782 results about "Melamine formaldehyde" patented technology

A perfume encapsulate comprises an aminoplast capsule, the capsule shell comprising urea-formaldehyde or melamine-formaldehyde polymer and a second polymer comprising a polymer or copolymer of one or more anhydrides, preferably ethylene/maleic anhydride copolymer. The second polymer improves the stability of the capsules with respect to surfactant, thus improving perfume retention properties and enabling use of the capsules in aqueous surfactant-containing products in a way that has not hitherto been possible.

Described is a method for freshening fabric articles by means of spraying the articles with an aqueous slurry of microcapsules having rupturable melamine-formaldehyde polymeric walls, containing substantive and efficacious functional substances, e.g., malodour counteractants and/or fragrances. The slurry may optionally contain non-confined functional substances, e.g. malodour counteractants and/or fragrances. The method is effective for the deposition of effectively-rupturable malodour suppressant and/or fragrance emitting microcapsules onto fabrics wherein the resulting emitted fragrance activity and/or malodour counteractant activity is long-lasting and where the resulting substantive aroma is aesthetically pleasing over the long period of time for which it is effective. Also described are efficacious and substantive malodour counteractant compositions useful for the aforementioned process containing a malodour composition composed of zinc ricinoleate and at least one of: 1-cyclohexylethan-1-yl butyrate; 1-cyclohexylethan-1-yl acetate; 1-cyclohexylethan-1-ol; 1-(4′-methylethyl)cyclohexylethan-1-yl propionate; and/or 2′-hydroxy-1′-ethyl(2-phenoxy)acetate. In addition, described are efficacious microcapsule slurries useful for the aforementioned process containing microcapsules having melamine-formaldehyde polymeric capsule walls with the microcapsules being in contact with one or more polymeric silicone phospholipids.

The invention discloses a high-flexibility melamino-formaldehyde foam material and a preparation method thereof. The preparation method comprises: firstly, preparing melamino-formaldehyde prepolymer modified by polyol into aqueous solution with definite weight concentration; weighting 100 parts by weight of prepolymer aqueous solution; adding 0-15 parts by weight of surfactant, 1-20 parts by weight of foaming agent, 0-10 parts by weight of accelerator and 0-10 parts by weight of curing agent to be fully stirred and mixed to prepare foaming liquid; filling foaming liquid into a microwave chemical reactor or a high-temperature oven; and foaming for 30s-15min at the temperature of 100-300 DEG C to prepare the foam material. The melamino-formaldehyde foam material disclosed by the invention solves the problems of big brittleness, poor flexibility, easy duslting of foam, complex preparation technology, high production cost and the like of the existing melamino-formaldehyde foam material and has wide application prospect.

A warm-mix asphalt additive machine preparation method, the additive is formed by reacting the following components in parts by weight: 4-15 parts of alkoxysilane, 1-8 parts of polyether, 0-1 part of melamine formaldehyde resin, and 0 parts of acid catalyst -1 part, 0-1 part of alkali catalyst, 2-10 parts of deionized water, 30-100 parts of solvent; the preparation method comprises the following steps: (1) adding a quantitative amount of solvent and Alkoxysilane, heated to 80°C; (2) Add a mixture of acid catalyst, base catalyst, and deionized water, and react at a constant temperature of 80°C for 90 minutes; (3) Heat up to 100°C, condense and reflux for 120 minutes, and collect about 55ml of distillate; ( 4) Add an acid catalyst and a certain amount of polyether into the flask, heat up the esterification reaction for 180 minutes; (5) evacuate, condense and reflux for 30 minutes, cool down to room temperature, add a certain amount of melamine formaldehyde resin and stir evenly, add an appropriate amount of alkali catalyst to adjust the pH = 8 or so, the finished product is obtained.

A liquid crystal material containing polymer network forming material is microencapsulated by a method utilizing an interfacial polymerization which creates a combination of polyurethane and polyurea polymers or melamine fromaldehyde or urea formaldehyde polymer which form the capsule walls surrounding the discrete liquid crystal droplets. The prepolymer of urethane acrylate and acrylate within the liquid crystal capsules is cured under UV light irradiation to form a web-like structure and induce the formation of polydomain configuration of nematic director. This allows to produce the display having faster switching property and showing significant lower threshold voltage.

