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50 results about "Iron pyrophosphate" patented technology

Ferric Pyrophosphate. In the US, Ferric Pyrophosphate (ferric pyrophosphate systemic) is a member of the drug class iron products and is used to treat Anemia Associated with Chronic Renal Failure.

Method for preparing lithium iron phosphate and lithium iron pyrophosphate by taking mineral leaching tail liquor as iron source

The invention discloses a method for preparing lithium iron phosphate and lithium iron pyrophosphate by taking mineral leaching tail liquor as an iron source. The method comprises the following steps: spraying a phosphate or pyrophosphate solution into the mineral leaching tail liquor, adding an organic flocculant after complete precipitation, and dehydrating and drying the precipitate to obtain ferric phosphate or ferric pyrophosphate; uniformly mixing ferric phosphate with lithium formate, or lithium acetate, or lithium oxalate, grinding the mixture, heating the ground mixture in a protective atmosphere, and cooling to obtain lithium iron phosphate or lithium iron pyrophosphate; and uniformly mixing ferric pyrophosphate with sodium pyrophosphate and lithium formate, or lithium acetate, or lithium oxalate, grinding the mixture, drying the ground mixture in a drying oven, heating the dried mixture in a protective atmosphere, cooling to the room temperature, leaching, and drying to obtain lithium iron pyrophosphate. The method realizes recycling of dissolved iron while achieving harmless disposal of mineral leaching tail liquor, and the prepared lithium iron phosphate and lithium iron pyrophosphate are easy for precipitation and recovery, are materials for manufacturing zincodes, are not cheap and have a wide market prospect.
Owner:ZHEJIANG UNIV

Electric calcination furnace and application of electric calcination furnace in preparing industrial-grade phosphoric acid

The invention relates to the field of production devices of industrial-grade phosphoric acid, in particular to an electric calcination furnace adopted in the process for producing industrial-grade phosphoric acid by using low-grade phosphate rock. A specific application method of the electric calcination furnace adopted in the process of preparing the industrial-grade phosphoric acid comprises the steps as follows: firstly, the temperature inside the furnace is set to be 100 DEG C, then a rotating tube is started and preheated for one hour, the temperature inside the furnace is heated to 250 DEG C, and the rotating tube is preheated for half an hour again; and materials are uniformly fed, solid materials are directly rolled into a hydrolyzing barrel, gaseous materials enter a fluorine recycling barrel from six gas collecting pipes at the top, pyrophosphoric acid and iron-aluminum oxides are solidified after the materials are calcinated, the spilt gas is hydrogen fluoride, and the temperature is controlled to be 100 DEG C during discharging. The electric calcination furnace is adopted for preparing the industrial-grade phosphoric acid and is low in energy consumption, simple in process, easy to operate, low in cost and capable of effectively saving energy.
Owner:SICHUAN SHANGZHOU IND

Ferric pyrophosphate citrate mixed complex preparation method

The invention discloses a ferric pyrophosphate citrate mixed complex preparation method, which comprises: (1) preparing an aqueous solution containing trivalent iron cations; (2) respectively preparing an aqueous solution containing citric acid anions and an aqueous solution containing pyrophosphoric acid anions, slowly adding the aqueous solution containing pyrophosphoric acid anions into the aqueous solution containing citric acid anions in a dropwise manner, and uniformly stirring and mixing to obtain a mixed aqueous solution; (3) slowly adding the aqueous solution prepared in the step (1) into the mixed aqueous solution prepared in the step (2) while stirring, carrying out a stirring reaction for 1-2 h after completing the adding to obtain a dark green solution, filtering out insoluble matters, and taking the filtrate; and (4) adding the filtrate obtained in the step (3) into a crystallization solvent in a dropwise manner, continuously stirring for 1-2 h after completing the adding to obtain a slight green precipitate, filtering, and drying the obtained solid so as to obtain the ferric pyrophosphate citrate mixed complex. According to the present invention, with the preparation method, the high-yield phosphate-radical-free ferric pyrophosphate citrate having the low organic impurity content can be stably obtained.
Owner:SHANDONG CHENGCHUANG BLUE OCEAN PHARM TECH CO LTD

High-temperature-resistant and corrosion-resistant paint for instrument shell, and preparation method thereof

