Electrolytic solution used for molybdenum gate screen electrolytic polishing and preparation method and application thereof
An electrolytic polishing and electrolyte technology, applied in the field of electrolyte, can solve problems such as damage to electronic tubes, achieve the effects of reducing the chance of ignition, improving quality, and scientific and reasonable proportioning
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[0029] Example 1
[0030] 1. An electrolyte for electropolishing molybdenum grid, which is composed of the following raw materials:
[0031] 400 ml of phosphoric acid, 150 ml of sulfuric acid, 40 g of nickel sulfate, and 150 ml of water.
[0032] 2. A method for preparing the electrolyte for electropolishing of molybdenum grid described in 1, comprising the following steps:
[0033] Take 150ml of water and pour it into the container, then add 400ml of phosphoric acid, stir well, then slowly add 150ml of sulfuric acid, keep stirring the solution during the process of adding sulfuric acid, and finally add 40g of nickel sulfate, heat to dissolve, and mix well.
[0034] 3. A method for electropolishing molybdenum grid with the electrolyte described in 1, comprising the following steps:
[0035] (1) Take the molybdenum grid and put it into a sodium hydroxide solution with a concentration of 20% and boil for 30 minutes to remove the grease and oxides on the surface of the molybden...
Example Embodiment
[0041] Example 2
[0042] 1. An electrolyte for electropolishing molybdenum grid, which is composed of the following raw materials:
[0043] 450 ml of phosphoric acid, 200 ml of sulfuric acid, 60 g of nickel sulfate, and 200 ml of water.
[0044] 2. A method for preparing the electrolyte for electropolishing of molybdenum grid described in 1, comprising the following steps:
[0045] Take 200ml of water and pour it into the container, then add 450ml of phosphoric acid, stir well, then slowly add 200ml of sulfuric acid, keep stirring the solution during the process of adding sulfuric acid, and finally add 60g of nickel sulfate, heat to dissolve, and mix well.
[0046] 3. A method for electropolishing molybdenum grid with the electrolyte described in 1, comprising the following steps:
[0047] (1) Take the molybdenum grid and put it into a sodium hydroxide solution with a concentration of 30% and boil for 40 minutes to remove the grease and oxides on the surface of the molybdenum...
Example Embodiment
[0053] Example 3
[0054] 1. An electrolyte for electropolishing molybdenum grid, which is composed of the following raw materials:
[0055] 400 ml of phosphoric acid, 180 ml of sulfuric acid, 50 g of nickel sulfate, and 160 ml of water.
[0056] 2. A method for preparing the electrolyte for electropolishing of molybdenum grid described in 1, comprising the following steps:
[0057] Take 160ml of water and pour it into the container, then add 400ml of phosphoric acid, stir well, then slowly add 180ml of sulfuric acid, keep stirring the solution during the process of adding sulfuric acid, and finally add 50g of nickel sulfate, heat to dissolve, and mix well.
[0058] 3. A method for electropolishing molybdenum grid with the electrolyte described in 1, comprising the following steps:
[0059] (1) Take the molybdenum grid and put it into a sodium hydroxide solution with a concentration of 20% and boil for 35 minutes to remove the grease and oxides on the surface of the molybden...
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