A thin drywall board that includes a gel coat, at least one polymer/gypsum layer, and a wet glass fiber layer is provided. The gel coat is formed of a gel coat composition that includes a water dispersible polymer, gypsum, and optionally a crosslinking agent and/or a coupling agent. The polymer/gypsum layer is formed of a matrix composition that includes a water dispersible polymeric resin and gypsum. Components including melamine formaldehyde, a filler material, coupling agents, acetic acid, an accelerator, and/or a hardener may also be added to the matrix composition. The wet glass fiber layer is preferably a glass fiber mat. The combination of the water dispersible polymeric resin and the gypsum in the matrix composition have a synergistic effect that creates a thin drywall board that is water resistant, fire resistant, and has improved mechanical properties. A method of forming the inventive thin drywall boards is also provided.

The invention discloses a three-source integrated microcapsule intumescent flame retardant and a preparation method thereof. The flame retardant integrates an acid source, a carbon source and a gas source; and the preparation method comprises the following steps of: reacting polyethylene glycol, melamine, aqueous solution of formaldehyde, a promoter with distilled water to prepare polyethylene glycol modified melamine-formaldehyde prepolymer; suspending ammonium polyphosphate powder particles in a dispersing agent; and adding the prepolymer and a hardener to finally obtain the three-source integrated microcapsule intumescent flame retardant powder particles. The flame retardant has good compatibility, flame retardancy and waterproofness.

The present invention discloses a preparation method for melamine formaldehyde resin closed-cell foam. The preparation method comprises the following steps: introducing a modifier to a melamine formaldehyde resin synthesis process to carry out copolymerization, and carrying out a dehydration treatment on the synthesized resin to obtain a modified melamine formaldehyde solid resin with a solid content of more than 85%; adding a viscosity adjusting agent, dissolving the solid resin, respectively adding a curing agent, a foam stabilizer, an emulsifier and a foaming agent, and uniformly stirring; placing the resulting mixture in an oven or a microwave oven to carry out foaming to achieve a predetermined density; and placing the resulting material in the oven or the microwave oven to carry out aging to obtain the melamine formaldehyde foam with a closed-cell rate of more than 90%. The melamine formaldehyde resin closed-cell foam produced by the preparation method has excellent mechanical strength and flame retardant property, and can be applicable for building exterior wall thermal insulation.

A suspension of microcapsules in an organic liquid, the microcapsules containing an aqueous phase, is produced by interfacial polymerization in the presence of a proton transfer catalyst of a water-in-oil emulsion in which the aqueous phase contains a urea/formaldehyde or melamine/formaldehyde prepolymer.

A process for the microencapsulation of phase transitional paraffin compounds is described. Polypropylene glycols with the average molecule weight over 400 were used as the surface tension modifiers for emulsifying the paraffin compounds. Polyisocyanates capable of being dissolved in the phase change materials were employed to promote the deposition of melamine, partially methylolated melamine and the precondensate of melamine-formaldehyde onto the hydrophobic droplets for the microencapsulation. The prepared emulsion of microencapsulated phase change materials was successfully coated on textile fabrics and the coated products showed improved thermal regulation function.

The invention relates to a halogen-free flame retardant polyurethane elastomer flame retardant and the preparation method. The flame retardant comprises the following components and contents (weight per cent): melamine-formaldehyde coating ammonium phosphate 30 per cent to 70 per cent, triethylol isocyanurate 10 per cent to 35 per cent, melamine cyanurate 5 per cent to 20 per cent, phosphonate 10 per cent to 20 per cent, organic silane coupling agent 0.1 per cent to 0.5 per cent and antioxidant 0.1 per cent to 0.8 per cent. The preparation method of the flame retardant comprises the process steps such as the mixture of the melamine-formaldehyde coating ammonium phosphate. Compared with the prior art, the invention overcomes the defect of harm of halogen flame retardant polyurethane elastomer on the environment and the human body, endows the materials with certain difficult-flammability, has good compatibility with the polyurethane and has no effect on the mechanical properties of the polyurethane.

