Methylprednisolone sodium succinate freeze dried powder injection and preparation method thereof
A kind of technology of methylprednisolone sodium succinate and freeze-dried powder injection, applied in the field of methylprednisolone sodium succinate composition, can solve problems such as low production efficiency
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[0017]
[0018] The preparation method is as follows:
[0019] 1. Weigh the prescription amount of NaHCO 3 , add 500ml of water for injection to dissolve, set aside.
[0020] 2. Weigh the prescription amount NaH 2 PO 4 ·H 2 O, add 500ml of water for injection to dissolve, set aside.
[0021] 3. Weigh the prescription amount Na 2 HPO 4 , add 500ml of water for injection to dissolve, set aside.
[0022] 4. Weigh the main drug of the prescribed amount, add 2500ml water for injection to stir into a suspension, and slowly add NaHCO under constant stirring 3 solution, heated to 40-50°C in a water bath and stirred, adding NaH 2 PO 4 ·H 2 O solution, followed by Na 2 HPO 4 Adjust the pH value of the solution, make up water for injection to 5000ml, keep warm in a water bath until the solution is clear, and circulate and filter the whole amount.
[0023] 5. Filter the medicinal solution with a 0.45 μm microporous membrane, and finally fine filter with a 0.22 μm microporo...
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