Zirconium-containing composition for zirconium-based amorphous alloy and zirconium-based amorphous alloy
A zirconium-based amorphous alloy and content technology are applied in the field of zirconium-containing compositions and zirconium-based amorphous alloys, which can solve the problems of high zirconium purity requirements and high preparation costs of amorphous alloys, and achieve the effect of reducing preparation costs
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Embodiment 1
[0021] This example illustrates the preparation method of the zirconium raw material and the amorphous alloy using the zirconium raw material of the present invention.
[0022] Vacuumize the vacuum arc melting furnace (Shanghai Chenhua Electric Furnace Co., Ltd.) to 2.0×10 -3 Pa, feed high-purity argon gas with a purity of 99.999% to the arcing pressure of 0.5Mpa; then vacuumize the system to 2.0×10 -3 Pa, and then pass the high-purity argon gas to the arc starting pressure of 0.5MPa. The titanium is then melted to absorb oxygen in a vacuum arc melting furnace.
[0023] Then according to the chemical composition ratio (Zr 62 Al 15 Ni 15 Fe 8 ) 99.7 (B 25 Si 50 Pb 25 ) 0.3 (wherein, the subscripts are mole percentages), zirconium sponge (Shanghai Teye Metallurgical Charge Co., Ltd., purity is 99.4%), B, Si, Pb, Al, Ni and Fe are put into the vacuum arc melting furnace, wherein, The above-mentioned various amorphous alloy raw materials are cleaned and dried with aceto...
Embodiment 2
[0026] This example illustrates the preparation method of the zirconium raw material and the amorphous alloy using the zirconium raw material of the present invention.
[0027] Prepare amorphous alloy samples according to the method of Example 1, the difference is that according to the chemical composition ratio (Zr 62 Al 15 Ni 15 Fe 8 ) 99.1 (B 30 Si 40 Pb 30 ) 0.9 (wherein, the subscripts are mole percentages), zirconium sponge (Shanghai Teye Metallurgical Charge Co., Ltd., purity is 99.4%), B, Si, Pb, Al, Ni and Fe are put into the vacuum arc melting furnace, wherein, The above-mentioned various amorphous alloy raw materials are cleaned and dried with acetone before being put into the vacuum arc melting furnace; relative to 100 parts by weight of sponge zirconium, the amount of the additive is 1.23 parts by weight; the molar amount of B, Si and Pb The ratio is 3:4:3; except for zirconium sponge, the purity of other amorphous alloy raw materials is above 99.9% by wei...
Embodiment 3
[0029] This example illustrates the preparation method of the zirconium raw material and the amorphous alloy using the zirconium raw material of the present invention.
[0030] Prepare amorphous alloy samples according to the method of Example 1, the difference is that according to the chemical composition ratio (Zr 45 Al 20 Ni 20 Fe 15 ) 98.5 (B 25 Si 45 Pb 30 ) 1.5 (wherein, the subscripts are mole percentages), zirconium sponge (Shanghai Teye Metallurgical Charge Co., Ltd., purity is 99.4%), B, Si, Pb, Al, Ni and Fe are put into the vacuum arc melting furnace, wherein, The above-mentioned various amorphous alloy raw materials are cleaned and dried with acetone before being put into the vacuum arc melting furnace; relative to 100 parts by weight of sponge zirconium, the amount of the additive is 2.47 parts by weight; the molar amount of B, Si and Pb The ratio is 5:9:6; except for zirconium sponge, the purity of other amorphous alloy raw materials is above 99.9% by we...
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Abstract
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