001] The invention belongs to the field of chemical additives, and in particular relates to a hydrophobic and waterproof emulsion and a preparation method thereof. Background technique [0002] Due to its diverse physical and chemical properties, hydrophobic and waterproof emulsions have been widely and importantly used in many important fields such as water-based coatings, construction, and papermaking, and new application paths have been continuously developed. [0003] However, most manufacturers currently use polyurethane emulsion, which not only has no hydrophobic lotus leaf effect, but also has poor system stability, and the water resistance effect cannot be maintained for a long time. In addition, most of the emulsifiers used are alkylphenols, which are harmful to the environment. [0004] Therefore based on this, propose technical scheme of the present invention. Contents of the invention [0005] In order to solve the problems in the prior art, ...

Claims

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Application Information

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IPC IPC(8): D21H19/20D21H19/18D21H19/14D21H21/16
Inventor 赖长凤韩裕龙
Owner 佛山市桥通新材料有限公司
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