Method of preparing synthetic rutile from ore type ilmenite concentrate

A technology of artificial rutile and ilmenite concentrate, applied in the direction of titanium dioxide, titanium oxide/hydroxide, etc., can solve the problems of difficult reduction technology, existing rotary kiln ring formation, long corrosion time, etc., to eliminate hidden dangers of ring formation, The effect of ensuring quality and reducing the reduction temperature

A technology of artificial rutile and ilmenite concentrate, applied in the direction of titanium dioxide, titanium oxide/hydroxide, etc., can solve the problems of difficult reduction technology, existing rotary kiln ring formation, long corrosion time, etc., to eliminate hidden dangers of ring formation, The effect of ensuring quality and reducing the reduction temperature

CN1923703AInactive Publication Date: 2007-03-07CENT SOUTH UNIV

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  • Method of preparing synthetic rutile from ore type ilmenite concentrate

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Embodiment Construction

[0016] 1: Rock ore type ilmenite concentrate (TiO 2 47.16%, TFe31.47%) with additive pelletizing. The additive sodium humate is added in an amount of 1.5%. After the raw balls are dried and preheated by the grate machine, they enter the rotary kiln for reduction. The drying and preheating system of the chain grate machine is as follows: the material height is 200mm, the air temperature in the blast drying section is 200°C, the wind speed is 1.0m / s, and the time is 2min. The air temperature in the section is 250°C, the wind speed is 1.0m / s, and the time is 5min. The air temperature in the preheating section is 800-950°C, the wind speed is 1.2m / s, and the time is 12min; , the reduction time is 150min, the C / Fe ratio is 0.8, and the metallization rate of the obtained reduced ilmenite is 93.78%. The reduced ilmenite ore is crushed and ground, and the grinding particle size is controlled at -1mm to account for 100%, and then the rust separation treatment is carried out. The rust...

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Abstract

The invention discloses an artificial rutile preparing method through rock ilmenite concentrate, which comprises the following steps: preheating rock ilmenite concentrate in the rotary kiln to reduce directly; separating the corrosion of reduced ilmenite; immersing material with titanium in the diluted acid to remove impurity to prepare the artificial rutile.

Description

technical field [0001] The invention belongs to the field of metallurgical engineering, and relates to a method for preparing artificial rutile by using a rock ore type ilmenite concentrate as a raw material and adopting a reduction-corrosion method. Background technique [0002] At present, the world's titanium resources that can be used for titanium industrial production are mainly natural rutile and ilmenite. However, the reserves of natural rutile concentrate are small, and ilmenite with abundant reserves has become the main raw material for the titanium industry. In nature, ilmenite is divided into two types: rock ore and placer, among which rock ore is the majority. The ilmenite concentrate selected from rock ore and placer can be directly used to produce metal titanium and titanium dioxide, but because of its low grade, it generally needs to be enriched into high-grade titanium-rich material-titanium slag or artificial rutile , and then used in the production of tit...

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Application Information

Patent Timeline
07 Mar 2007
Publication
CN1923703A
IPC
C01G23/047
Inventors
邱冠周; 姜涛