Toner composition
A composition and toner technology, applied in the direction of developer, instrument, electric recording process applying charge pattern, etc., can solve problems such as not yet applied
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[0058] Preparation of unsaturated resin A
[0059] In a 1 liter Parr reactor equipped with a mechanical twin-turbine stirrer, a distillation unit, and a bottom discharge valve, dimethyl terephthalate (263 g), fumaric acid (27.75 g), 5-sulfo-meta Sodium salt of dimethyl phthalate (38.5g), 1,2-propanediol (243g), diethylene glycol (36.3g), N-phenyldiethanolamine (2.9g), fascat 4100 (1g) and p-phenylene Diphenol (0.2 g). The reactor was heated to about 140° C. under a carbon dioxide purge (to prevent crosslinking), where the solids melted. Turn the stirrer to about 100 rpm. The reactor was then warmed to 165°C over 20 min, where the methanol / water by-product started to distill out. The temperature was then slowly raised to 190° C. over 3 hours, and the stirring speed was increased to 200 rpm. The reaction mixture was then warmed to 200 °C and the pressure was slowly decreased from atmospheric pressure to about 1 Torr over 2 hours and then maintained at this condition for an ...
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