A process for production of an abrasive foam based on a melamine-formaldehyde condensate comprising inorganic nanoparticles, comprising the steps of:

• • (1) preparation of a solution or dispersion comprising a precondensate of the foam to be produced, and also comprising inorganic nanoparticles,
  • (2) foaming of the precondensate via heating of the solution or dispersion from step (1), in order to obtain a foam which comprises inorganic nanoparticles, and also, if appropriate,
  • (3) heat-conditioning of the foam obtained in step (2),

leads to improved abrasion in the polishing of delicate surfaces.

A composition useful in paper and board making comprises a carboxylated surface size containing at least 40 mole percent of hydrophobic groups and at least about 25 mole percent of carboxylated groups such as styrene-(meth)acrylic aicd copolymers or styrene-maleic acid (anhydride or salt) copolymers, a hydrophilic polyacrylamide and a crosslinking agent such as glyoxylated vinylamide polymers, formaldehyde, melamine-formaldehyde condensates and glyoxyl-extended materials.

A fire blocking non-woven needle-punched textile structure, comprising a first fiber component containing polyacrylonitrile copolymer with a halogen containing monomer, a second fiber component comprising a viscose fiber containing silicic acid or a regenerated cellulose fiber and a third fiber component comprising an aramid fiber or a melamine/formaldehyde fiber or a polyester fiber.

The invention provides an encapsulate comprising a benefit agent core (preferably containing perfume), one or more inner shells (preferably of melamine urea or melamine formaldehyde) and an outer shell comprising a polymer (for example locust bean gum, tamarind xyloglucan, guar gum or mixtures thereof) which is substantive to cellulose (preferably in the form of cotton), at least one of said shells being impermeable to the benefit agent.

Adhesive and sealant systems Adhesive and sealant systems on the basis of unsaturated polyester resins, epoxy resins, polyurethane, silane-terminated polymers, vinyl ester resins, acrylates, polyvinyl acetate, polyvinyl alcohol, polyvinyl ethers, ethylene-vinyl acetate, ethylene-acrylic acid copolymers, polyvinyl acetates, polystyrene, polyvinyl chloride, styrene-butadiene rubber, chloroprene rubber, nitrile rubber, butyl rubber, polysulphide, polyethylene, polypropylene, fluorinated hydrocarbons, polyamides, saturated polyesters and copolyesters, phenol-formaldehyde resins, cresol-/resorcinol-formaldehyde resins, urea-formaldehyde resins, melamine-formaldehyde resins, polyimides, polybenzimidazoles or polysulphones and containing 1% to 15% by weight of a hydrophilic fumed silica structurally modified by grinding.

The invention relates to a method for manufacturing surface wear-resisting impregnated paper of a laminate floor by dry-spraying Al2O3. The method comprises the following steps: impregnating pure wood pulp roll paper with a melamine-formaldehyde (MF) resin liquid; uniformly spraying the Al2O3 on the surface of the impregnated paper by utilizing a dry sprayer; allowing the impregnated and sprayed paper to enter a first oven for drying at the temperature of 100-150 DEG C; roll-coating 300-500% (relative to the weight of the paper) of the MF resin liquid on the paper surface after preliminary drying; and allowing the roll-coated paper to enter a second oven for drying at the temperature of 100-150 DEG C, controlling the whole-course running speed of the paper at 10-12m/minute, cooling, adjusting the temperature of the oven and machine speed so as to reach 6.0-7.5% of volatile matters and 40-60% of pre-curing degree, cutting and packaging. By means of the method, the defects of the prior art are overcome, and the spray quantity of the Al2O3 can be adjusted by controlling the dry sprayer so as to obtain the surface wear-resisting impregnated paper with reliable quality according to different wear-resisting requirements; and the method has the advantages of reasonable process and obvious effect, and is simple in operation, thus effectively improving the product quality.

