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A high-pressure solid iron phosphate sodium pyrophosphate cathode material, its preparation method and application

PendingCN122276701AWill not destroy uniformityDoes not destroy activityPyrophosphateSlurry
This invention provides a high-pressure compacted sodium iron pyrophosphate cathode material, its preparation method, and its application. The preparation method of the high-pressure compacted sodium iron pyrophosphate cathode material includes: weighing sodium, iron, and phosphorus sources according to the stoichiometric ratio of sodium iron pyrophosphate, adding carbon source and solvent, and mixing and grinding to obtain a precursor slurry; spray drying the precursor slurry to obtain precursor powder; compacting and granulating the precursor powder under a pressure of 10 MPa to 80 MPa to obtain denser precursor particles; and finally sintering at 500℃ to 650℃ for 6 to 15 hours under an inert atmosphere. This invention effectively eliminates internal cavities and interparticle gaps in the precursor through compaction and granulation, and controls the pressure within the range of 10 MPa to 80 MPa. The subsequent sintering process improves the density of the cathode material while controlling the impurity phase content to below 1 wt% and maintaining good electrochemical performance.
Owner:GEM WUXI ENERGY MATERIAL CO LTD