Unlock instant, AI-driven research and patent intelligence for your innovation.

Method and apparatus for obtaining heavy oil samples from a reservoir sample

The mechanical extraction apparatus efficiently extracts unaltered bitumen or heavy oil samples using a cylinder and piston assembly with a filter, addressing the inefficiencies of existing methods by enabling rapid, high-quality sample collection for viscosity and chemical analysis, thus supporting informed drilling and production decisions.

Inactive Publication Date: 2013-11-28
GUSHOR
View PDF1 Cites 3 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

The method provides high-quality, sediment- and water-free oil samples that can be analyzed quickly, assisting in timely drilling and production decisions, with improved retention of low boiling components and reduced costs compared to existing techniques.

Problems solved by technology

However, recovery of oil from HOTS reservoirs is generally difficult due to the high viscosity and poor mobility of oil, difficult production and high fluid property heterogeneity in reservoirs.
Ideally, however, the viscosity should be measured directly on a live oil sample that contains the in situ gas content of the reservoir sample, which is mostly not possible due to limitations of the methods by which oil or bitumen is extracted from samples and by which viscosity measured.
Usually, solvents cannot be completely removed without losing some of the low molecular weight petroleum components within the bitumen.
Thus, viscosity measurements on solvent extracted bitumen are considered unreliable with existing procedures.
However, this method proceeds slowly due to the high viscosity of the petroleum in many samples and cannot be performed easily or quickly enough at the well-site.
Moreover, even if time is available in a laboratory the expense of engineering-rated centrifuges raises costs dramatically.
In addition, large quantities of reservoir rock (>0.5 kg or equivalent to a minimum of 30 to 50 cm lengths of slabbed 4″ core) are usually required to acquire adequate samples for fluid property determinations, which is both destructive and difficult to handle.
These techniques are both time-consuming and expensive or ineffective as often insufficient liquid samples are obtained for subsequent physical property testing.
At present, these slow mechanical laboratory petroleum recovery processes are a bottleneck in most bitumen or very heavy oil production planning operations.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

example 1

Sample Preparation and Procedure

[0091]Bitumen or heavy oil reservoir rocks (containing approximately 5-15 wt % bitumen and having up to 40% porosity) can be mechanically extracted in a single operation. Typically, about 150 to 200 g of lightly disaggregated oil sand sample (oil sand disaggregated while frozen in a mortar and pestle for 5 minutes) is placed in the extraction cylinder (1) to produce between 1 and 10 ml of heavy oil. The amount of sample used depends on the bitumen and heavy oil richness of the sample and the amount of oil required for analysis. For example, a low oil-saturation or low porosity sample would necessitate a larger sample size to ensure that the required liquid oil volume could be extracted.

[0092]While water addition to the sample is not necessary with frozen wet core samples, the addition of an amount of water (up to 20 volume percent) to the top of the samples can increase the amount of oil recovered by the procedure, particularly from dried out samples....

example 2

Water Extraction

[0093]1. Load an appropriate amount of crushed reservoir sample into the cylinder.

[0094]2. Position the piston above the top of the cylinder.

[0095]3. Place a water collection vial below within the collection chamber of the ME device.

[0096]4. Turn on the heating system to pre-heat (typically 40° C. to 80° C.) the device for approximately 10 minutes.

[0097]5. Position the piston at the top of the sample so that it is just in contact with the sample, applying minimal force to the sample. At this point, between about 1 and 10 ml of water will quickly flow into the water collection vial if water has been added to the sample. The piston should be held at this position for several minutes.

[0098]6. Increase the load applied by the press to approximately 25 MPa and hold for several minutes. Additional water will flow out if water has been added, otherwise for unwetted native samples only drops of water may be collected.

[0099]7. The water sample may be large enough for detailed...

example 3

Oil Extraction

[0100]The following description relates to an example of one set of conditions that may be applied to extract oil samples from a typical western Canadian tar sand (oil sand) reservoir sample of high porosity.

[0101]1. Replace the water collection vial with an oil collection vial that has been weighed.

[0102]2. Increase the applied load of the press to about 50 MPa (absolute stress) and hold for 5 minutes. Oil may start dripping into the collection vial at this pressure for rich samples and / or samples containing less viscous oil.

[0103]3. Increase the applied load of the press to 75 MPa (absolute stress) and hold for a time interval longer than that in Step 2 (for example, 10 minutes). Increase the applied load of the press to 100 MPa (absolute) and hold for a time interval exceeding that of Step 3 (for example, 15 minutes).

[0104]4. Increase the applied load of the press to 25 tons (125 MPa) and hold for a time interval greater than that of Step 4 (for example, 15 minutes)...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
pore sizeaaaaaaaaaa
pressureaaaaaaaaaa
lengthaaaaaaaaaa
Login to View More

Abstract

The invention relates to an apparatus and method to obtain a bitumen or heavy oil sample from an oil reservoir sample, such as a core sample, to enable measurement of physical properties such as viscosity, API gravity, or chemical properties such as sulphur content of the obtained bitumen or heavy oil sample. The analyses performed on the samples obtained in accordance with the invention are effective in assisting oil field operators in making timely drilling and production decisions at the oil reservoir or for routine laboratory extraction of oils and bitumens. The invention also permits the collection of samples from simulated thermal recovery operations and also allows the collection of bitumens and oils for online analysis of live oil physical properties.

Description

FIELD OF THE INVENTION[0001]The present invention relates generally to an apparatus and method to obtain a bitumen or heavy oil sample from an oil reservoir sample, such as a core or drill cuttings sample.BACKGROUND OF THE INVENTION[0002]As the world's conventional oil reserves are being consumed, Heavy Oil and Tar Sands (HOTS) reservoirs are becoming increasingly important as a source of petroleum fluids. However, recovery of oil from HOTS reservoirs is generally difficult due to the high viscosity and poor mobility of oil, difficult production and high fluid property heterogeneity in reservoirs. Of the world's petroleum reserves (6 trillion barrels), most exists as heavy oil or oil sand (tar sand) bitumen. Currently, only an average of 17% of this oil can be recovered.[0003]In high porosity and permeability reservoirs, development strategy and production depends on fluid mobility, of which oil viscosity is a major controlling factor. Thus, assessing viscosity of oil throughout HOT...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(United States)
IPC IPC(8): G01N1/10
CPCG01N1/10G01N1/34G01N33/26G01N2001/4088C10G2300/202C10G2300/302C10G2300/308
Owner GUSHOR