Infrared spectrum detection method of ginseng and astragalus injection liquid
A technology of Shenqi injection and infrared spectroscopy, which is applied in the field of traditional Chinese medicine detection, can solve the problems of poor accuracy and reproducibility, long time required, and high cost, and achieve the effect of strong characteristics and small sampling volume
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Embodiment 1
[0028] Embodiment 1: a kind of infrared spectrum detection method of Shenqi injection, the method comprises the following steps: a, injection sample processing: adopt KBr adsorption method, get 0.07 milliliter of Shenqi injection and place in evaporating dish, add 80 milligrams The KBr spectrum is pure, evaporated to dryness on a water bath at 80 degrees Celsius, then scraped off, then added 65 mg of KBr, mixed and ground fully and evenly, and then pressed into tablets; Detect in the IR spectrum detector, measure the infrared spectrogram of the tablet sample; c, standard comparison: select 1 batch of Radix Codonopsis contrast medical materials, draw Radix Codonopsis infrared spectrum, find out 779, 818, 867, 1056 nearby specific substances according to Radix Codonopsis infrared spectrum Characteristic peaks; then select 10 batches of Shenqi injection control samples, draw infrared spectra, and use software to average the above spectra as standard control spectra. d, compare th...
Embodiment 2
[0029] Embodiment 2: a kind of infrared spectrum detection method of Shenqi injection, the method comprises the following steps: a, injection sample processing: adopt KBr adsorption method, get 0.15 milliliter of Shenqi injection and place in evaporating dish, add 100 milligrams The KBr spectrum is pure, evaporated to dryness on a water bath at 90 degrees Celsius, then scraped off, then added 75 mg of KBr, mixed and ground fully and evenly, and then pressed into tablets; Detect in the IR spectrum detector, measure the infrared spectrogram of the tablet sample; c, standard comparison: select 1 batch of Radix Codonopsis contrast medical materials, draw Radix Codonopsis infrared spectrum, find out 779, 818, 867, 1056 nearby specific substances according to Radix Codonopsis infrared spectrum Characteristic peaks; then select 10 batches of Shenqi injection control samples, draw infrared spectra, and use software to average the above spectra as standard control spectra. d, compare t...
Embodiment 3
[0030] Embodiment 3: a kind of infrared spectrum detection method of Shenqi injection, the method comprises the following steps: a, injection sample processing: adopt KBr adsorption method, get 0.20 milliliter of Shenqi injection and place in evaporating dish, add 120 milligrams The KBr spectrum is pure, evaporated to dryness on a water bath at 100 degrees Celsius, then scraped off, then added 80 mg of KBr, mixed and ground fully and evenly, and then pressed into tablets; Detect in the IR spectrum detector, measure the infrared spectrogram of the tablet sample; c, standard comparison: select 1 batch of Radix Codonopsis contrast medical materials, draw Radix Codonopsis infrared spectrum, find out 779, 818, 867, 1056 nearby specific substances according to Radix Codonopsis infrared spectrum Characteristic peaks; then select 10 batches of Shenqi injection control samples, draw infrared spectra, and use software to average the above spectra as standard control spectra. d, compare ...
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