The invention discloses a high-temperature-resistant and corrosion-resistant paint. The high-temperature-resistant and corrosion-resistant paint is characterized by comprising the following raw materials in parts by weight: 30 to 35 parts of cyanamide resin, 1 to 2 parts of ferric pyrophosphate, 5 to 6 parts of iron oxide red, 2 to 4 parts of glycolic acid, 3 to 5 parts of glass flake, 5 to 8 parts of polycarbonate, 3 to 5 parts of silicon-aluminum oxide powder, 2 to 3 parts of epoxidized soybean oil, 12 to 16 parts of rosin cis-butenedioic acid glyceride, 1 to 2 parts of coconut oil diethanolamine, 0.5 to 1.0 part of ozocerite oxide, 0.5 to 1.0 part of dicumyl peroxide, 0.5 to 0.7 part of fumed silica, 3 to 4 parts of aluminum dihydrogen tripolyphosphate, 2 to 4 parts of quartz powder, 7 to 9 parts of acetone, 12 to 16 parts of butyl acetate and 4 to 7 parts of an additive. Aluminum dihydrogen tripolyphosphate added into the paint disclosed by the invention has high corrosion resistance and high high-temperature resistance; the glass flake serving as a filler is added into the paint, so that the paint has high chemical resistance, high anti-aging resistance, high cohesiveness and high corrosion resistance; the added additive promotes the uniform dispersion of the filler in the paint; moreover, damping and noise reducing functions to some extent are also realized, and the damage of noises to human bodies is weakened.
Owner:王小波

A method for synthesizing carbon-coated lithium iron pyrophosphate by hydrothermal method

The invention discloses a method for synthesizing carbon-coated lithium ferrous pyrophosphate by a hydrothermal method. The method comprises the following steps of (1) weighing raw materials, dissolving a carbon source into distilled water or deionized water, and heating, stirring and dissolving in a water bath at the temperature of 50-90 DEG C; respectively dissolving a lithium source, an iron source and a phosphorus source into the deionized water, uniformly stirring the sources, sequentially adding the iron source and the lithium source into a solution dissolved with the carbon source, adding ammonia water to adjust the pH of the mixed solution to 4-6, adding the phosphorus source, heating the mixed solution in the water bath at the temperature of 50-90 DEG C, and stirring for 1-2 hours; (2) performing reaction on the mixed solution at 150-350 DEG C and the pressure of 1-10MPa for 3-10 hours, cooling to room temperature after the reaction is finished, and performing solid-liquid separation to obtain a solid which is a precursor solid-phase product; (3) drying the precursor solid-phase product, and then sintering to obtain the carbon-coated lithium ferrous pyrophosphate. The method has the advantage that the reaction temperature is relatively low, and the synthesis method is simple; the prepared carbon-coated lithium ferrous pyrophosphate serving as a positive electrode material is excellent in electrochemical performance.
Owner:CENT SOUTH UNIV

Preparation method of sodium ferric pyrophosphate electrode material coated with metal oxide, product and application of sodium ferric pyrophosphate electrode material

The invention relates to a preparation method of a metallic oxide coated sodium ferric pyrophosphate electrode material, a product and application thereof, and belongs to the technical field of electrode material preparation. The metallic oxide-coated sodium ferric pyrophosphate electrode material comprises sodium ferric pyrophosphate and a metallic oxide coated on the surface of the sodium ferric pyrophosphate, a simple continuous ball milling method is used as a synthesis method, the process is simple and easy to copy and amplify, and after the sodium ferric pyrophosphate is coated with the metallic oxide on the surface, the sodium ferric pyrophosphate can be used for preparing the metallic oxide-coated sodium ferric pyrophosphate electrode material. The stability of the material is further improved, the intrinsic ion diffusivity of the material is also obviously improved, the first effect reaches 88% or above, the specific capacity per gram can reach 107 mA h g <-1 >, the capacity retention rate exceeds 90% after 200 cycles, and the electrochemical performance is close to that of other polyanion materials. Therefore, the material is beneficial to large-current charging and discharging and long-time cycle application in a sodium-ion battery material.
Owner:SOUTHWEST UNIVERSITY

Lithium ion battery positive electrode lithium iron pyrophosphate preparation method

