7results about How to "Method stable" patented technology

The invention relates to a detection method of a medicine for dispelling wind and eliminating dampness. The detection method comprises the following steps: thin-layer identification of a notopterygium root medicinal material, thin-layer identification of a radix angelicae pubescentis medicinal material, thin-layer identification of a radix saposhnikoviae medicinal material, thin-layer identification of ligusticum and ligusticum wallichii medicinal materials, and thin-layer identification of a honey-fried licorice root medicinal material. Through methodological investigation, the detection method has the effects of strong specificity, good durability, clear spots after thin layer expansion, satisfactory separation degree and the like, can effectively control the product quality condition, improves the product quality detection standard, and ensures the product quality.

This invention relates to the field of alloy purification technology, specifically to a method, system, and aluminum alloy welding material for preparation of self-purifying aluminum alloy welding material. The method for preparing the self-purifying aluminum alloy welding material includes the following steps: cold pressing a mixture of aluminum alloy powder and refining agent powder to obtain a cold-pressed billet; hot pressing the cold-pressed billet to obtain a hot-pressed aluminum ingot; removing impurities from the surface of the hot-pressed aluminum ingot, followed by preheating to obtain a preheated ingot; and extruding the preheated ingot into wire. This invention uses powder metallurgy to prepare aluminum alloy welding material with self-purifying function, extending the degassing method of aluminum alloy smelting to the aluminum alloy welding process. This relaxes the strict requirements on the hydrogen content of the aluminum alloy base material, achieving a weld with lower hydrogen content. The method is more efficient, more stable, and less expensive.

The invention relates to a magnesium-based hydrogen storage material and a preparation method thereof, and belongs to the technical field of hydrogen storage alloy materials and preparation thereof. The hydrogen storage material is an Mg-5Ni alloy with Sm powder uniformly distributed on the surface layer and an amorphous / nanocrystalline structure in the interior. The Sm powder is wrapped by the surface layer of the Mg-5Ni alloy to form composite powder of a core-shell structure; the hydrogen storage material is prepared from Mg-5Ni alloy powder and Sm powder as raw materials, and the raw materials are mixed and then subjected to dry ball milling. The hydrogen absorption and desorption kinetics of the existing magnesium-based hydrogen storage material can be effectively improved, the hydrogen desorption activation energy of the magnesium-based hydrogen storage material is reduced, and the problem that a solid additive is difficult to uniformly distribute on the surface is solved.

The application discloses a kind of characteristic chromatogram detection methods of Qinggan Jieyu granules. After the solvent and microporous filter membrane treatment of Qinggan Jieyu granules, different batches of test solution are obtained, and the chromatogram of each is obtained by preparing the reference solution; the chromatogram of different batches of test solution and reference solution is combined to obtain the characteristic chromatogram and characteristic chromatographic peak of control, and then the relative retention time of the characteristic chromatographic peak and reference berberine hydrochloride peak solution is used to obtain the relative retention time of the control characteristic chromatogram as the specified value; the chromatogram is obtained by detecting the to-be-tested granules, and S peak correction is carried out, and the detection result is obtained by comparing the specified value of relative retention time. The characteristic chromatogram detection method of Qinggan Jieyu granules established by the application is simple in operation, reliable in result, high in stability and precision, and good in repeatability; the characteristic chromatogram of Qinggan Jieyu granules provided by the application can comprehensively and effectively control the quality of the preparation, and ensure the stability, reliability and safety of the preparation.

The application discloses a kind of continuous flow photocatalytic decarboxylation preparation biological hydrocarbon method, belong to the technical field of biofuel preparation.The method includes the following steps: high fatty acid compound, hydrogen atom transfer catalyst and acridine photocatalyst are dissolved in organic solvent, and mixed solution is obtained;The mixed solution is passed into circulating continuous flow light reactor, and photocatalytic decarboxylation reaction is carried out at room temperature for 12-24 hours, and reaction liquid is obtained;Reaction liquid is separated by reduced pressure distillation, and the biological hydrocarbon compound after decarboxylation is obtained.The application uses continuous flow light reactor to strengthen mass transfer and heat transfer efficiency, solves the problem that light penetration depth is limited in traditional batch photoreactor, and reaction is not uniform;Metal-free catalytic system is used, and the use of noble metal and potential residual risk is avoided.The method has mild reaction condition, higher product yield, good atom economy, and for unsaturated high fatty acid, olefin configuration can be maintained before and after decarboxylation, and has good industrial application prospect.

The application belongs to the technical field of biomedicine, and specifically discloses a squamous cell carcinoma antigen determination kit and application, which comprises anti-reagent A, anti-reagent B and magnetic micro-particle reagent, wherein the anti-reagent A is a biotin-labeled squamous cell carcinoma antigen antibody; the anti-reagent B is an alkaline phosphatase-labeled squamous cell carcinoma antigen antibody; the squamous cell carcinoma antigen determination kit can effectively detect the concentration of squamous cell carcinoma antigen (SCC) in serum and plasma samples, and is mainly used for the treatment monitoring of cervical cancer, non-small cell carcinoma and the like, and has a wide application prospect.

The application provides a kind of method and system for dissimilar metal molten pool flow visualization based on synchrotron radiation.The method comprises preparing dissimilar metal sample;Clamping dissimilar metal sample in sample clamping table, adjusting the X-ray incident direction of synchrotron imaging device to penetrate dissimilar metal sample;Irradiate dissimilar metal sample with laser;Transmitting imaging of mixed molten pool is carried out using synchrotron radiation source, and a sequence of transmission imaging is obtained;The transmission imaging sequence is analyzed to obtain the dynamic migration and flow pattern image information and data of the metal in the mixed molten pool.The method does not need to introduce tracer particles or bubbles, and does not change the intrinsic flow of the molten pool;The imaging contrast is high, the space-time resolution is high, the real and repeatable molten pool internal flow field information can be obtained, and it is suitable for the molten pool dynamics research and mechanism analysis in the process of laser welding and additive manufacturing, to provide reliable data support for molten pool flow model verification and process optimization.