Ferric pyrophosphate microcapsule powder applied to Vc-containing series products and preparation method thereof
A technology of ferric pyrophosphate and series products, applied in the preparation of microspheres, microcapsule preparation, application, etc., can solve the problems of heavy color, short time, poor dispersion solubility and fluidity, and achieve the effect of light color
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[0023] The present invention also provides a preparation method of ferric pyrophosphate microcapsule powder applied to Vc series products, comprising the following steps:
[0024] S1. Take sodium starch octenyl succinate and maltodextrin as wall materials, and use Span 80 as emulsifier, add them to water above 80°C, stir evenly, add iron pyrophosphate, and use 1000-5000r / min Stir and shear at a rotating speed for 5-10 minutes to form a shear liquid; the solid content in the shear liquid is 30-40%;
[0025] S2. The microcapsule powder is obtained by adopting a milling process.
[0026] In order to improve the preparation efficiency, the wall material and emulsifier are added into high-temperature water above 80°C, stirred evenly and then cooled to room temperature. After adding ferric pyrophosphate, high-speed shearing is adopted, and the high tangential speed generated by the high-speed rotation of the rotor is used to fully mix the wall material, emulsifier, ferric pyrophosp...
Embodiment 1
[0030] Take sodium starch octenyl succinate and maltodextrin as wall materials, add Span 80 to purified water at 90°C, stir well, add ferric pyrophosphate CW-003, stir and shear at 3000r / min for 7min , forming a shear fluid; the mass ratio of the wall material to iron pyrophosphate is 2:1, the addition of Span 80 is 1% of the total mass of the microcapsule powder, and the sodium starch octenyl succinate and maltodextrin in the wall material The mass ratio is 1:3, and the solid content in the shear fluid is 35%;
[0031] Then spray drying, the inlet air temperature is 155°C, and the outlet air temperature is 80°C to obtain microcapsule powder.
Embodiment 2
[0061] Take sodium starch octenyl succinate and maltodextrin as wall materials, add Span 80 to purified water at 90°C, stir well, add ferric pyrophosphate CW-003, stir and shear at 3000r / min for 7min , form shear liquid; The mass ratio of wall material and ferric pyrophosphate is 2:1, and the addition of Span 80 is 0.5%, and the mass ratio of sodium starch octenyl succinate and maltodextrin in the wall material is 1: 3. The solid content in the shear fluid is 35%;
[0062] Then spray drying, the inlet air temperature is 155°C, and the outlet air temperature is 80°C to obtain microcapsule powder.
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