Unlock instant, AI-driven research and patent intelligence for your innovation.

Method for preparing wearproof electric corrosion-resisting alloy layer on pure copper surface through magnetron sputtering

A magnetron sputtering and anti-corrosion technology, which is applied in surface polishing machine tools, sputtering coating, metal material coating technology, etc., to achieve high current breaking capacity, good purification and activation effect, and high voltage withstand capacity

Inactive Publication Date: 2010-04-21
HENAN POLYTECHNIC UNIV
View PDF0 Cites 10 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

As a result, copper-based alloys encounter contradictions that are difficult to balance between conductivity, anti-burning loss, anti-welding resistance, and low current interception.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] A pure copper plate with a thickness of 2mm, with a length and width of 10mm×20mm, is coated with a layer of Cu-Cr wear-resistant and anti-corrosion alloy on its surface by magnetron sputtering. The process steps are:

[0025] The first step is to polish the pure copper surface and install it in the furnace, and then vacuumize it to about 5×10 -2 Pa, through argon to 15Pa;

[0026] The second step is to connect the DC power supply A, apply a 200V negative bias voltage between the pure copper parts and the vacuum chamber shell, and purify and activate the pure copper surface through glow ion bombardment, remove the oil film on the surface, and oxidize the surface. film, the bombardment time is 10min, and the DC power supply is turned off;

[0027] The third step, connect the DC power supply B, add 300 volts of negative bias between the Cu-Cr (15%wt) alloy magnetron target and the vacuum chamber shell, and bombard the Cu-Cr alloy target by glow ions, so that Atoms on th...

Embodiment 2

[0030] A pure copper plate with a thickness of 5mm and a length and width of 12mm×25mm is coated with a layer of Cu-Cr wear-resistant and anti-corrosion alloy on its surface by magnetron sputtering. The process steps are the same as above, and the specific parameters are:

[0031] After polishing the pure copper surface, put it into the furnace and vacuumize it to about 10 -1 Pa, pass argon gas to 25Pa; connect the DC power supply A, apply a 300V negative bias voltage between the pure copper parts and the vacuum chamber shell, and purify and activate the pure copper surface by glow ion bombardment to remove pure The oil film and oxide film on the copper surface, the bombardment time is 8min, turn off the DC power supply A; then connect the DC power supply B, and add a 400 volt negative bias between the Cu-Cr (20%wt) alloy magnetron target and the vacuum chamber shell By bombarding the Cu-Cr alloy target with glow ions, the atoms on the surface of the target escape with a certa...

Embodiment 3

[0033] A pure copper plate with a thickness of 8mm and a length and width of 15mm×30mm is coated with a layer of Cu-Cr wear-resistant and anti-corrosion alloy on its surface by magnetron sputtering. The process steps are the same as above, and the specific parameters are:

[0034] Put the pure copper surface into the furnace after polishing, evacuate to about 1Pa, pass argon gas to 30Pa; connect the DC power supply A, apply a 400V negative bias voltage between the pure copper parts and the vacuum chamber shell, and bombard it with glow ions Carry out purification and activation pretreatment to the pure copper surface, remove the oil film and oxide film on the pure copper surface, bombard for 6 minutes, turn off the DC power supply A; A negative bias of 500 volts is applied between the shell and the vacuum chamber, and the Cu-Cr alloy target is bombarded by glow ions, so that the surface atoms of the target escape with a certain energy, and then deposit on the surface of the pur...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention provides a method for preparing an abrasion-resisting electric corrosion-resisting alloy layer on a pure copper surface through magnetron sputtering. The method comprises the following steps: carrying out polishing and deoiling treatments on the pure copper surface and completing furnace charging after airing; carrying out vacuumizing, introducing argon and switching on a direct current power supply A to apply negative bias between a pure copper part and a vacuum chamber shell body; eliminating oil films and oxidation films on the pure copper surface through glow ion bombardment, and turning off the direct current power supply A; switching on a direct current power supply B to apply negative bias between a Cu-Cr alloy magnetron target and the vacuum chamber shell body, and bombarding the magnetron target through glow ion to ensure that target atoms are deposited on the pure copper surface to form an even Cu-Cr alloy layer; and turning off the direct current power supply B, cooling the alloy layer under the protection of argon and polishing the alloy layer after furnace discharging. By adopting the method, an alloy layer with ideal abrasion resistance and electric corrosion resistance can be obtained on the pure copper surface; and the central part of the alloy layer maintains the excellent electric conductivity of pure copper, while the surface fully shows the characteristics of Cu-Cr alloy such as high current breaking capacity and voltage enduring capacity, ideal fusing soldering resistance, low electric arc burning loss rate and abrasion rate and the like.

Description

Technical field: [0001] The invention belongs to the technical field of surface modification of metal materials, and in particular relates to a method for preparing a wear-resistant and anti-corrosion alloy layer by magnetron sputtering on a pure copper surface. Background technique: [0002] Pure copper has excellent electrical and thermal conductivity, and is widely used in conductive components, heat transfer elements of heat exchangers and other components. However, in some applications, especially those requiring wear and corrosion resistance, pure copper obviously shows its own shortcomings. [0003] Take the electrical contacts of conductive components as an example. The electrical contact is the key component of the vacuum circuit breaker. The ideal electrical contact material should have the following properties: ① High current breaking capacity; ② High voltage withstand capacity; ③ High electrical conductivity and thermal conductivity; ④ Anti-welding performance ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C23C14/35C23C14/16C23C14/02C23C14/58C23C14/54C23G5/024B24B29/02
Inventor 袁庆龙侯文义曹晶晶苏志俊冯旭东
Owner HENAN POLYTECHNIC UNIV