The present invention relates to a lithium ion battery positive electrode lithium iron pyrophosphate preparation method, which comprises: 1, mixing a lithium source-containing compound, an iron source-containing compound and a phosphorus source-containing compound, adding a solvent to form a transparent solution containing the lithium compound, the phosphorus compound and the iron compound, placing the transparent solution into an evaporator, and carrying out pressure reducing evaporation to obtain a small volume transparent gel; and 2, carrying out pre-decomposition and high temperature sintering on the small volume transparent gel, and naturally cooling so as to complete the lithium ion battery positive electrode lithium iron pyrophosphate preparation process. According to the present invention, the material synthesized through the wet sol-gel is sequentially subjected to pressure reducing evaporation, pre-decomposition and sintering so as to achieve the uniform molecular level of the raw material mixing, the material synthesis uniformity is good, the particle size is small, the rate performance is good, and the initial charge-discharge efficiency and the discharge capacity are high; and the inexpensive lithium source, the inexpensive iron source, the inexpensive phosphorus source and the doped elements are used so as to achieve the cheap material price, and the materials are easy to store.
Owner:CHINA ELECTRONIC TECH GRP CORP NO 18 RES INST

Composite colostrum and preparation method thereof

The invention provides composite colostrum and a preparation method thereof. The composite colostrum is prepared from the following components in percentage by weight: 20-40% of soybean protein isolate; 5-10% of lactoferrin-containing whey protein, 0.05-0.5% of a transfer factor, 1-10% of bovine colostrum, 3-40% of oligomeric polysaccharide, 1-10% of polydextrose, 1-20% of a traditional Chinese medicinal extract, 0.18-10% of calcium carbonate, 0.013-0.073% of iron pyrophosphate, 0.002-0.128% of zinc oxide, 0.0003-0.022% of vitamin A, 0.000001-0.00045% of vitamin D, 0.005-1.3% of vitamin C, 0.005-0.85% of vitamin E and 0.0001-1% of B-vitamin. The composite colostrum has the advantages that the spleen can be strengthened, the intestinal microenvironment can be improved, the absorption rate of trace elements can be increased, the composite colostrum is better utilized by the human body, and accordingly, the effects of strengthening nutrition and enhancing human immunity are achieved; through the comprehensive synergistic effect of the components, the human immune system can be enhanced, rehabilitation of patients suffering from respiratory diseases such as recurrent respiratory tractinfections is promoted, and the frequency of developing a disease is reduced.
Owner:JIANGXI DETAI MEDICINE BIOTECH CO LTD

Milk powder beneficial to improving immunity, and preparation method of milk powder

The invention discloses a milk powder beneficial to improve immunity, and a preparation method of the milk powder, and relates to the technical field of milk powder production. The milk powder comprises the following raw material components in parts by weight: 280-320 parts of whole milk powder, 40-60 parts of skimmed milk powder, 4-6 parts of lactose, 8-12 parts of whey protein, 4-6 parts of fructo-oligosaccharide, 1.8-2.2 parts of sodium citrate phospholipid, 0.8-1.2 parts of docosahexaenoic acid oil, 0.7-0.9 part of L-sodium ascorbate, 0.4-0.6 part of milk calcium, 0.7-0.9 part of arachidonic acid oil, 0.4-0.6 part of D-calcium pantothenate, 0.5-0.7 part of iron pyrophosphate, 0.5-0.7 part of zinc sulfate, 0.001-0.003 part of d-alpha-tocopherol acetate, 0.04-0.06 part of manganese gluconate, 0.07-0.09 part of nicotinic acid, 0.07-0.09 part of lutein, 0.5-0.7 part of retinyl acetate, 0.4-0.6 part of cholecalciferol, 3-5 parts of Lactobacillus acidophilus, 3-5 parts of Bifidobacteriumlactis HN019, 4-6 parts of Lactobacillus casei, 0.05-0.07 part of phytomenadione, 0.06-0.08 part of thiamine hydrochloride, 0.07-0.09 part of pyridoxine hydrochloride, 0.08-0.12 part of folic acid, 0.8-1.2 parts of lactoferrin, 0.8-1.2 parts of bovine colostrum, and 3-5 parts of a food flavor.
Owner:安徽贝尔宝母婴用品有限公司
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