Therapeutic compounds and their use in treating diseases and disorders
A compound and halogen technology, applied in the direction of carbohydrate active ingredients, metabolic diseases, allergic diseases, etc., can solve the problems that cannot be treated, cancer cannot be cured, and become resistant to standard treatment regimens, etc.
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[0391] Chemical Synthesis and Purification of Example Compounds
[0392] All reactions were performed in flame-dried or oven-dried glassware under positive pressure of dry nitrogen or dry argon with magnetic stirring unless otherwise indicated. Chemicals were purchased from standard commercial vendors and used as received unless otherwise noted. Additionally, their preparation is readily and well known to those of ordinary skill in the art, or such preparation is mentioned or illustrated herein. The yield is not optimal. The names of the example compounds and intermediates were either obtained using the "ACD / Name" chemical naming software (version 8.08) from Advanced Chemistry Development, Inc. (Toronto, Ontario, Canada) or from MDL Information Systems (i.e. Isis, a Symyx Technologies, Inc. division (Santa Clara, CA) TM Generated by the "Autonom 2000" plug-in program of / Draw 2.5SP1 chemical drawing program.
[0393] Use analytical TLC plate (Silica Gel 60F254 or Merck EM-57...
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