Resin solution for preparing melamine formaldehyde resin foam plastics and preparation method thereof
A technology of melamine and formaldehyde resin, which is applied in the field of resin solutions, can solve the problems of short pot life, gelation, and only 4-5 hours of resin, and achieve excellent mechanical properties, convenient preparation, and good storage stability.
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Embodiment 1
[0031] Preparation of MF resin solution:
[0032] Add 400g of formaldehyde solution with a weight concentration of 37% into a 1000ml three-necked reaction flask equipped with a condenser, a stirrer and a thermometer, adjust the pH value to 8.0 with a weight concentration of 10% sodium hydroxide solution, and then add 250g of melamine to the reaction In the bottle, heated to 78°C, reacted for 2 hours, cooled to 50°C, added 20g of sodium citrate, stirred evenly, and obtained MF resin solution, the viscosity of the solution changed with time is shown in Table 1.
Embodiment 2
[0034] Add 400g of 37% formaldehyde solution into a 1000ml three-necked reaction flask equipped with a condenser, agitator and thermometer, adjust the pH value to 9.5 with sodium hydroxide solution, then add 250g of melamine into the reaction flask, heat to 83°C, After reacting for 2.5 hours, cool to 50° C., add 25 g of sodium borate, and stir evenly to obtain a MF resin solution. See Table 1 for the viscosity of the solution over time.
Embodiment 3
[0041] In the embodiments, the consumption of each material is the weight consumption.
[0042] Preparation of melamine foam:
[0043] The above-mentioned MF resin solution is mixed with relevant foaming aids to make a foamed MF resin solution, and foamed in a microwave foaming device. The foaming formula and the properties of the foam are shown in Table 2.
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