The present invention discloses a reversible thermochromic microcapsule pigment preparation method, which comprises: weighing 0.08-0.1% by mass of crystal violet lactone, 0.4-0.5% by mass of bisphenol A, 3-6% by mass of hexadecanol, 2-4% by mass of melamine, 4.03-5% by mass of a formaldehyde solution, 0.4-0.6% by mass of sodium dodecyl benzene sulfonate, 0.09-0.11% by mass of sodium dodecyl sulfate ammonium, and 87-90% by mass of distilled water, preparing a complex A, preparing an O/W type emulsion and a melamine-formaldehyde pre-polymerization liquid, and carrying out a condensation polymerization reaction to prepare the pigment. According to the present invention, advantages of high color change sensitivity, low color change temperature and good color change stability are provided when the prepared monomer thermochromic material is adopted as the pigment, and the prepared reversible thermochromic microcapsule pigment can be widely used in the fields of anti-counterfeiting inks, temperature showing materials, and the like.

The invention provides a method for preparing a double-wall self-repairing microcapsule by compounding an epoxy resin or a mixture of epoxy resins and carbon nanotubes as an inner capsule core repairing agent and using a curing agent as an outer capsule core. The invention belongs to the field of organic compound materials. The method comprises the following steps: intensely stirring and ultrasonically dispersing the epoxy resin or the mixture of epoxy resins and carbon nanotubes under the action of an emulsifier, so as to form an epoxy resin emulsion or an epoxy resin carbon nanotube emulsion; after preparing a melamine formaldehyde pre-polymer solution, preparing a single-wall microcapsule by using the melamine formaldehyde pre-polymer solution together with the epoxy resin emulsion or the epoxy resin carbon nanotube emulsion under an acid condition; after preparing a curing agent emulsion, stirring the curing agent emulsion and the single-wall microcapsule under an acid environment, thereby leading the curing agent grains to be uniformly attached on the periphery of the single-wall microcapsule; and then generating a second capsule wall layer by adding the melamine formaldehydepre-polymer solution. The prepared microcapsule contains the enhancing repairing agent and the curing agent, which can further enhance the repairing effect of the microcapsule and increase the mechanical property.

The invention discloses a nano composite modified melamine-formaldehyde abrasion-resisting resin and a preparation method thereof. The resin is mainly prepared from a mixture of nano alumina and nano silica, melamine, water, formaldehyde, a stabilizer and an alcohol substance by process steps of mixing, warming polycondensation and cooling discharging. The production method of the modified melamine-formaldehyde abrasion-resisting resin prepared by using the method is very simple and product property is stable; and decorative paper impregnated with the resin still remains the patterns of the surface of the original paper. The resin can be used for the production of impregnated glue film paper facing artificial boards and impregnated paper laminated wood floors, and the wear resistance of the resin reaches 4000 turns.

The invention discloses high-glowing filament anti-soaking separate-out-free halogen-free inflaming retarding polypropylene materials which comprise the following components: by weight, 40-80 parts of polypropylene (PP) resins, 20-40 parts of compound halogen-free flame retarding agents, 0.5-5 parts of flame retardant synergists, 0-30 parts of inorganic fillers, 0.1-0.5 part of antioxidants, and 0.4-1 part of lubricating agents. The compound halogen-free flame retarding agents are composed of the following components: by weight, 30-50 parts of silane-wrapped organic or inorganic hypophosphite, 35-50 parts of melamine formaldehyde resin (MF)-wrapped halogen-free organic phosphate ester or the ramification thereof, and 15-40 parts of melamine cyanuric acid ester. The compound halogen-free flame retarding agents are easy to disperse in the process of processing, so that processing is convenient. The halogen-free inflaming retarding polypropylene materials prepared by the method have high-glow filaments, and have the advantages of being anti-soaking, separate-out-free and the like. In addition, the production process is simple, so that industrial production can be achieved.

The invention discloses a preparing method of globular char gas gel, which comprises the following steps: making phenol- melamine-formaldehyde or water soluble phenol resin- melamine-formaldehyde as raw material; forming colloidal sols through pre-polymerization; adding into discontinuous phase with surface activator; forming floating system under the function of stirring; generating colloidal sols- gel transition at 60-85 deg.c; forming globular aquagel; proceeding organic solvent replace and hypercritical dry; getting organic aerogel; proceeding high temperature degradation; getting globular char gas gel; setting the specific surface area at 400-1000m2/g, bore diameter at 3-20 nanometer and ball calipers at 0.01-3 millimeter.